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1.
The tetragonal → monoclinic ( t → m ) martensitic phase transformation in ZrO2 –0.5–4 mol% Y2 O3 proceeds during isothermal aging at various temperatures from 350 to 800 K; i.e., the transformation increases sigmoidally with aging time. The time-temperature-transformation ( T - T - T ) curves show a typical C shape, with very high rate for lower Y2 O3 -content specimens, and the rate decreases with higher Y2 O3 content. The transformation temperature ( M s ) of the t → m transformation obtained from dilatation curves during the cooling stage coincides well with C curves above the nose temperature. The t → m transformation should occur isothermally, as suggested by a nucleation and growth mode. 相似文献
2.
Artificial Life and Robotics - The aging population and expectations for nursing care robots increased significantly recently. We focused on mobile assistive robots. When various types of robots... 相似文献
3.
A data-driven design method for a cascade control system is proposed. The cascade control system consists of inner and outer loops, where the control interval of the outer loop is an integer multiple of the inner loop; hence, the system is a dual-rate system. In the proposed method, controllers in the inner and outer loops are designed based on one-shot data. In such a dual-rate cascade system, since the controllers are designed using different data-rate signals, the lifting technique is applied to align the dual-rate data. To show its effectiveness, the proposed method is compared with a conventional single-rate cascade control method, and numerical simulations and experiments are presented to examine servo and regulation performance. 相似文献
4.
Functionally graded nano‐TiO2 epoxy matrix composites were successfully fabricated using a centrifugal method. In the preparation of the composite, the aggregation of nano‐TiO2 occurred during curing, which had a negative effect on the composite performance. To solve this problem, we introduced a silane coupling agent to modify the surface of the nano‐TiO2, thereby improving the performance and mechanical properties simultaneously. The modified nano‐TiO2 (s‐TiO2) had better dispersion in the epoxy resin, making it possible to produce depth gradients of the mechanical properties of functionally graded materials (FGMs). The s‐TiO2 was characterized with respect to functional groups, morphology, and chemical elements using transmission electron microscopy, X‐ray photoelectron spectroscopy, and Fourier‐transform infrared spectroscopy. The results show that a silane layer was successfully coated on the surface. Also, the gradients of the mechanical and permittivity properties of the FGM indicated that by modifying the surface of the nano‐filler, it is possible to fabricate nano‐filler‐reinforced epoxy matrix FGMs using a centrifugal method. POLYM. COMPOS., 35:557–563, 2014. © 2013 Society of Plastics Engineers 相似文献
5.
Shigenori KashimuraHajime Yamashita Yoshihiro MuraiYoshiya Kera Natsuki YamashitaHiroaki Murase Manabu Ishifune 《Electrochimica acta》2002,48(1):7-10
Electroreduction of aliphatic esters in THF was found to be promoted by the catalytic amount of porphine-magnesium(II) complexes and afforded 2-alkoxytetrahydrofuran derivatives, the coupling products between alkoxide anions formed by the electroreduction of aliphatic esters and THF cation generated by the anodic oxidation of the solvent (THF). In this reaction, chlorophyll a extracted from Trifolium repens L was remarkably effective. In addition, lanthanide metal(III) ions such as samarium trichloride were also found to be effective for the electroreduction of aliphatic esters. 相似文献
6.
Yanagitani T Mishima N Matsukawa M Watanabe Y 《IEEE transactions on ultrasonics, ferroelectrics, and frequency control》2007,54(4):701-704
The (1120) textured polycrystalline ZnO films with a high shear mode electromechanical coupling coefficient k15 are obtained by sputter deposition. An over-moded resonator, a layered structure of metal electrode film/(1120) textured ZnO piezoelectric film/metal electrode film/silica glass substrate was used to characterize k15 by a resonant spectrum method. The (1120) textured ZnO piezoelectric films with excellent crystallite c-axis alignment showed an electromechanical coupling coefficient k15 of 0.24. This value was 92% of k15 value in single-crystal (k15 = 0.26). 相似文献
7.
Kazuyoshi Torii Kenichi Shoji Hiroshi Kawakami Takao Kumihashi Toshihiko Itoga Natsuki Yokoyama Masahiro Moniwa Tooru Kaga Yoshihisa Fujisaki 《Electrical Engineering in Japan》1997,121(1):43-50
A one-mask-patterned ferroelectric capacitor test structure designed with a 0.5-μm feature size was fabricated. Oxygen plasma treatment after dry etching decreased the leakage current to as low as that of as-deposited film. These one-mask-patterned ferroelectric capacitors, with switching charge almost equal to as-deposited film, were successfully fabricated. Ferroelectric memories as dense as dynamic random access memories will become possible with this technology. However, the leakage current density for micron-sized capacitors is 2 to 10 times that of large capacitors. The leakage current in small capacitors is increased due to perimeter leakage that runs through the damaged region on the capacitor sidewall. © Scripta Technica, Inc. Electr Eng Jpn, 121(1): 43–50, 1997 相似文献
8.
In this report, we introduce a new entry of high-performance polymer-based monolithic capillary column for mainly small molecules. This capillary column was prepared using a newly introduced epoxy monomer with diamines. Simply heat-induced polycondensation in an appropriate porogenic solvent afforded a really homogeneous co-continuous monolithic structure having submicrometer-size skeletons with micrometer-size through-pores. We were also able to prepare chiral monolithic columns using a chiral epoxy monomer as well as a chiral diamine. A 21.5-cm-long, 100-mum-i.d. column afforded up to 40 000 theoretical plate numbers (N) for alkylbenzenes in 60% aqueous acetonitrile as a reversed-phase-mode stationary phase. Due to a quite low column pressure drop, a 150-cm-long column was prepared. This long column afforded up to 200 000 plates for alkylbenzenes with only a 4-MPa column pressure drop. In contrast, in 100% acetonitrile, this column has "HILIC" property to show up to 60 000 plates for methanol with a 17.5-cm-long column. In this mode, we were able to separate nucleic acids. In addition, we have prepared a chiral column with both of the chiral epoxy monomers and an amine. This column was able to chirally discriminate a racemic alcohol in a reversed-phase mode. 相似文献
9.
Li Zhang Qing‐Qing Ni Akihiko Shiga Yaqin Fu Toshiaki Natsuki 《Polymer Composites》2010,31(3):491-496
Polybenzimidazole (PBI) nanocomposites containing 0.5–5 wt% vapor grown carbon nanofibers (VGNFs) were successfully synthesized by solvent evaporation method. Fracture morphology examination confirmed the uniform dispersion of VGNFs in the matrix. The mechanical properties of neat PBI and the nanocomposites were systematically measured by tensile test, dynamic mechanical analysis (DMA), hardness measurement, and friction test. Tensile tests revealed that Young's modulus increased by about 43.7% at 2 wt% VGNFs loading, and further modulus growth was observed at higher filler loadings. DMA studies showed that the nanocomposites have higher storage modulus than neat PBI in the temperature range of 30–350°C, holding storage modulus larger than 1.54 GPa below 300°C. Outstanding improvement of hardness was achieved for PBI upon incorporating 2 wt% of VGNFs. The results of friction test showed that coefficient of friction of PBI nanocomposites decreased with VGNFs content compared with neat PBI. POLYM. COMPOS., 2010. © 2009 Society of Plastics Engineers 相似文献
10.
Natural rubber (NR) composites with different contents of 1, 3, 10, and 20 wt% vapor‐grown carbon nanofibers (VGCFs) were synthesized using a solvent casting method. The initial modulus of composites was improved by 26.5 %/wt% as the VGCFs were added, and the NR/3 wt%VGCF composite had the largest tensile strength. The experiment values of initial moduli agreed well with the values predicted by the Halpin‐Tsai theory. The reinforcement mechanisms of the composites were investigated by scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectroscopy and wide‐angle X‐ray diffraction (WAXD). It was found that an efficient stress transfer occurred from NR to VGCFs under the uniaxial stretching. The addition of 10 wt% VGCFs could promote the nucleation process of NR, which resulted in the characteristic of the strain‐induced crystallization (SIC) in NR/10 wt%VGCF composite even for low strain. POLYM. COMPOS., 2010. © 2009 Society of Plastics Engineers 相似文献