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排序方式: 共有105条查询结果,搜索用时 15 毫秒
1.
N. M. Sanghavi Hema Venkatesh Varsha Tandel 《Drug development and industrial pharmacy》1994,20(7):1275-1283
Gilbenclamide, a widely used potent hypoglycaemic agent was solubllized using β -Cyclodextrin and β -Cyclodextrin derivatives. Complexes were prepared by kneading method in a molar ratio of 1:1 of the drug and the cyclodextrlns respectively. The Glibenclamide β -Cyelocextrin complex was characterized and evaluated by I.R. studies, Differential Scanning Calorimotry 6 X-ray diffractometry. The in-vitro dissolution rates of drug from inclusion complexes of β Cyclodextrins and its derivatives were compared. A significant Improvement In dissolution lor, rates of Gllbenclamide was observed with Inclusion complexes of all the Cyclodextrins. However, the solubilizing effect was more in case of β-Cyclodextrin derivatives. 相似文献
2.
An improved analytical model for the current-voltage (I-V) characteristics of the 4H-SiC metal semiconductor field effect transistor (MESFET) on a high purity semi-insulating (HPSI) substrate with trapping and thermal effects is presented. The 4H-SiC MESFET structure includes a stack of HPSI substrates and a uniformly doped channel layer. The trapping effects include both the effect of multiple deep-level traps in the substrate and surface traps between the gate to source/drain. The self-heating effects are also incorporated to obtain the accurate and realistic nature of the analytical model. The importance of the proposed model is emphasised through the inclusion of the recent and exact nature of the traps in the 4H-SiC HPSI substrate responsible for substrate compensation. The analytical model is used to exhibit DC I-V characteristics of the device with and without trapping and thermal effects. From the results, the current degradation is observed due to the surface and substrate trapping effects and the negative conductance introduced by the self-heating effect at a high drain voltage. The calculated results are compared with reported experimental and two-dimensional simulations (Silvaco®-TCAD). The proposed model also illustrates the effectiveness of the gate-source distance scaling effect compared to the gate-drain scaling effect in optimizing 4H-SiC MESFET performance. Results demonstrate that the proposed I-V model of 4H-SiC MESFET is suitable for realizing SiC based monolithic circuits (MMICs) on HPSI substrates. 相似文献
3.
Vivek Baban Borhade Hema Ajit Nair Chandrashekhar R. Barhate 《Drug development and industrial pharmacy》2013,39(4):440-448
A new, simple, and rapid high-performance thin-layer chromatographic method with a derivatization procedure was developed and validated for quantitative determination of tacrolimus. Tacrolimus was chromatographed on silica gel 60 F254 TLC plate using toluene–acetonitrile–glacial acetic acid (6:4:0.1, by volume) as mobile phase. Tacrolimus was visualized using a derivatization reagent containing anisaldehyde–sulfuric acid in absolute alcohol and quantified by densitometric analysis in the reflectance mode at 675 nm. The method was found to give compact spots for the drug (Rf?=?0.40?±?0.03). The linear regression analysis data for the calibration plots showed good linear relationship with r2?=?.9989 in the concentration range 100–800 ng/spot. The method was validated for precision, recovery, repeatability, and robustness as per the International Conference on Harmonization guidelines. The minimum detectable amount was found to be 28.90 ng, whereas the limit of quantitation was found to be 97.04 ng. Statistical analysis of the data showed that the method is precise, accurate, reproducible, and selective for the analysis of tacrolimus. The method was successfully employed for the estimation of equilibrium solubility and quantification of tacrolimus as a bulk drug and in commercially available capsules and in-house developed self-microemulsifying formulations. 相似文献
4.
Sree Hari Krishnan Parthasarathi R. Padmanabhan Hema A. Murthy 《International Journal of Speech Technology》2011,14(4):361-368
This paper demonstrates the robustness of group delay based features to additive noise. First, we analytically show the robustness
of group delay based representations. The analysis makes use of the fact that, for minimum-phase signals, the group delay
function can be represented in terms of the cepstral coefficients of the log-magnitude spectrum. Such a representation results
in the speech spectrum dominating over the noise spectrum, both at low and high SNRs. Further, we experimentally demonstrate
the robustness of the representation on a voice activity detection (VAD) task, comparing a group delay based VAD algorithm
with standard VAD methods as well as a magnitude-spectrum based method. 相似文献
5.
The focus of this paper is to automatically segment and label continuous speech signal into syllable-like units for Indian
languages. In this approach, the continuous speech signal is first automatically segmented into syllable-like units using
group delay based algorithm. Similar syllable segments are then grouped together using an unsupervised and incremental training
(UIT) technique. Isolated style HMM models are generated for each of the clusters during training. During testing, the speech
signal is segmented into syllable-like units which are then tested against the HMMs obtained during training. This results
in a syllable recognition performance of 42·6% and 39·94% for Tamil and Telugu. A new feature extraction technique that uses
features extracted from multiple frame sizes and frame rates during both training and testing is explored for the syllable
recognition task. This results in a recognition performance of 48·7% and 45·36%, for Tamil and Telugu respectively. The performance
of segmentation followed by labelling is superior to that of a flat start syllable recogniser (27·8%and 28·8%for Tamil and
Telugu respectively). 相似文献
6.
Jerusha A. Hema Rajkumari Malaka Narayanan P. Muthukumarasamy Akilandeswari Sambandam Subakanmani Subramanian Murugan Sevanan 《IET nanobiotechnology / IET》2016,10(5):288
The biosynthesis of silver nanoparticles (AgNPs) has been proved to be a cost effective and environmental friendly approach toward chemical and physical methods. In the present study, biosynthesis of AgNPs was carried out using aqueous extract of Zea mays (Zm) husk. The initial colour change from golden yellow to orange was observed between 410 and 450 nm which confirmed the synthesis of AgNPs. Also, dynamic light scattering‐particle size analysis confirmed the average size to be 113 nm and zeta potential value of −28 kV. The morphology of synthesised Zm AgNPs displayed flower‐shaped structure, X‐ray diffraction pattern revealed the strongest peaks at 2θ = 38.6° and 64° which proved that the nanoparticle has the face centred crystalline structure. The Fourier transform infrared spectroscopy results showed strong absorption bands at 1394.53, 2980.02 and 2980.02 cm−1 due to the presence of alkynes, carboxylic acids, alcoholic and phenolic groups. The maximum zone of inhibition was observed against Salmonella typhi (22 mm) and Candida albicans (18 mm). The synthesised nanoparticles exhibited more free radical scavenging activity than the aqueous plant extract. This is the first report on the synthesis of AgNP from Zm husk, delivers the efficient and stable Zm AgNPs through simple feasible approach toward green biotechnology.Inspec keywords: silver, nanoparticles, nanofabrication, light scattering, particle size, X‐ray diffraction, crystal structure, Fourier transform infrared spectra, absorption coefficients, free radicalsOther keywords: green synthesis, silver nanoparticles, biosynthesis, environmental friendly approach, aqueous extract, Zea mays husk, colour change, golden yellow, dynamic light scattering‐particle size analysis, average size, zeta potential value, flower‐shaped structure, X‐ray diffraction pattern, face centred crystalline structure, Fourier transform infrared spectroscopy, absorption bands, alkynes, carboxylic acids, alcoholic groups, phenolic groups, Salmonella typhi, Candida albicans, free radical scavenging activity, aqueous plant extraction, green biotechnology, size 113 nm, wavelength 410 nm to 450 nm 相似文献
7.
Chinmay Mallik Shyam Lal Manish Naja Duli Chand S. Venkataramani Hema Joshi 《International journal of remote sensing》2013,34(8):2749-2762
The combustion of fossil fuels (coal and petroleum products) constitutes a source of continuous release of anthropogenic SO2 into the atmosphere. Furthermore, natural sources such as volcanoes can inject large amounts of SO2 directly into the troposphere and sometimes even into the stratosphere. These event-based volcanic eruptions provide solitary opportunities to study the transport and transformation of atmospheric constituents. In this study, we present an episode of high SO2 concentration over northern India as a result of long-range transport from Africa using multiple satellite observations. Monthly averaged column SO2 values over the Indo-Gangetic Plain (IGP) were observed in the range of 0.6–0.9 Dobson units (DU) during November 2008 using observations from the Ozone Monitoring Instrument (OMI). These concentrations were conspicuously higher than the background concentrations (<0.3 DU) observed during 2005–2010 over this region. The columnar SO2 loadings were highest on 6 November over most of the IGP region and even exceeded 6 DU, a factor of 10–20 higher than background levels in some places. These enhanced SO2 levels were not reciprocated in satellite-derived NO2 or CO columns, indicating transport from a non-anthropogenic SO2 source. As most of the local aerosols over the IGP region occur below 3 km, a well-separated layer at 4–5 km was observed from the Cloud-Aerosol Lidar and Infrared Pathfinder Satellite Observations (CALIPSO) satellite. Wind fields and back-trajectory analysis revealed a strong flow originating from the Dalaffilla volcanic eruption in Ethiopia during 4–6 November 2008. Although volcanic SO2 plumes have been extensively studied over many parts of Asia, Europe, and the USA, analysis of such events for the IGP region is being reported for the first time in this study. 相似文献
8.
Computed tomography images are widely used in the diagnosis of intracranial hematoma and hemorrhage. This paper presents a new approach for automated diagnosis based on classification of the normal and abnormal images of computed tomography. The computed tomography images used in the classification consists of non-enhanced computed tomography images. The proposed method consists of four stages namely pre-processing, feature extraction, feature reduction and classification. The discrete wavelet transform coefficients are the features extracted in this method. The essential coefficients are selected by the principal component analysis. The features derived are used to train the binary classifier, which infer automatically whether the image is that of a normal brain or a pathological brain, suffering from brain lesion. The proposed method has been evaluated on a dataset of 80 images. A classification with a success of 92, 97 and 98 % has been obtained by artificial neural network, k-nearest neighbor and support vector machine, respectively. This result shows that the proposed technique is robust and effective. 相似文献
9.
G. Hema Chandra C. Udayakumar N. Padhy S. Uthanna 《Materials Science in Semiconductor Processing》2010,13(4):288-294
CuIn0.75Al0.25Se2 thin films prepared onto glass substrates at TS=573 K were single phase, nearly stoichiometric and polycrystalline with a strong (1 1 1) preferred orientation showing sphalerite structure. The results of X-ray diffraction and electron diffraction studies are compared, interpreted and correlated with micro-Raman spectra. The optical absorption studies indicated a direct band gap of 1.16 eV with high absorption coefficient (>104 cm?1) near the fundamental absorption edge. 相似文献
10.
Hema Bhandari Vineet Bansal Veena Choudhary Sundeep K Dhawan 《Polymer International》2009,58(5):489-502
BACKGROUND: Poly(1‐amino‐2‐naphthol‐4‐sulfonic acid) and its copolymers with aniline are a new class of conducting polymers which can acquire intrinsic protonic doping ability, leading to the formation of highly soluble self‐doped homopolymers and copolymers. Free ? OH and ? NH2 groups in the polymer chain can combine with other functional groups that could be present in protective paints which can thus be successfully used as antistatic materials. RESULTS: This paper reports the formation of nanotubes of polyaniline on carrying out oxidative polymerization of aniline in the presence of 1‐amino‐2‐naphthol‐4‐sulfonic acid (ANSA) in p‐toluenesulfonic acid (PTSA) as an external dopant. The presence of ? SO3H groups in the ANSA comonomer allows the copolymer to acquire intrinsic protonic doping ability. The polymerization mechanism was investigated by analysing the 1H NMR, 13C NMR, Fourier transform infrared and X‐ray photoelectron spectra of the copolymers and homopolymers, which revealed the involvement of ? OH/? NH2 in the reaction mechanism. Scanning and transmission electron microscopy showed how the reaction route and the presence of a dopant can affect the morphology and size of the polymers. Static decay time measurements were also carried out on conducting copolymer films prepared by blending of 1 wt% of copolymers of ANSA and aniline with low‐density polyethylene (LDPE) which showed a static decay time of 0.1 to 0.31 s on dissipating a charge from 5000 to 500 V. CONCLUSION: Copolymers of ANSA with aniline were synthesized in different reaction media, leading to the formation of nanotubes and nanoparticles of copolymer. Blends of 1 wt% of PTSA‐ and self‐doped copolymers of ANSA and aniline with LDPE can be formulated into films with effective antistatic properties. Copyright © 2009 Society of Chemical Industry 相似文献