Ti基MnO_x型DSA析氧电极材料的性能

本文报导了新型 Ti/SnO_2+MnO_x+RuO_2/MnO_x(DSA)电极材料的各种性能,其中包括电极的导电性、表面粗糙度、电化学活性表面积、析氧阳极特性等,并用 X 射线衍射法进行了物相分析、用 SEM观察了表面形貌。确认该电极性能良好,加之成本较低,可作为酸性介质中的析氧电极材料。     

察尔汗盐湖镁资源的开发及展望

察尔汗盐湖不仅具有丰富的镁资源，而且具有开发盐湖的能源，政策优势，由脱水氯化镁可制得多种镁产品。氯化镁脱水技术，氯化镁制金属镁技术是综合开发盐湖水镁资源的关键技术，将纳米技术应用于盐湖镁资源的开发，使镁产品高值化，精细化，将是察尔汗盐湖镁资源的开发方向。     

浅论宋代陶瓷造型

陶瓷器首先是为实际生活需要而“造物”的产品，同时又是按着审美规律寻求“造型”的艺术创造。每个时代的陶瓷造型都会有所不同。宋代是瓷的时代，此时陶瓷造型追求一种质朴静润，自然天成，趣味高雅的意境，其轮廓线条流畅，造型端庄。法度严谨，做工精细，优美的形象体现着宋人典雅朴素的气质风度和追求的美学境界。本文试图从宋代当时社会政治生活和生产、制瓷工艺的发展、审美观等几方面对宋代陶瓷造型的影响进行了初步的研究。     

Characterization and performance of Pd-La/spinel catalyst for preparation of 2,6-diisopropylaniline

The Pd-La/spinel catalyst for the preparation of 2,6-diisopropylaniline (2,6-DIPA) by gas-phase amination of 2,6-diisopropylphenol (2,6-DIPP) has been studied. The catalysts before and after reaction were characterized by BET, XRD, differential thermal analysis (DTA)-thermo gravimetric analysis (TGA), FTIR, and NH₃-TPD techniques. The DTA study results show two kinds of coke deposited on the metal and support of Pd-La/spinel catalyst, and they are combusted at about 242 and 324 °C, respectively. The XRD and FTIR spectra of the Pd-La/spinel catalyst show that the coke contains the aromatic and aliphatic rings, alkyl groups, polynuclear aromatic system, hydroxyl groups, and amine groups. The reason for catalyst deactivation can be expressed as follows: coke formed on palladium metals may move from metal to the interface or boundaries of metal-support and acid sites of the support where further dehydrogenation and polymerization are occurring. The H₂ plays a key role in retarding coke formation, but must be in suitable amount to get relatively high selectivity. The rare earth promoter La not only promotes the activity and selectivity by retaining Pd species in the metallic state, but also decreases the formation of carbon by neutralizing the strong acid sites on the catalyst.     

烧结助剂对氮化硅陶瓷显微结构和性能的影响

氮化硅中氮原子和硅原子的自扩散系数很低，致密化所必需的扩散速度和烧结驱动力都很小，在烧结过程中需采用烧结助剂。烧结助剂是影响氮化硅陶瓷的显微结构和性能的关键因素之一。有效的烧结助剂不但可以改善氮化硅陶瓷的显微结构，而且可以提高氮化硅陶瓷的高温性能和抗氧化性能。     

7.50-16 12PR轻型载重轮胎的优化设计

介绍轻型载重轮胎的优化设计。采取的主要措施是：减小轮胎外缘尺寸，外直径由８０８ｍｍ减至７９８ｍｍ，断面宽由１９８ｍｍ减至１９５ｍｍ；胎面花纹以纵向花纹为主，肩部为纵横结合花纹并加深肩部通挖花纹沟的深度，改善肩部生热；胎体帘布采用加粗减层的方法，用６层１８７０ｄｔｅｘ／２尼龙帘布代替８层１４００ｄｔｅｘ／２帘布。优化轮胎重量减轻４ｋｇ，轮胎性能符合国家标准。     

基于态势熵的网络安全态势评估指标体系研究

针对网络安全态势评估指标体系的不完善和难以选取及构建等问题,以相关标准和规范为基础,从系统安全机制出发,按照既定原则,提出了基于态势熵的网络安全态势评估指标体系的构建方法,并给出了网络可用性方面的态势评估指标值的计算方法.实验表明,态势熵值的变化与所反映的网络安全态势是一致的,说明该指标体系的构建具有一定的科学性,为网...     

模糊层次分析法在B2C网购中的应用

信息网络技术的不断发展使网购逐渐成为人们购买物品的方式之一,但是网上信息的真实与否也带来了购物烦恼.通过调查问卷和已有文献,分析了消费者在商家对顾客模式(B2C)网站上购物时主要考虑的影响因素指标,用模糊层次分析(Fuzzy-AHP)法对这些指标进行了评价分析,从而把模糊的信息指标量化.研究结果以直观的评价结果为消费者网购提供了参考.     

Virtual-Point-Based asymptotic tracking control of 4WS vehicles

This paper studies the lateral and longitudinal path tracking control of four-wheel steering vehicles. By the introduction of virtual points, a robust and adaptive path tracking control strategy is proposed to simultaneously counteract modeling uncertainties, unexpected disturbances, and coupling effects. An adaptive model-based feedforward adaptive term and the robust integral of the sign of the error (RISE) feedback term can be used to yield an asymptotic tracking result, which improve the tracking performance and reduce the control effort. The stability of closed-loop system is analyzed using a Lyapunov-based method. Simulation results are provided to demonstrate the performance of the proposed controller under different driving conditions.     

Fe_3O_4@MgO纳米复合材料的制备及其对Pb~(2+)的吸附性能

采用两步化学沉淀法制备了Fe_3O_4@MgO纳米复合材料,研究了纳米复合材料对Pb~(2+)的吸附性能。结果表明,所制备的复合材料具有较高的顺磁性和稳定性,其饱和磁化强度为58.07 emu/g,初始氧化增重温度为125℃,对Pb~(2+)有较好的吸附能力,在50 min内可以达到吸附平衡,最大吸附量为711.5 mg/g,其吸附过程符合准二级动力学模型和Langmuir等温吸附模型。