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1.
The c-axis preferred orientation of ZnO film is the most important factor for its successful application in piezoelectric devices. The effects of surface roughness of the substrate on the c-axis preferred orientation of ZnO thin films, deposited by radio frequency magnetron sputtering, were investigated. During sputtering, the oxygen content in the argon environment used was varied from 0 to 70% at a total sputtering pressure of 10 mTorr. Very smooth Si, smooth evaporated Au/Si, smooth evaporated-Al/Si, and rough sputtered-Al/Si were used as substrates. Their r.m.s. roughnesses, as measured by atomic force microscopy, were 1.27, 17.1, 21.1 and 65-118 Å, respectively. The crystalline structure and the angular spread of the (0 0* 2) plane normal to the ZnO films were determined using X-ray diffraction and X-ray rocking curves, respectively. The crystallinity and the preferred c-axis orientation of the ZnO films were strongly dependent on the surface roughness of the substrates rather than on the oxygen content of the working environment or on the chemical nature of the substrate. 相似文献
2.
Seung-Yeop Kwak 《应用聚合物科学杂志》1995,55(12):1683-1690
The structural changes of poly(vinyl chloride) (PVC) plastisols during mixing of PVC with a plasticizer was investigated; as the temperature was increased, the system was found to transform from a suspension of solid particles in a liquid medium to a swollen gel and ultimately to a fused homogeneous matrix. The dynamic viscoelastic measurements were utilized to continuously monitor the changes of moduli under a controlled heating rate, employing a mechanical spectrometer. Characteristic changes in the viscoelastic behavior were associated with changes in particulate morphology as observed with a scanning electron microscope (SEM). Both viscoelastic and morphological observations were shown to provide details of structural changes in conjunction with the behavior of the PVC–plasticizer interaction, enabling a qualitative discrimination of the gelation and fusion processes. An in situ small-angle light-scattering (SALS) method was performed to make a quantitative estimate for the swollen particles of PVC while they were in the progress of gelation and fusion. From the manner of increase in correlation distances, along with the changes in viscoelastic moduli and morphology, the swelling behavior of the particulate structures were examined on the quantitative basis and brief insight into the complex behavior of the PVC–plasticizer interaction began to be unfolded. © 1995 John Wiley & Sons, Inc. 相似文献
3.
The energy release rate, which is the total derivative of the energy with respect to crack length, is recognized as corresponding to the shape sensitivity analysis with the crack length change represented by the tangential component of design velocity. In this paper the sensitivity formula recently developed for a changing boundary condition has been further extended to cover crack kinking under mixed mode loading. Due to difficulty in defining the velocity field at the corner, the energy release rate at the onset of crack kinking is obtained by extrapolating the energy release rates for finite length kinked cracks. A rectangular plate with a single edge slant crack under uniform tension is taken as a numerical example. The multi-region technique in the numerical implementation of the boundary integral equation is adopted to consider the asymmetry of the problem. Excellent accuracy is observed as compared with reference analytic solutions. 相似文献
4.
5.
ABSTRACT: Degrees of hydrolysis and emulsifying activity of casein hydrolysates were the highest at 4 h hydrolysis. The oil-off values of the mixture of hydrolysate (H) or supernatant (S) and traditional emulsifier (T) were not significantly different from the control made with traditional emulsifier, except for S + T = 3:1. Two other samples made with hydrolysate or supernatant only (H or S) showed higher oil-off value than the others (p < 0.05). In flavor property, no difference was found between samples made with traditional emulsifier and those made with the mixture of hydrolysate or supernatant at the ratio of 3 to 1. Therefore, these results indicated that a mixture of the hydrolysate or supernatant and traditional emulsifier might replace a traditional emulsifier in process cheese manufacturing. 相似文献
6.
Chul Kwak Stanley I. Sandler Hun-Soo Byun 《Korean Journal of Chemical Engineering》2006,23(6):1016-1022
The correlation of vapor-liquid equilibrium data for high-pressure carbon dioxide systems is of interest in a number of industrial
applications, including supercritical extraction. Here, we consider the correlation of data for 12 binary systems of carbon
dioxide separately with alcohols, with hydrocarbons, and with acetone, benzene, and water. The Wong-Sandler (W-S) and modified
Huron — Vidal first order (MHV1) free energy-based equation of state mixing rules (the W-S and MHV1 models) were used in the
calculations. Both combined equation of state+free energy models generally resulted in good correlations of the experimental
data over wide ranges of temperature and pressure with temperature — independent parameters. However, for the carbon dioxide+water
system, the W-S model produced an 11% average absolute deviation in pressure, while no parameter that resulted in an AAD in
pressure of less than 20% could be found for the MHV1 model. 相似文献
7.
In Gwun Jang Kyung-Soo Kim Byung Man Kwak 《Structural and Multidisciplinary Optimization》2014,50(3):505-515
The Mobile Harbor (MH) has been recently proposed as a novel maritime cargo transfer system that can move to a container ship anchored in the deep sea and handle containers directly at sea with the aid of a stabilized MH crane. Because this system operates under at-sea conditions, the MH crane must be designed to support an inertia load and wind force, as well as its self-weight. The wave-induced motions of the MH, e.g. rolling, pitching, and heaving, generate a significant amount of inertia load, which has not been considered in the design of conventional quayside cranes installed on stable ground. Wind force is also a critical design factor due to the higher wind velocity in the open sea. In addition to the aforementioned structural rigidity, mass minimization is also important in the structural design of MH cranes because it reduces the overturning moment and therefore enhances ship stability. In this paper, the sensitivities of the design-dependent loads (i.e. self-weight, inertia load, and wind force) are derived with respect to the design variables, and then a topology optimization is conducted with the derived sensitivities in order to obtain a conceptual design. Then, the conceptual design is elaborated into a three-dimensional basic design through shape optimization with design regulations for offshore cranes. Through the integrated design process with the topology and shape optimizations, a conceptual and basic design is successfully obtained for the MH crane. 相似文献
8.
The effect of the reaction kinetics on the ionic conductivity for a comblike‐type polyether (MEO) electrolyte with lithium bis(trifluoromethane sulfonyl)imide (LiTFSI) was characterized by DSC, complex impedance measurements, and 1H pulse NMR spectroscopy. The ionic conductivity of these electrolytes was affected by the reaction condition of the methacrylate monomer and revealed by the glass transition temperature (Tg), spin–spin relaxation time (T2), steric effects of the terminal groups, and the number of charge carriers indicated by the VTF kinetic parameter. In this system, the electrolytes prepared by the reaction heating rate of 10°C/min of MEO–H and 15°C/min of MEO–CH3 showed maximum ionic conductivity, σi, two to three times higher in magnitude than that of the σi of the others at room temperature. As experimental results, the reaction kinetic rate affected the degree of conversion, the ionic conductivity, and the relaxation behaviors of polyether electrolytes. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 89: 2149–2156, 2003 相似文献
9.
Jose E. Herrera Ja Hun Kwak Jian Zhi Hu Yong Wang Charles H. F. Peden 《Topics in Catalysis》2006,39(3-4):245-255
The advantages of the atomic layer deposition (ALD) method for preparation of tungsten, vanadium, titanium, and molybdenum
oxide catalyst supported on mesoporous silica are discussed, with emphasis on the importance of synthesis conditions on dispersion,
structure and activity of the resulting materials. A suite of complementary techniques such as DRS-UV/Vis, BET, 1H-NMR, XRD, and TEM were used to study the structural properties of the supported metal oxides, and probe reactions such as
2-butanol dehydration and ethanol partial oxidation were used to demonstrate the potential advantages of the ALD-prepared
catalysts. Specifically, highly dispersed oxides of titanium, molybdenum, and tungsten oxide on mesoporous silica were synthesized
using the ALD method. It is also demonstrated that attainment of high dispersions of vanadium oxide on mesoporous silica requires
the presence of at least a single layer of titanium oxide due to the well-known poor interaction between vanadia and silica.
The highly dispersed catalysts prepared here by ALD methods exhibited superior catalytic performance relative to those prepared
using conventional incipient wetness impregnation. 相似文献
10.
Jung-Ho Ahn Cheolmin Choi Sooyeong Kwak Kilcheon Kim Hyeran Byun 《Pattern Analysis & Applications》2009,12(2):167-177
In this study, we propose a new integrated computer vision system designed to track multiple human beings and extract their
silhouette with a pan-tilt stereo camera, so that it can assist in gesture and gait recognition in the field of Human–Robot
Interaction (HRI). The proposed system consists of three modules: detection, tracking and silhouette extraction. These modules
are robust to camera movements, and they work interactively in near real-time. Detection was performed by camera ego-motion
compensation and disparity segmentation. For tracking, we present an efficient mean shift-based tracking method in which the
tracking objects are characterized as disparity weighted color histograms. The silhouette was obtained by two-step segmentation.
A trimap was estimated in advance and then effectively incorporated into the graph-cut framework for fine segmentation. The
proposed system was evaluated with respect to ground truth data, and it was shown to detect and track multiple people very
well and also produce high-quality silhouettes.
相似文献
Hyeran ByunEmail: |