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Assem Barakat Mousa Al-Noaimi Mohammed Suleiman Abdullah S. Aldwayyan Belkheir Hammouti Taibi Ben Hadda Salim F. Haddad Ahmed Boshaala Ismail Warad 《International journal of molecular sciences》2013,14(12):23941-23954
[NiCl2(C14H12N2)(H2O)] complex has been synthesized from nickel chloride hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired complex, subjected to thermal decomposition at low temperature of 400 ºC in an open atmosphere, revealed a novel and facile synthesis of pure NiO nanoparticles with uniform spherical particle; the structure of the NiO nanoparticles product was elucidated on the basis of Fourier transform infrared (FT-IR), UV-vis spectroscopy, TG/DTA, XRD, scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDXS) and transmission electron microscopy (TEM). 相似文献
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Venkatesan A. Muthuvel A. Mohana V. Mahendran N. Al-Zaqri Nabil Boshaala Ahmed Warad Ismail 《Journal of Materials Science: Materials in Electronics》2022,33(27):21246-21257
Journal of Materials Science: Materials in Electronics - The green pigment cobalt aluminate nanoparticles have been prepared by the simple and cost-effective co-precipitation method. And also, the... 相似文献
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Warad I Omar Abd-Elkader H Al-Resayes S Husein A Al-Nuri M Boshaala A Al-Zaqri N Ben Hadda T 《International journal of molecular sciences》2012,13(5):6279-6291
Novel hybrid xerogel materials were synthesized by a sol-gel procedure. n-octadecyltriethoxysilane was co-condensed with and without different cross-linkers using Q(0) and T(0) mono-functionalized organosilanes in the presence of n-hexadecylamine with different hydroxyl silica functional groups at the surface. These polymer networks have shown new properties, for example, a high degree of cross-linking and hydrolysis. Two different synthesis steps were carried out: simple self-assembly followed by sol-gel transition and precipitation of homogenous sols. Due to the lack of solubility of these materials, the compositions of the new materials were determined by infrared spectroscopy, (13)C and (29)Si CP/MAS NMR spectroscopy and scanning electron microscopy. 相似文献
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Al-Zaqri Nabil Umamakeshvari K. Mohana V. Muthuvel A. Boshaala Ahmed 《Journal of Materials Science: Materials in Electronics》2022,33(15):11864-11880
Journal of Materials Science: Materials in Electronics - In the present work, we report the biosynthesis of Nickel oxide (NiO) nanoparticles using Senna auriculata aqueous flower extract and their... 相似文献
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