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排序方式: 共有357条查询结果,搜索用时 15 毫秒
1.
Christoph Gottschalk Aiko Huckauf Arne Dübecke Florian Kaltner Matthias Zimmermann Ines Rahaus 《Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment》2018,35(7):1366-1383
The contamination of honey with hepatotoxic pyrrolizidine alkaloids (PAs) is a well-known hazard for food safety. While management strategies and controls of the honey industry aim to reduce the PA levels, uncertainties remain with regard to the safety of regionally produced and marketed honey. In addition, a previous study showed large differences of results obtained after various periods of storage and apparent differences between the analytical results of different laboratories. Therefore, this study aimed at examining these uncertainties by monitoring the impact of storage on the PA and PA N-oxide (PANO) content of two freshly harvested honeys and on possible demixing effects caused by pollen settling. Additionally, three analytical approaches – target analysis with matrix-matched calibration or standard addition and a sum parameter method – were applied for a comparative analysis of 20 honeys harvested in summer 2016. All samples originated from Schleswig-Holstein in Northern Germany where the PA plant Jacobaea vulgaris is currently observed on a massive scale. The results of the time series analyses showed that PANO levels markedly decreased within a few weeks and practically reached the LOD 16 weeks after harvest. Tertiary PAs, by contrast, remained stable and did not increase as a consequence of PANO decrease. The experiments on a putative demixing, which may result in a heterogeneous distribution of PAs/PANOs, revealed that there was no such effect during storage of up to 12 weeks. A comparison of the PA/PANO levels obtained by different analytical approaches showed that in some cases the sum parameter method yielded much higher levels than the target approaches, whereas in other cases, the target analysis with standard addition found higher levels than the other two methods. In summary, the results of this study highlight uncertainties regarding the validity and comparability of analytical results and consequently regarding health risk assessment. 相似文献
2.
Monique Jackson Ines Benkhemis Micka?l Begon Philippe Sardain Claude Vallée Patrick Lacouture 《Multibody System Dynamics》2012,28(3):225-237
Optimal synthesis of human movement or the prediction of the kinematics of a new movement require not only that the multi-body system be modeled but also that a performance criterion is specified. For sub-maximal movements the selection of a suitable performance criterion, able to generate realistic dynamic behavior is difficult. A two-dimensional simulation model of the take-off phase of a sub-maximal long jump was developed to study the effect of criterion choice on the realism of simulated movements. A parametric optimization technique was employed to obtain solutions to the constrained equations of motion. Seven different criteria were evaluated, by comparing simulated movements with an actual performance, to identify the criterion which most closely approximated that spontaneously minimized by the athlete. Synthesis of the take-off phase of a sub-maximal long jump was found to be sensitive to the chosen criterion, with a criterion based on minimizing joint intersegmental forces found to perform well. 相似文献
3.
The anionic polymerization of lauryllactam was initiated at 270°C using sodium hydride as an initiator and N,N′‐ethylene‐bisstearamide (EBS) as an activator (NaH:EBS molar ratio of 2). Polymerization occurred in less than 2 min and was successfully performed in an internal mixer and a twin‐screw extruder with corotating intermeshing screws (Werner & Pfleiderer ZSK 25). The content of residual monomer, as determined by thermogravimetric analysis, was lower than 0.5 wt %. Molecular weight, as measured by size exclusion chromatography, was governed by the lauryllactam:NaH molar ratio calculated on a Mn of 25 kg/mol at a constant NaH:EBS molar ratio of 2. Blends were prepared in situ by polymerization of lauryllactam solutions of various polymers. When poly(ethylene‐co‐butylacrylate) (Lotryl®; Atofina) was dissolved in lauryllactam, rubber‐toughened polyamide 12 blends were obtained. Mechanical properties of the injection‐molded polymers were examined by stress–strain as well as notched Charpy impact tests at different temperatures. Blend morphologies were imaged by scanning electron microscopy (SEM). © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 90: 344–351, 2003 相似文献
4.
Bourouis Sami Channoufi Ines Alroobaea Roobaea Rubaiee Saeed Andejany Murad Bouguila Nizar 《Multimedia Tools and Applications》2021,80(4):5809-5831
Multimedia Tools and Applications - This study presents an unsupervised novel algorithm for color image segmentation, object detection and tracking based on unsupervised learning step followed with... 相似文献
5.
Ines Hofinger Jörg Möller Manfred Bobeth Karen Raab 《Journal of Thermal Spray Technology》2002,11(3):387-392
The adherence of plasma sprayed NiCrAlY bond coats can be improved by an appropriate substrate surface finish. The interface
fracture energy for crack propagation along the coating/substrate interface has been measured for different surface roughness
by means of a specially designed four-point bending test. An increase of the interface fracture energy of about 15% was observed
for a three times higher surface roughness. In addition, four-point bending tests with the coating on the side face of bending
specimens were performed to analyze the fracture and spalling behavior of the coatings both under large tensile and compressive
substrate deformations. 相似文献
6.
Shuai Song Xiao-Na Song Nimisha Pathak Ines Tejado Balsera 《International Journal of Control, Automation and Systems》2017,15(4):1524-1535
In this work, we combine the active and adaptive control theories, and propose a novel synchronization scheme for a class of fractional-order chaotic systems with different structure and different order. Based on the new version of fractional-order Lyapunov stability theory, we design the adaptive controllers and updating laws of different switching. We use the fractional-order Lorenz chaotic system and the fractional-order Chen chaotic system as examples to analyze the multi-switching synchronization process for fractional-order chaotic systems with different structures and different orders. Finally, numerical simulations are also given to illustrate the effectiveness and validation of the proposed method, and the model uncertainties and external disturbances are added to the considered systems to verify the robustness of the proposed controllers. 相似文献
7.
Mirjana D. Timotijevi Tanja Ili Bojan Markovi Danijela Randjelovi Neboja Ceki Ines Nikoli Sneana Savi Ivana Panteli 《International journal of molecular sciences》2022,23(11)
Polymeric film-forming systems have emerged as an esthetically acceptable option for targeted, less frequent and controlled dermal drug delivery. However, their dynamic nature (rapid evaporation of solvents leading to the formation of thin films) presents a true characterization challenge. In this study, we tested a tiered characterization approach, leading to more efficient definition of the quality target product profiles of film-forming systems. After assessing a number of physico-chemico-mechanical properties, thermal, spectroscopic and microscopic techniques were introduced. Final confirmation of betamethasone dipropionate-loaded FFS biopharmaceutical properties was sought via an in vitro skin permeation study. A number of applied characterization methods showed complementarity. The sample based on a combination of hydrophobic Eudragit® RS PO and hydroxypropyl cellulose showed higher viscosity (47.17 ± 3.06 mPa·s) and film thickness, resulting in sustained skin permeation (permeation rate of 0.348 ± 0.157 ng/cm2 h), and even the pH of the sample with Eudragit® NE 30D, along with higher surface roughness and thermal analysis, implied its immediate delivery through the epidermal membrane. Therefore, this study revealed the utility of several methods able to refine the number of needed tests within the final product profile. 相似文献
8.
Ines J. P. Colle Lien Lemmens Griet Knockaert Ann Van Loey 《Critical reviews in food science and nutrition》2016,56(11):1844-1855
Kinetic models are important tools for process design and optimization to balance desired and undesired reactions taking place in complex food systems during food processing and preservation. This review covers the state of the art on kinetic models available to describe heat-induced conversion of carotenoids, in particular lycopene and β-carotene. First, relevant properties of these carotenoids are discussed. Second, some general aspects of kinetic modeling are introduced, including both empirical single-response modeling and mechanism-based multi-response modeling. The merits of multi-response modeling to simultaneously describe carotene degradation and isomerization are demonstrated. The future challenge in this research field lies in the extension of the current multi-response models to better approach the real reaction pathway and in the integration of kinetic models with mass transfer models in case of reaction in multi-phase food systems. 相似文献
9.
Marte A. Ramírez-Ortegón Lilia L. Ramírez-Ramírez Volker Märgner Ines Ben Messaoud Erik Cuevas Raúl Rojas 《Pattern recognition》2014
In this paper, we will present a mathematical analysis of the transition proportion for the normal threshold (NorT) based on the transition method. The transition proportion is a parameter of NorT which plays an important role in the theoretical development of NorT. We will study the mathematical forms of the quadratic equation from which NorT is computed. Through this analysis, we will describe how the transition proportion affects NorT. Then, we will prove that NorT is robust to inaccurate estimations of the transition proportion. Furthermore, our analysis extends to thresholding methods that rely on Bayes rule, and it also gives the mathematical bases for potential applications of the transition proportion as a feature to estimate stroke width and detect regions of interest. In the majority of our experiments, we used a database composed of small images that were extracted from DIBCO 2009 and H-DIBCO 2010 benchmarks. However, we also report evaluations using the original (H-)DIBCO?s benchmarks. 相似文献
10.
Yousra Turki Hada Ouzari Ines Mehri Aouatef Ben Ammar Abdennaceur Hassen 《Food research international (Ottawa, Ont.)》2012,45(2):1099-1105
Salmonella serovars are increasing in importance as significant pathogens of both human and animals. Although water and wastewater are treated to eliminate pathogenic microorganisms, they still play an important role in the transmission of Salmonella spp. In this study, bacteriophages infecting Salmonella spp. were isolated from wastewater and evaluated; for their potential to lyse environmental Salmonella strains in vitro at different MOIs and temperatures; and to control the wastewater bacterial community. Three distinct phages designated sww65, sww275, and sww297; as defined by plaque morphology, electron microscopy and host range; were obtained from wastewater. Challenge tests were performed at 37, and 30 °C with the infection of the Salmonella cultures with individual phage, a mixture of two phages, and cocktail of three phages at MOIs of 100, 102, and 104 PFU/CFU. At 30, and 37 °C, a cocktail of three phages reduced all of the Salmonella cultures tested. These results required a high multiplicity of infection. However, when infected with only one phage or a mixture of two phages at MOIs of 100 or 10 2 PFU/CFU, an emergence of bacterial resistance was observed. The dynamic monitoring of wastewater enterobacterial community was conducted using Enterobacterial Repetitive Intergenic Consensus-PCR (ERIC-PCR). The number of bands decreased gradually with the use of individual phage or phage cocktails. Moreover, the dynamic monitoring of Salmonella community during wastewater treatment was performed using PCR detection of virulence gene invA. The results correlated with the ERIC-PCR fingerprints, and suggested that Salmonella community was affected by the phage treatment. Indeed, in wastewater, bacteriophages are reducing Salmonella and other members of the Enterobacteriaceae. These results indicated that dynamic changes are closely related with the process of treatment. The introduction of wide host range bacteriophages in wastewater can have a potential impact on the dynamics of the microbial communities, manifested by the reduction or the elimination of microbial species. 相似文献