In this article, modification of carbon fiber surface by carbon based nanofillers (multi-walled carbon nanotubes [CNT], carbon nanofibers, and multi-layered graphene) has been achieved by electrophoretic deposition technique to improve its interfacial bonding with epoxy matrix, with a target to improve the mechanical performance of carbon fiber reinforced polymer composites. Flexural and short beam shear properties of the composites were studied at extreme temperature conditions; in-situ cryo, room and elevated temperature (−196, 30, and 120°C respectively). Laminate reinforced with CNT grafted carbon fibers exhibited highest delamination resistance with maximum improvement in flexural strength as well as in inter-laminar shear strength (ILSS) among all the carbon fiber reinforced epoxy (CE) composites at all in-situ temperatures. CNT modified CE composite showed increment of 9% in flexural strength and 17.43% in ILSS when compared to that of unmodified CE composite at room temperature (30°C). Thermomechanical properties were investigated using dynamic mechanical analysis. Fractography was also carried out to study different modes of failure of the composites. 相似文献
Carbon fiber reinforced epoxy (CE) composite is ideal for a cryogenic fuel storage tank in space applications due to its unmatched specific strength and modulus. In this article, inter-laminar shear strength (ILSS) of carbon fiber/epoxy (CE) composite is shown to be considerably improved by engineering the interface with carboxyl functionalized multi-walled carbon nanotube (FCNT) using electrophoretic deposition technique. FCNT deposited fibers from different bath concentrations (0.3, 0.5, and 1.0 g/L) were used to fabricate the laminates, which were then tested at room (30°C) and in-situ liquid nitrogen (LN) (−196°C) temperature as well as conditioning for different time durations (0.25, 0.5, 1, 6, and 12 h) followed by immediate RT testing to study the applicability of these engineered materials at the cryogenic environment. A maximum increment in ILSS was noticed at bath concentration of 0.5 g/L, which was ~21% and ~ 17% higher than neat composite at 30°C and − 196°C, respectively. Short-term LN conditioning was found to be detrimental due to developed cryogenic shock, which was further found to be compensated by cryogenic interfacial clamping upon long-term exposure. 相似文献
Wireless body area network (WBAN) has witnessed significant attentions in the healthcare domain using biomedical sensor-based monitoring of heterogeneous nature of vital signs of a patient’s body. The design of frequency band, MAC superframe structure, and slots allocation to the heterogeneous nature of the patient’s packets have become the challenging problems in WBAN due to the diverse QoS requirements. In this context, this paper proposes an Energy Efficient Traffic Prioritization for Medium Access Control (EETP-MAC) protocol, which provides sufficient slots with higher bandwidth and guard bands to avoid channels interference causing longer delay. Specifically, the design of EETP-MAC is broadly divided in to four folds. Firstly, patient data traffic prioritization is presented with broad categorization including Non-Constrained Data (NCD), Delay-Constrained Data (DCD), Reliability-Constrained Data (RCD) and Critical Data (CD). Secondly, a modified superframe structure design is proposed for effectively handling the traffic prioritization. Thirdly, threshold based slot allocation technique is developed to reduce contention by effectively quantifying criticality on patient data. Forth, an energy efficient frame design is presented focusing on beacon interval, superframe duration, and packet size and inactive period. Simulations are performed to comparatively evaluate the performance of the proposed EETP-MAC with the state-of-the-art MAC protocols. The comparative evaluation attests the benefit of EETP-MAC in terms of efficient slot allocation resulting in lower delay and energy consumption.
Synthesis of SiC ceramic from processed cellulosic bio-precursor was investigated. Bamboo (Bambusa tulda Roxb.) plants abundantly available in the Jorhat district of Assam, India, were selected for extraction of fibers following Kraft pulping method and bleached bamboo pulp fibers were suitably cast in the form of rectangular boards. Coir fibers available in the Alleppy district of Kerala, India, were initially digested with dilute alkali, mixed with cellulose acetate solution, air dried and then hot-pressed at 140 ± 5 °C under 2.0–2.5 MPa pressure to make rectangular boards. Well-characterized processed bio-precursors were pyrolysed at ~800 °C under flowing N2 atmosphere to prepare the bio-carbonaceous preforms (carbon templates) which showed nearly uniform shrinkages in all directions. Coir fiber composite board carbon showed lower pyrolytic weight loss (~66%), higher density (0.49 g cm?3), lower porosity (~58%) and narrower pore diameter (10 μm) compared to the cast bamboo pulp fiber board carbon. The carbon samples showed perfect retention of fibrous morphological features of hierarchically grown bio-structures. Ceramization of carbon templates could be done by reactive melt silicon infiltration into porous channels at ~1600 °C under vacuum. The final ceramics were adequately dense (%theoretical density > 99%), showed negligible linear dimensional changes (indicating net-dimension formation capability), presence of crystalline Si and SiC phases and duplex microstructure with complete preservation of fibrous architecture of plant bio-structure. The Si/SiC ceramic composite synthesized from coir fiber board gave room temperature 3-point flexural strength and Young's modulus values of 121 MPa and 276 GPa, respectively. Both the ceramic composites showed adequate oxidation resistance during heating at 1300 °C for 7 h in air. 相似文献
Stems of Jute (Corchorus capsularis L.) and sticks of Cane (Calamus rotang L.), plants of immense economic importance in the Indian subcontinent, were converted into carbonaceous perform (C-preform)
maintaining the circular cylindrical shapes in lengths of 0.02–0.05 m by controlled thermal processing. Plant material precursors
were characterized by analysis of elemental (C, H, N) and molecular (cellulose, hemicellulose, lignin) compositions, by determination
of Bulk Density (BD) and ash content and by optical microscopy and X-ray diffractometry (XRD). C-preforms were also characterized
by measurement of BD and by Scanning Electron Microscopy (SEM) and XRD. The C-preforms were further subjected to infiltration
with Si-melt (1823–1923 K) under vacuum. Spontaneous infiltration and reaction yielded composite ceramics preserving the morphology
of native Jute Stem (JS) and Cane Stick (CS) precursors on macro and micro scale. The materials were found to be duplex composites
with Si and β-SiC as crystalline phases. The end ceramics were characterized by measurement of BD, and also by SEM and by
XRD. Measured mean BD of the Si/SiC composites derived from JS and CS were 2190 Kg m−3 and 2250 Kg m−3. The respective volume fractions of large diameter (>100 μm) bulk pores were 0.134 and 0.204, in the composites derived from
JS and CS. Taking into account the measured volume fraction internal pores of 0.11 and 0.149, the volume fractions of SiC
were calculated to be 0.136 and 0.307 in the composites derived from JS and CS respectively, closely tallying with those calculated
from the C-preform bulk densities. The cellular Si/SiC ceramics derived from JS and CS having special morphologies with long
and large porous channels and oriented growth of constituent phases are likely to be suitable for devices such as high temperature
insulators, catalyst support structures for gas phase reactions at elevated temperatures, molten metal filters and others. 相似文献
Recently, Underwater Wireless Sensor Networks (UWSNs) has witnessed significant attention from both academia and industries in research and development, due to the growing number of applications for wide range of purposes including commercial, scientific, environmental and military. Some of the major applications include pollution monitoring, tactical surveillance, tsunami warnings and offshore exploration. Efficient communication among sensors in UWSNs is a challenging task due to the harsh environments and peculiar characteristics of UWSNs. Therefore, design of routing protocol for efficient communication among sensors and sink is one of the fundamental research themes in UWSNs. In this context, this paper proposes a location-free Reliable and Energy efficient Pressure-Based Routing (RE-PBR) protocol for UWSNs. RE-PBR considers three parameters including link quality, depth and residual energy for balancing energy consumption and reliable data delivery. Specifically, link quality is estimated using triangle metric method. A light weight information acquisition algorithm is developed for efficient knowledge discovery of the network. Multi-metric data forwarding algorithm is designed based on route cost calculation which utilizes residual energy and link quality. Simulations are carried out in NS-2 with Aqua-Sim package to evaluate the performance of RE-PBR. The performance of the proposed protocol is compared with the stat-of-the-art techniques: DBR and EEDBR. The comprehensive performance evaluation attests the benefit of RE-PBR as compared to the state-of-the-art techniques in terms of network lifetime, energy consumption, end-to-end delay and packet delivery ratio. 相似文献
A new, short, and quick method was developed for preparation of specimen for observing Actinomycetes of genus Streptomyces by scanning electron microscopy. The cultures were directly grown on stubs and coated with a film of gold without using any fixative and dehydrating procedures. Using this simple preparation procedure, surface of intact sporing structures of Streptomyces was observed over a range of magnifications. As the preparation procedure is so simple and rapid, this procedure could be most useful for the routine examination and identification of Streptomyces. 相似文献