排序方式: 共有39条查询结果,搜索用时 15 毫秒
1.
M T Zaranski G W Patton L L McConnell T F Bidleman J D Mulik 《Analytical chemistry》1991,63(13):1228-1232
Glass cartridges containing 6-10 g of Tenax-GC or 15 g of XAD-2 resin packed between two slices of polyurethane foam (PUF) were used in a General Metal Works PS-1 high-volume sampler to collect chlorobenzenes (CBs) containing three to six chlorine atoms, hexachlorocyclohexanes (HCHs), and two-ring aromatic hydrocarbons from 35-385 m3 of air. Laboratory experiments were run by vaporizing known quantities of analytes into a clean airstream for sampling by the PS-1 system at 20 degrees C. Collection efficiencies, determined from mass balance of the quantities introduced and recovered, ranged from 70 to 120% for individual compounds and averaged 93% overall. Penetration of analytes to backup adsorbent traps showed an inverse correlation to vapor pressure. The method was used to collect the above compounds from urban and rural air. 相似文献
2.
P.Richard Mulik 《Fuel》1984,63(12):1731-1737
The testing of 18 alternative fuels was the basis for an extensive data bank of combustion parameters and fuel properties. This Paper represents an effort to correlate the three key dependent variables (NOx, smoke, and wall temperature) to the process conditions and fuel properties. Correlation was facilitated by the use of a multiple linear regression computer program. Linear terms, second-order terms, and their interactions were investigated. Correlation development is discussed and the results presented. Determining the physical meaning of the correlations is attempted together with a discussion concerning extrapolation of the correlations over the range of current operational gas turbine combustors. The correlations can be described as excellent for NOx and good-to-fair for smoke and wall temperature. 相似文献
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Kore Ekanath K. Shahane Guruling S. Mulik Ramesh N. 《Journal of Materials Science: Materials in Electronics》2022,33(13):9815-9829
Journal of Materials Science: Materials in Electronics - The Co1?xZnxFe2O4 (Co–Zn) ferrite nanoparticles with x varying from 0.0 to 0.4 have been manufactured by facile chemical... 相似文献
5.
The wear and friction properties of poly (ether‐ether‐ketone) (PEEK) reinforced with 0–33 vol % (60 wt %) micron size Al2O3 composites were evaluated at a sliding speed of 1.0 m/s and nominal pressure from 0.5 to 1.25 MPa under dry sliding conditions using a pin‐on‐disk wear tester. The wear resistance of the pure PEEK is 10‐fold higher than that of mild steel under the similar test condition. It is improved to 18‐fold as compared with mild steel at 3.5 vol % Al2O3 content. The improvement in wear properties may be attributed to the thin, tenacious, and coherent transfer film formed between the steel countersurface and composite pin. However, the wear resistance of PEEK containing above 3.5 vol % Al2O3 was deteriorated, despite their higher hardness and stiffness as compared with that of composites containing lower Al2O3 content. This is attributed to the formation of thick and noncoherent transfer film, which does not prevent the wear of the composites from hard asperities of countersurface. Moreover, hard Al2O3 particles present in transfer film act as third body wear mechanism. The coefficient of friction of the composites is higher than that of pure PEEK. SEM and optical microscopy have shown that wear of pure PEEK occurs by the mechanism of adhesion mainly whereas of PEEK composites by microploughing and abrasion. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
6.
Parag V. Adhyapak Uttam P. Mulik Dinesh P. Amalnerkar Imtiaz S. Mulla 《Journal of the American Ceramic Society》2013,96(3):731-735
In this study, we report template and surfactant‐free, low temperature (70°C) synthesis of needle‐like α‐FeOOH and its conversion at 400°C into α‐Fe2O3 nanorods using Fe(+2) and Fe(+3) chlorides and urea as a hydrolysis‐controlling agent. The isolated needle‐like α‐FeOOH indicates asparagus‐type growth pattern having length ca. 600 nm with 80 nm diameter at base and apex diameter of around 10 nm. The sample on heating (α‐Fe2O3) shows nanorod‐like morphology. The samples were characterized using various physicochemical characterization techniques such as XRD, Raman spectroscopy, UV‐Vis spectroscopy, particle size distribution analysis, Field Emission Scanning Electron Microscopy (FE‐SEM), and humidity sensing performance. The humidity sensing behavior of both α‐FeOOH and α‐Fe2O3 was studied. The α‐FeOOH shows quicker (10 s) and higher response toward change in humidity from 20%RH to 90%RH as compared with α‐Fe2O3 (60 s). Their typical morphology and crystalline structure plays an important role in humidity sensing behavior. 相似文献
7.
Milind V. Kulkarni Annamraju Kasi Viswanath R. Marimuthu U. P. Mulik 《Journal of Materials Science: Materials in Electronics》2004,15(12):781-785
Conducting polymer, Poly(o-toluidine) was synthesized by chemical oxidative polymerization method using different inorganic acids such as HCl, H2SO4, HClO4, HNO3, H3PO4 and H3BO3 as protonic acid media. Synthesized polymers were characterized by UV-Visible and FT-IR spectroscopy. Conducting emeraldine salt phase of the polymer has been confirmed with the help of spectroscopic analysis. Thermal stability of these polymers were investigated by thermogravimetric (TG/SDTA) analysis. Increase in conductivity with increase in temperature was observed in all the samples. 相似文献
8.
The dynamic mechanical properties of high‐performance polymer matrix composites based on semicrystalline poly(ether ether ketone) (PEEK) and aluminum oxide (Al2O3) were evaluated in the temperature range of 30–250°C with a three‐point‐bending mode at a frequency of 1 Hz. The storage modulus and loss modulus changed significantly with the variation of the Al2O3 content in the PEEK matrix. The Al2O3 reinforcement was more pronounced above the glass‐transition temperature (Tg). A composite containing 60 wt % (33 vol %) Al2O3 exhibited about a 78% increase in the storage modulus at 50°C and about a 200% increase at 200°C. However, there was no significant change in the mechanical loss factor and Tg associated with the peak of the mechanical loss factor or loss modulus with the addition of Al2O3. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 568–575, 2007 相似文献
9.
Parag Adhyapak Poonam Mahapure Rohini Aiyer Suresh Gosavi Uttamrao Mulik Dinesh Amalnerkar 《应用聚合物科学杂志》2012,123(6):3565-3574
Cobalt (Co) nanoparticles (with different loadings, 1 and 2 wt %, of Co) were synthesized in situ in a poly(vinyl alcohol) (PVA) matrix with and without meta‐nitroaniline (m‐NA) as a dopant (2.5 wt %). The obtained nanocomposite films were characterized with various physicochemical techniques, including ultraviolet–visible spectrophotometry, X‐ray diffraction analysis, scanning electron microscopy, and Fourier transform infrared analysis. To study the effect of the humidity, the nanocomposite solutions were coated on planar glass substrates. The beam of an He–Ne laser was incident normal to the film surface and was subjected to variable relative humidities (RHs; 4–93%); the transmitted intensity was measured on a photovoltaic diode. Variations in the intensity of light caused by the changes in RH within the range 3–93% were recorded. We optimized the response by varying the film thickness by coating the solution layer by layer. We generated the RH (4–100%) by passing wet water vapors. The neat PVA film of similar thickness gave humidity sensing in the range 78–93% RH. The sensors with m‐NA‐doped Co/PVA gave better sensitivity (6.4 mV/% RH) than the undoped samples (1.78–2.45 mV/% RH), exhibiting a fast response of 3 s (2–93% RH) and a recovery of 10 s (93 to 2% RH). These samples also showed reversible behavior and long‐term stability (for nearly a year) with a good sensitivity and a large dynamic range (2–95% RH). An attempt was made to explain the results on the basis of a bulk mechanism. © 2011 Wiley Periodicals, Inc. J Appl Polym Sci, 2012 相似文献
10.
We herewith report the thermal, mechanical (modulus), and dielectric properties of polystyrene (PS)/expanded graphite (EG) nanocomposites fabricated by a simple technique of dispersing EG (up to 2.5 vol %) in PS matrix via solution method followed by hot pressing. The thermal stability and char yield of the nanocomposites are improved marginally. The modulus, electrical conductivity, dielectric constant, and dielectric loss tangent of the nanocomposites are significantly increased with EG content. The modulus of the nanocomposites increases by about twofold at 30°C compared with that of pure PS. The dielectric constant and the loss tangent of nanocomposites are increased up to 13‐fold and 200‐fold compared with that of pure PS, respectively, at 1 MHz and varied with frequency. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2009 相似文献