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M. Del C. Ruiz J. A. González J. B. Rivarola 《Metallurgical and Materials Transactions B》2004,35(3):439-448
The mechanism and kinetics of β-Ta2O5 chlorination, mixed with sucrose carbon, have been studied by a thermogravimetric technique. The investigated temperature
range was 500 °C to 850 °C. The reactants and reaction residues were analyzed by scanning electronic microscopy (SEM), X-ray
diffraction (XRD), and Brunauer-Emmett-Teller method for surface area (BET). The effect of various experimental parameters
was studied, such as carbon percentage, temperature, chlorine partial pressure, and flow, use of the multiple sample method,
and carbon previous oxidation. The carbon percentage and previous treatment have an effect on the system reactivity. The temperature
has a marked effect on the reaction rate. In the 500 °C to 600 °C temperature interval, the apparent activation energy is
144 kJ/mol of oxide, while at higher temperatures, the activation energy decreases. With high chorine partial pressures, the
order of reaction is near zero. The kinetic contractile plate model, X=kt, considering carbon oxidation as the controlling stage, is the one with the best fit to the experimental data. A probable
mechanism for the carbochlorination of β-Ta2O5 is proposed: (1) activation of chlorine on the carbon surface, (2) chlorination of Ta2O5, (3) oxidation of carbon, and (4) recrystallization of β-Ta2O5. 相似文献
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The effect of 2,4-dichlorophenoxyacetic acid (2,4-D) on the in vitro synthesis of proteins was studied in Chinese hamster ovary cells. A remarkable inhibition of the synthesis of proteins was observed when cells grew for 24 h in presence of 1 mM 2,4-D. This effect was reversed by adding 0.1 mM of the three polyamines (putrescine, spermidine and spermine) to the cultured cells. The mRNA is not altered, indicating that the 2,4-D action is located at a different locus, which may be the ribosomes. From these studies, one can speculate that the alterations in the protein synthesis may be a consequence of the effect of 2,4-D on the polyamine metabolism. 相似文献
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Prati C. Rocca F. Kost Y. Damonti E. 《Geoscience and Remote Sensing, IEEE Transactions on》1991,29(6):934-941
For high-quality SAR (synthetic aperture radar) processing, the Doppler centroid frequency is needed. However, SAR data are sampled along the azimuth direction at the pulse repetition frequency (PRF); the estimation of the Doppler centroid frequency by means of spectral analysis techniques may produce ambiguous results due to aliases. The mathematical expression of the residual error that occurs when SAR data are focused with an incorrect alias of the PRF is thus derived. Then, a blind deconvolution technique is used to estimate the actual PRF replica from the focused image. Squinted X -band data, corresponding to those that will be generated by the SIR-C mission, have been generated from the JPL-AirSAR L - and C -band data by means of an inversion of the focusing process. Even if the real data may show differences with respect to the simulated data, the blind deconvolution method appears to be more precise and robust than the other conventional techniques tested 相似文献
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The kinetics of the chlorination reaction of molybdenum trioxide with gaseous carbon tetrachloride has been studied at temperatures between 713 and 753 K. The effects of temperature, reaction time, residence time and gaseous reactant concentration on conversion were studied throughout the reaction. In all cases, there was an increase in conversion when the above operating variables were increased. The kinetic model proposed is consistent with and correlates the experimental data. In the range studied for the different variables, the step that controls the rate of reaction is the surface chemical reaction. Values of the rate constant and the activation energy were estimated. 相似文献
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Watson M.E. Chilla J.L.A. Rocca J.J. Kim J.-W. Lile D.L. Vogt T.J. Robinson G.Y. 《Quantum Electronics, IEEE Journal of》1995,31(2):254-260
We report modulation saturation and time response measurements on InGaAs-InGaP MQW modulators. The measurements yield a saturation intensity of (3.7±0.1) kW/cm2 for a 0-10 V swing and switching times between 10 and 90 ns, depending on the bias voltage and incident light intensity. The observed dependence indicates that field screening due to carrier build-up is the dominant physical mechanism determining both the speed and the saturation intensity. This conclusion is supported by results of theoretical calculations 相似文献
10.
Crystallization of hydrogenated sunflower-cottonseed oil 总被引:1,自引:0,他引:1
G. Rivarola J. A. Segura M. C. Añón A. Calvelo 《Journal of the American Oil Chemists' Society》1987,64(11):1537-1543
Crystal structures formed during solidification of hydrogenated cottonseed oil, sunflowerseed oil and their blends were analyzed
by using an X-ray diffraction technique, differential scanning calorimetry (DSC) and polarized light microscopy. Temperatures
and times of crystallization under conditions which tend to produce β′ type structures were determined in terms of refrigeration
parameters. Microscopy with polarized light also helped clarify some aspects of the tridimensional network of crystals that
contribute to the consistency of products made from hydrogenated oils. 相似文献