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A novel process for increasing β-SiC yield on solid state reaction of coal fly ash and micro powder activated carbon powder has been proposed. β-SiC powder was synthesized at temperature 1300°C for 2 h under vacuum condition with 1 l/min argon flow. Cycling synthesis process has been developed for increasing β-SiC yield on solid state reaction of coal fly ash and activated carbon powder. Synthesized products were analyzed by XRD with Cu-Kα radiation, FTIR spectrometer and SEM fitted with EDAX. The results show that the amount of relative β-SiC is increased with the number of cycling synthesis.  相似文献   
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