Internal deterioration of concrete by the oxidation of pyrrhotitic aggregates

This paper presents research results on the causes of a severe concrete deterioration, which occurred in many building foundations approximately 2 years after construction. Concrete samples were investigated with X-ray diffraction (XRD) analysis, a scanning electron microscope (SEM) and a petrographic examination performed with a stereomicroscope. It was found that the early cracking of concrete stemmed from the oxidation of the pyrrhotite found in the anorthosite aggregates used to produce the concrete. The oxidation process led to the precipitation of iron hydroxides having a higher volume than the original pyrrhotite does. The presence of micas (biotite) close to the pyrrhotite seemed to promote and accelerate the oxidation process.     

Comparative morphology of leaf epidermis in eight populations of Atlas Pistachio (Pistacia atlantica Desf., Anacardiaceae)

A comparative analysis was undertaken to conduct a micromorphological study of Pistacia atlantica leaves by comparing different populations grown under different climatic conditions. Leaf epidermis of eight wild populations was investigated under scanning electron microscope. Micromorphological characteristics (epidermis ornament, stomata type, waxes as well as trichomes) of the adaxial and abaxial leaf surfaces were examined. The epidermis ornament varied among populations and leaf surface, the abaxial leaf surface is reticulate with a striate surface. Messaad site shows a smooth uneven surface. The adaxial leaf surface is smooth but several ornamentations can be seen. The leaflet is amphistomatic; the stomata appeared to be slightly sunken. A variety of stomatal types were recorded; actinocytic and anomocytic types are the most frequent. The indumentum consisted of glandular and nonglandular trichomes. Unicellular glandular trichomes are recorded for P. atlantica leaves in this study. Their density is higher in Oued safene site, located at the highest altitude in comparison with the other populations. The wax occurred in all the sites and its pattern varied according to the populations studied, particularly between Berriane and Messaad. The morphological variability exhibited by the eight populations of P. atlantica may be interpreted as relevant to the ecological plasticity and the physiological mechanisms involved are discussed in this report.     

Diffusion-limited evaporation of thin polar liquid films

The stability of evaporating very thin films of a polar liquid is investigated. The microscopic interaction with the substrate and capillarity are taken into account in a lubrication equation. The stability of a flat interface is studied when evaporation is limited by the diffusion of the vapour in the gas phase. The evaporation rate is computed and evaporation is shown to be stabilizing. A stability phase diagram is obtained. A weakly nonlinear analysis leads to a film-thickness amplitude equation that is non local in space. Physical consequences of the results are eventually discussed.     

Study of thermal and acoustic noise interferences in low stiffness atomic force microscope cantilevers and characterization of their dynamic properties

The atomic force microscope (AFM) is a powerful tool for the measurement of forces at the micro/nano scale when calibrated cantilevers are used. Besides many existing calibration techniques, the thermal calibration is one of the simplest and fastest methods for the dynamic characterization of an AFM cantilever. This method is efficient provided that the Brownian motion (thermal noise) is the most important source of excitation during the calibration process. Otherwise, the value of spring constant is underestimated. This paper investigates noise interference ranges in low stiffness AFM cantilevers taking into account thermal fluctuations and acoustic pressures as two main sources of noise. As a result, a preliminary knowledge about the conditions in which thermal fluctuations and acoustic pressures have closely the same effect on the AFM cantilever (noise interference) is provided with both theoretical and experimental arguments. Consequently, beyond the noise interference range, commercial low stiffness AFM cantilevers are calibrated in two ways: using the thermal noise (in a wide temperature range) and acoustic pressures generated by a loudspeaker. We then demonstrate that acoustic noises can also be used for an efficient characterization and calibration of low stiffness AFM cantilevers. The accuracy of the acoustic characterization is evaluated by comparison with results from the thermal calibration.     

Fast Fourier and discrete wavelet transforms applied to sensorless vector control induction motor for rotor bar faults diagnosis

This paper presents new techniques to evaluate faults in case of broken rotor bars of induction motors. Procedures are applied with closed-loop control. Electrical and mechanical variables are treated using fast Fourier transform (FFT), and discrete wavelet transform (DWT) at start-up and steady state. The wavelet transform has proven to be an excellent mathematical tool for the detection of the faults particularly broken rotor bars type. As a performance, DWT can provide a local representation of the non-stationary current signals for the healthy machine and with fault. For sensorless control, a Luenberger observer is applied; the estimation rotor speed is analyzed; the effect of the faults in the speed pulsation is compensated; a quadratic current appears and used for fault detection.     

Antioxidant and anticholinesterase activity of essential oils and ethanol extracts of <Emphasis Type="Italic">Thymus algeriensis</Emphasis> and <Emphasis Type="Italic">Teucrium polium</Emphasis> from Algeria

This study aimed to investigate the cholinesterase (ChE) inhibitory and antioxidant activities of essential oil (EO) and ethanolic extract (EE) of two Lamiaceae medicinal plants from Algeria: Thymus algeriensis Boiss. & Reut. and Teucrieum polium subsp capitatum. The chemical composition of EOs analyzed by GC and GC–MS revealed the presence of carvacrol (43.2%), p-cymene (18.7%) and γ-terpinene (14.8%) as major compounds in T. algeriensis, while germacrene D (25.0%), bicyclogermacrene (10.4%), β-pinene (11.3%) and spathulenol (5.8%) were the most important components in T. polium oil. The best inhibitory activity on acetylcholinesterase (AChE) was exhibited by the EO of T. algeriensis. On the other hand, T. polium oil was more efficient against butyrylcholinesterase (BChE) than against AChE, whereas EEs showed weak or no inhibitory effect, particularly against AChE. Antioxidant activity was evaluated by β-carotene bleaching, ferric and cupric reducing powers and inhibition of ABTS^?+, DPPH^? and superoxide radicals. EOs showed different antioxidant trends depending on the assay used while ethanol extracts had high activity with all tests.     

Adaptive noise reduction using numerically stable fast recursive least squares algorithm

This paper is concerned with adaptive noise reduction based on the fast recursive least squares (FRLS) algorithm. It is well known that the fast recursive least squares (FRLS) algorithm suffers from numerical instability when operating under the effects of finite precision arithmetic. Several numerical solutions of stabilization were proposed in the case of stationary signals. In this work a new version of a numerically stable FRLS algorithm (NS‐FRLS) is proposed. The stability characteristics of this new stabilized algorithm are analysed. The analysis is based on a linear model for the errors in the states of the adaptive filter. Experimental results confirm the merits of adaptive filtering with the NS‐FRLS algorithm over optimum filtering using the solution provided by Wiener–Hopf equations. Copyright © 2006 John Wiley & Sons, Ltd.     

A numerical method for nonlinear complex modes with application to active–passive damped sandwich structures

In this paper, a numerical method is proposed for determining complex vibrations modes of sandwich structures with piezoelectric and viscoelastic layers. Based on homotopy and asymptotic numerical techniques, this method leads to the damping properties calculation (loss factor and natural frequency per mode) of the hybrid sandwich structure. The numerical results of the loss factor and natural frequency are compared to those obtained from analytical beam model and from numerical studies the modal strain energy method.     

Effect of the type of superplasticizer on the properties of cementitious systems incorporating slag

Superplasticizers have become an integral ingredient in the formulation of concretes. After 40?years, their use and dosage remain uncertain due to variations in their compositions and those of cement. In addition, the substitution of cement by supplementary cementitious materials having different chemical compositions exacerbates the problem without counting the multiplicity of superplasticizers to choose from. The present work consists of a study of the rheological and mechanical properties of cementitious systems containing slag and various types of superplasticizers. The tests were carried out on pastes, mortars and concretes incorporating slag in partial cement replacement and four superplasticizers types, polynaphthalene sulphonate (PNS) and three polycarboxylates (PC). The results of this study demonstrate that the viscosity and the yield stress increase with the rate of incorporation of the slag. The air increases with the polycarboxylates but this effect is less perceptible in the presence of the slag. Polycarboxylates improve workability more than PNS. The use of polycarboxylates reduces the viscosity and the yield stress. The compressive strength of concretes containing slag is low at early age but high at long run. They exhibit good resistances to scaling. The permeability to chloride ions is considerably reduced in the presence of the slag independently of the type of superplasticizer, suggesting good durability of these concretes in potentially aggressive external environments.