高分子铁盐絮凝剂制备及其应用研究

研究了以废铁屑和工业硫酸亚铁为原料,在常压和加热条件下,用氯酸钾作为氧化剂制取聚合硫酸铁(PFS)的工艺条件,并在PFS制备的基础上,合成了聚磷硫酸铁(PPFS)和聚氯硫酸铁(PFCS)。将所制备的聚铁用于污水处理实验,结果表明:用该方法制备的聚铁絮凝剂对实际水样具有较好的混凝处理效果,且制备工艺简单、速度快,从根本上消除了用NaNO_2催化氧化法制备聚铁对环境造成的二次污染。     

回归正交设计在PEK-C增韧酚醛树脂研究中的应用

采用计算机辅助回归正交设计的方法对酚酞型聚醚酮(PEK-C)增韧酚醛树脂进行研究，通过回归正交设计，对共混体系的组分配比和成型工艺参数进行优化，预测出最佳配比和工艺参数，并通过试验得到验证。     

纳米晶体Ni－P合金晶粒微观结构的研究

采用非晶晶化法制备出晶粒尺寸不同的Ｎｉ－Ｐ合金复相纳米晶体样品。利用Ｘ射线衍射技术分别对样品中Ｎｉ固溶体和Ｎｉ_３Ｐ的晶格参数随晶粒尺寸的变化进行了测试，发现在Ｎｉ固溶体纳米相中Ｐ的固溶浓度增大，约为平衡固溶度的１０－１５倍，形成超过饱和固溶晶格结构；在Ｎｉ_３Ｐ化合物纳米相中空位浓度增加导致晶格畸变发生，而且随晶粒尺寸减小晶格畸变程度增大。     

Interaction of {112¯2} twin variants in hexagonal close-packed titanium

As multiple {11$\overline{2}$ 2} twin variants are often formed during deformation in hexagonal close-packed (hcp) titanium, the twin-twin interaction structure has a profound influence on mechanical properties. In this paper, the twin-twin interaction structures of the {11$\overline{2}$2} contraction twin in cold-rolled commercial purity titanium were studied by using electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM). Formation of the {11$\overline{2}$2} twin variants was found to deviate the rank of Schmid factor, and the non-Schmid behavior was explained by the high-angle grain boundary nucleation mechanism. All the observed twin-twin pairs manifested a quilted-looking structure, which consists of the incoming twins being arrested by the obstacle twins. Furthermore, the quilted-looking {11$\overline{2}$2} twin-twin boundary was revealed by TEM and high resolution TEM observations. De-twinning, lattice rotation and curved twin boundary were observed in the obstacle twin due to the twin-twin reaction with the impinging twin. A twin-twin interaction mechanism for the {11$\overline{2}$2} twin variants was proposed in terms of the dislocation dissociation, which will enrich the understanding for the propagation of twins and twinning-induced hardening in hcp metals and alloys.     

海藻乳酸菌发酵的研究进展

海藻是一类重要的海洋资源,富含大量营养元素如蛋白质、碳水化合物、维生素和矿物质,以及多糖、酚类等生物活性物质。由于海藻营养价值极高,利用乳酸菌发酵海藻促进生物活性化合物的产生和释放,具有良好的健康效益。因此,本文根据国内外近年来利用乳酸菌发酵海藻的相关研究报道,对乳酸菌发酵类型、乳酸菌发酵海藻的可行性和乳酸菌主要种类、以及乳酸菌在海藻发酵中的效果和作用进行阐述,同时综述了乳酸菌发酵海藻在食品行业中的开发应用现状,并对今后发展趋势和前景进行展望,为藻类乳酸菌发酵制品的开发提供一定参考。     

3种测试溶液对搪瓷用钢抗鳞爆性能评价指标的影响

采用3种常见的测试溶液检测了10组搪瓷用钢板的氢渗透性能,并同时采用涂搪实验进行验证。结果显示,测试溶液A适用于试验选定的各种厚度的搪瓷用钢,其检测结果准确率可达100%;而溶液B和溶液C在测试厚度1.5 mm以上的搪瓷用钢板料出现部分误判现象。溶液B若基于有效氢扩散系数D_eff,其准确率为70%,若基于TH值,其准确率仅为50%;而溶液C误判率达30%。     

散热型印制电路板环氧胶粘剂的研究

散热型金属复合印制电路板 (HDPCB)是使电子设备更加轻型化、小型化、简单化 ,同时能提高其可靠性的措施之一。用改性环氧胶粘剂制得的HDPCB能满足航空机载电子设备的使用要求 ,实现了HDPCB的国产化。