汽车自动传动液的研制

介绍了自动传统液的分类规格、自动传动液的特性和相关的评定方法；研制了无锌和低锌配方的两种产品，经评定试验和实机使用，符合ＤｅｘｒｏｎⅡＤ、Ｍｅｒｃｏｎ和ＡｌｌｉｓｏｎＣ－４的规格要求，达到了国外同类产品的质量水平。     

Advance of gene therapy for neurological diseases by direct in vivo gene transfer

Gene therapy for neurological diseases is a rapidly expanding field in neurosciences. It has been demonstrated that some viral vectors from HSV-1 (herpes simplex virus type 1), Ad (adenovirus) and AAV (adeno-associated virus) can transfer foreign genes into nondividing cell types (including neurons). In addition, physical/chemical methods are also used in direct in vivo gene transfer. The direct gene transfer techniques will open a new way to study neurophysiology, neuropathology and therapy for neurological diseases at molecular level. They will hopefully lead to surprising progress in gene therapy for neurological diseases.     

二辊轧机轧辊堆焊新技术应用

介绍了二辊粗轧机轧辊利用堆焊新技术开展堆焊修复试验与应用，并介绍了堆焊材料的选择、堆焊工艺以及取得的良好效果。     

First-Principles Study of the High-Temperature Behaviors of the Willemite-Ⅱ and Post-Phenacite Phases of Silicon Nitride

The structural and elastic properties of the recently-discovered wⅡ- and δ-Si_3N_4 are investigated through the plane-wave pseudo-potential method within ultrasoft pseudopotentials.The elastic constants show that wⅡ- and δ-Si_3N_4 are mechanically stable in the pressure ranges of 0-50 GPa and 40-50 GPa,respectively.The α→wⅡ phase transition can be observed at 18.6 GPa and 300 K.The β→δ phase transformation occurs at pressures of 29.6,32.1,35.9,39.6,41.8,and 44.1 GPa when the temperatures are100,200,300,400,500,and 600 K,respectively.The results show that the interactions among the N-2s,Si-3s,3p bands(lower valence band) and the Si-3p,N-2p bands(upper valence band) play an important role in the stabilities of the wⅡ and S phases.Moreover,several thermodynamic parameters(thermal expansion,free energy,bulk modulus and heat capacity) of δ-Si_3N_4 are also obtained.Some interesting features are found in these properties.δ-Si_3N_4 is predicted to be a negative thermal expansion material.The adiabatic bulk modulus decreases with applied pressure,but a majority of materials show the opposite trend.Further experimental investigations with higher precisions may be required to determine the fundamental properties of wⅡ- andδ-Si_3N_4.     

原位模板法在铝基底上制备TiO2纳米管阵列薄膜

采用液相沉积法，将铝基多孔阳极氧化铝（AAO）模板浸入到（NH4）2TiF6溶液中，制备出高度有序的TiO2纳米管阵列薄膜，并在不同的温度下进行了热处理。用场发射扫描电子显微镜、透射电子显微镜和X射线衍射仪等手段对试样的微观形貌、结构及物相进行了表征。结果表明，TiO2纳米管的形貌依赖于AAO的特征，薄膜是由外径大约200nm，壁厚约40nm的TiO2纳米管阵列组成，薄膜厚度约25μm。原位模板法制备的TiO2纳米管阵列薄膜为非晶态，在400℃空气中焙烧2h转变为锐钛矿相TiO2。经过650℃焙烧仍保持纳米管结构，表现出较好的热稳定性。     

电脉冲孕育处理Al-22Si合金衰退性的研究

研究了电脉冲孕育处理后不同静置时间对Al-22Si合金凝固组织中初生相形态、大小、分布的影响。结果表明，电脉冲处理后立刻浇注对Al-22Si合金有较明显的变质作用，初生Si相形态由粗大板条状变为块状，其平均尺寸由153．15μm降至77．35μm，分布也较均匀；但电脉冲处理也存在着较明显的衰退性，即随着熔体静置时间的延长孕育效果逐渐消失，当静置时间为80min时，其组织形态与未经电脉冲处理的组织相似，其平均尺寸由77．35μm升至143．67μm。     

电脉冲孕育处理对Al-5Cu合金热裂的影响

研究了不同电脉冲孕育处理参数对Al-5Cu合金热裂倾向的影响.结果表明,不同电脉冲孕育处理参数均可降低Al-5Cu合金的热裂倾向,处理后该合金热裂临界应力比未处理试样提高了约3倍.合金热裂倾向改善的原因是,电脉冲孕育处理细化了Al-5Cu合金组织,减少了共晶相的数量,缩短了合金凝固温度区间.     

Influences of Ta, Nb, or Mo additions in Zr-based bulk metallic glasses on microstructure and thermal properties

The master-alloy ingots for casting bulk metallic glasses are routinely prepared by arc melting a mixture of pure elements. This paper addresses the difficulty in achieving complete and homogeneous melting of refractory component additions in Zr-based BMGs using the above procedure, and its influences on the microstructure and thermal behavior of alloys.     

Effect of porosity and hydrostatic pressure on water absorption in a semicrystalline fluoropolymer

This paper discusses the effect of porosity and hydrostatic pressure on diffusion kinetics and equilibrium water uptake in a semicrystalline fluoropolymer. Water sorption experiments at atmospheric pressure and under water pressures up to 250 MPa were carried out during 18 months at 40 °C on reference and porous samples. Porosity of samples was induced due to a cavitation process occurring at the highest triaxiality area of waisted and notched specimens during tensile tests. Water uptake was found to be very sensitive to porosity, showing an increase in samples with a high void fraction. On the other hand, water content decreased with increasing pressure suggesting a compaction of the porous space in which water can be stored. Two models describing this water uptake behaviour were considered. The first is a classical model which assumes that sorption occurs only by diffusion following Fick’s law. Fick’s model was found to be in agreement with the experimental results. A “Langmuir-type” sorption model was also proposed to describe water uptake in porous samples, considering a two-phase water transport mechanism: one portion of the absorbed water diffuses through the polymer matrix and the other portion is stored in voids. This model was implemented in a user subroutine using ABAQUS? software and simulations were confronted to experimental sorption curves showing satisfactory agreements. The potential of the Langmuir-type sorption model resides on its availability to be coupled to a poro-mechanical model, in order to improve the understanding of coupling between the mechanical behaviour and water sorption mechanism in a porous polymer.