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排序方式: 共有219条查询结果,搜索用时 31 毫秒
1.
Mohammad Afshari Amir-Reza Rouhani Isfahani Saeed Hasani Fatemeh Davar Khadijeh Jahanbani Ardakani 《International Journal of Applied Ceramic Technology》2019,16(4):1612-1621
In the present study, spinel structure CoFe2O4 nanoparticles were successfully synthesized by the sol-gel auto-combustion technique. The effect of apple cider vinegar (ACV) addition as an organic biocompatible agent on the size, morphology, and magnetic properties of CoFe2O4 nanoparticles was investigated in detail. The phase evolution, particle size, and lattice parameter changes of the synthesized phase have been estimated by using Rietveld structure refinement analysis of X-ray powder diffraction data. Also, Fourier transform infrared spectra (FT-IR) of the samples verified the presence of two expected bands correspond to tetrahedral and octahedral metal-oxygen complexes within the spinel structure. Furthermore, microstructural observations revealed that ultrafine particles have a semi-spherical morphology. It was shown that the particles size decreased from ~45 to ~17 nm with an increase in the amount of ACV. Magnetic properties were carried out by vibrating sample magnetometer (VSM) at room temperature. Both the saturation magnetization (Ms) and coercivity (Hc) were found to be significantly dependent on the crystallite size and the amount of ACV. 相似文献
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Nonnegative matrix factorization (NMF) algorithms have been utilized in a wide range of real applications; however, the performance of NMF is highly dependent on three factors including: (1) choosing a problem dependent cost function; (2) using an effective initialization method to start the updating procedure from a near‐optimal point; and (3) determining the rank of factorized matrices prior to decomposition. Due to the nonconvex nature of the NMF cost function, finding an analytical‐based optimal solution is impossible. This paper is aimed at proposing an efficient initialization method to modify the NMF performance. To widely explore the search space for initializing the factorized matrices in NMF, the island genetic algorithm (IGA) is employed as a diverse multiagent search scheme. To adapt IGA for NMF initialization, we present a specific mutation operator. To assess how the proposed IGA initialization method efficiently enhances NMF performance, we have implemented state‐of‐the‐art initialization methods and applied to the Japanese Female Facial Expression dataset to recognize the facial expression states. Experimental results demonstrate the superiority of the proposed approach to the compared methods in terms of relative error and fast convergence. 相似文献
4.
Abdol-Samad Abedi Fatemeh Hemmati Amir Hossein Abedini Abdorreza Mohammadi Masoumeh Moslemi 《Journal of the American Oil Chemists' Society》2021,98(10):969-978
A simple, fast, and reliable liquid–liquid micro-extraction (LLME) method assisted by thermal ultrasound approach was developed for simultaneous determination of synthetic phenolic antioxidants (SPAs) in edible oils by high-performance liquid chromatography equipped with ultraviolet detector (HPLC-UV). The synthetic antioxidants were propyl gallate (PG), butylated hydroxyanisole (BHA), tert-butylhydroquinone (TBHQ), and butylated hydroxyltoluene (BHT). The best extraction conditions were observed were methanol/acetonitrile (1:1, v/v) as the solvent, ultrasound at 4 min, and a temperature of 40°C. The linearity of the calibration curves for the optimum conditions were R2 > 0.989 for all of the SPAs in a range from 1–200 μg ml−1. Relative standard deviation (RSD %) for five analysis was in range of 2.83% to 4.21%. Limit of detection (LOD) and limit of quantification (LOQ) were obtained in range of 0.012–0.06 and 0.04–0.2 μg g−1, respectively. With regard to recovery, a range of 91%–116% was calculated for the spiked edible oils. 相似文献
5.
Seyed Mohammad Reza Derakhshandeh Seyed Mohammad Mehdi Hadavi Mohammad Javad Eshraghi Masoumeh Javaheri Masoud Mozafari 《IET nanobiotechnology / IET》2017,11(6):656
In this study, hydrogenated amorphous carbon thin films, structurally similar to diamond‐like carbon (DLC), were deposited on the surface of untreated and plasma nitrocarburised (Nitrocarburizing‐treated) stainless steel medical implants using a plasma‐enhanced chemical vapour deposition method. The deposited DLC thin films on the nitrocarburising‐treated implants (CN+DLC) exhibited an appropriate adhesion to the substrates. The results clearly indicated that the applied DLC thin films showed excellent pitting and corrosion resistance with no considerable damage on the surface in comparison with the other samples. The CN+DLC thin films could be considered as an efficient approach for improving the biocompatibility and chemical inertness of metallic implants.Inspec keywords: tissue engineering, bone, biomedical materials, electrochemistry, amorphous state, carbon, hydrogen, thin films, plasma CVD, adhesion, corrosion resistance, surface hardeningOther keywords: electrochemical performance, plasma nitrocarburised stainless steel medical implants, hydrogenated amorphous carbon thin films, bone tissue engineering, plasma‐enhanced chemical vapour deposition method, adhesion, corrosion resistance, biocompatibility, chemical inertness, metallic implants, C:H 相似文献
6.
Microfluidic Manipulation of Core/Shell Nanoparticles for Oral Delivery of Chemotherapeutics: A New Treatment Approach for Colorectal Cancer 下载免费PDF全文
Mohammad Mahdi Hasani‐Sadrabadi Shahrouz Taranejoo Erfan Dashtimoghadam Ghasem Bahlakeh Fatemeh Sadat Majedi Jules John VanDersarl Mohsen Janmaleki Fatemeh Sharifi Arnaud Bertsch Kerry Hourigan Lobat Tayebi Philippe Renaud Karl I. Jacob 《Advanced materials (Deerfield Beach, Fla.)》2016,28(21):4134-4141
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The characterization of an optical sensor membrane is described for simultaneous determination of sulfite and sulfide ions based on the immobilization of crystal violet on a triacetylcellulose membrane. The absorbance of the membranes decreased by increasing sulfite and sulfide concentration. The partial least squares (PLS-1) calibration model based on spectrophotometric measurement for simultaneous determination of sulfite and sulfide ions was applied. This method is based on the difference between the rate of the reaction of sulfide and sulfite with membranes in pH 7.0 buffer solution and at 25 °C. The experimental calibration matrix for partial least squares (PLS-1) calibration was designed with 18 samples. The cross-validation method was used for selecting the number of factors. The results showed that simultaneous determination could be performed in the range of 200–2000 μg mL−1 (2.5–25 mmol L−1) and 80–900 μg mL−1 (2.5–28.125 mmol L−1) for sulfite and sulfide, respectively. The sensor can readily be regenerated with water and the color is fully reversible. The sensor was successfully applied to the simultaneous determination of sulfide and sulfite in water samples. 相似文献
8.
Alireza Shamsi Amir Shamloo Negar Mohammadaliha Hassan Hajghassem Jalil Fallah Mehrabadi Masoumeh Bazzaz 《Microsystem Technologies》2016,22(10):2447-2454
Since plasma is rich in many biomarkers used in clinical diagnostic experiments, microscale blood plasma separation is a primitive step in most of microfluidic analytical chips. In this paper, a passive microfluidic device for on-chip blood plasma separation based on Zweifach–Fung effect and plasma skimming was designed and fabricated by hot embossing of microchannels on a PMMA substrate and thermal bonding process. Human blood was diluted in various times and injected into the device. The main novelty of the proposed microfluidic device is the design of diffuser-shaped daughter channels. Our results demonstrated that this design exerted a considerable positive influence on the separation efficiency of the passive separator device, and the separation efficiency of 66.6 % was achieved. The optimum purity efficiency of 70 % was achieved for 1:100 dilution times. 相似文献
9.
Robust Stability and Stabilization Of TCP‐Networked Control Systems with Multiple Delay System Modeling 下载免费PDF全文
This paper presents a new model for networked control systems (NCSs) under transmission control protocol (TCP) as a multiple‐delay system by considering both sensor to controller and controller to actuator delays. An analytical TCP model has been considered for the network part, and an active queue management (AQM) controller is designed to regulate the desired queue length, which ensures holding the network induced delay and its variation within their lower bounds. The model is assumed to possess structured uncertainties due to the stochastic nature of the network. Robust stability and stabilization conditions are derived in terms of linear matrix inequalities (LMIs) by applying the Lyapunov‐Krasovskii stability criterion. Illustrative examples are presented and it has been shown that the proposed method will obtain less conservative results compared to the existing approaches in the literature. 相似文献
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