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排序方式: 共有92条查询结果,搜索用时 15 毫秒
1.
P.Y. Raval P.R. Pansara A.R. Makadiya N.H. Vasoya S.N. Dolia K.B. Modi 《Ceramics International》2018,44(15):17667-17674
The consequences of high energy mechanical milling, microwave-assisted heating and rapid thermal cooling on magnetic ordering in polycrystalline CaCu3Ti4O12 cubic perovskite have been investigated by means of X-ray powder diffractometry (300?K), dc magnetization in field – cooled and zero – field cooled modes (H = 100?Oe and 1000?Oe, T?=?5–300?K) (M – T curves) and M – H loop characteristics (T?=?5?K and 300?K, Hmax = 70?kOe). The M – T curves of unmilled and 16?h milled samples show pure antiferromagnetic and weak ferromagnetic ordering, respectively, 1?h and 6?h milled samples demonstrate the coexistence of both the phases while microwave-assisted and quenched samples exhibit classic antiferromagnetic transition and a low temperature paramagnetic–like contribution with different weights, well supported by the M – H loop characteristics. The observed transformations in the magnetic ordering are attributed to the ball-milling induced stress which curtails hybridization of empty Ti-3d orbitals with Cu-3d and O-2p orbitals and secondary phase formation. Oxygen vacancies associated with bound magnetic polarons originate ferromagnetism in the milled samples while unpaired electrons inhabited at the empty sites are the cause of paramagnetic centers. The low-temperature Curie – tail in M – T curve for quenched and microwave assisted samples is attributed to Ti3+ cations. 相似文献
2.
Methods for the production of mutants of the cellulase producer Clostridium cellulolyticum ATCC 35319 were examined using an agar plate screening technique. Spontaneous and UV light-induced mutants were isolated, some of which exhibited a high level of both endoglucanase and exoglucanase activities as assayed using CMC (carboxymethyl cellulose) and PNPCb (paranitrophenyi-β-cellobioside) respectively. The volumetric enzyme activities were up to 2.5 times those of the wild strain. 相似文献
3.
Graft copolymerization of methyl methacrylate (MMA) onto guar gum (GG) in aqueous slurry has been carried out using hydrogen peroxide (H2O2) as initiator. The copolymers were characterized by infrared spectroscopy. The grafting parameters like percent grafting, grafting efficiency, percent add-on, and the grafting frequency were determined, and the effect of reaction time, concentration of initiator, and [GG]/[MMA] ratios on the grafting parameters have been discussed. The decrease in % add-on at increasing concentration of H2O2 indicated enhancement in the rate of homopolymerization of methyl methacrylate. 相似文献
4.
Sodiummonochloroacetate and sodiumhydroxide were employed under different conditions to prepare and optimize the carboxymethyl derivative of Leucaena glauca seed gum. The effects of concentration of reactants, reaction temperature and time have been interpreted in terms of degree of carboxymethylation as well as efficiency and rate of carboxymethylation reaction. The formation of the proposed derivative has also been supported by providing infra-red spectral characterization. 相似文献
5.
Amit Kumar Gorai Simit Raval Ashok Kumar Patel Snehamoy Chatterjee Tarini Gautam 《国际煤炭科学技术学报(英文)》2021,8(4):737-755
Coal is heterogeneous in nature,and thus the characterization of coal is essential before its use for a specific purpose.Thus,the current study aims to develop ... 相似文献
6.
N,N-bis (2-hydroxyethyl) fatty amide (HAFA) derived from dehydrated castor oil (DCO) has been employed as a curing agent for
a carboxylic acid functional acrylic resin (AAR). Coating compositions with a varying AAR/HAFA ratio have been prepared and
their various film properties have been studied and compared with the conventional butylated melamine formaldehyde (MF) based
systems. The study reveals that HAFA can be used successfully as a crosslinking agent for AAR in baking systems. In addition
to other technical advantages, the use of HAFA is environmentally friendly as no toxic volatiles are evolved during curing
reaction, unlike in MF-cured systems.
Department of Industrial Chemistry, Vallabh Vidyanagar, Gujarat 388 120 India.
Hyderabad, India. 相似文献
7.
Heta Vuontisjärvi Marja Keinänen Pekka J. Vuorinen Kimmo Peltonen 《Polycyclic Aromatic Compounds》2013,33(4-5):333-342
Fish exposed to polycyclic aromatic hydrocarbons (PAHs) accumulate only a small amount of PAH in their tissues. Hydrophobic PAHs are readily transformed into hydrophilic metabolites and excreted in bile. Bile samples of five fish species were collected from the Baltic Sea and analyzed using two methods: high-performance liquid chromatography (HPLC) with fluorescence detection and a fixed wavelength fluorescence method. With the HPLC method PAH compounds were quantitated after hydrolysis, and with the fluorescence method without enzyme-assisted hydrolysis. In HPLC analysis the major metabolite in all fish species, 1-hydroxypyrene, was the only metabolite detected in perch and salmon samples. 1-Hydroxyphenanthrene was detected in a few flounder and in most eelpouts. The correlation between the two methods for pyrene-type metabolites was good (r2 = 0.773). 相似文献
8.
9.
Multimedia Tools and Applications - Nowadays, sports video analysis is gaining a lot of traction. Cricket is an exciting team sport to watch. Cricket is becoming more popular, but due to the... 相似文献
10.