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Synthesis of Single-Crystalline Silicon Nitride Nanobelts Via Catalyst-Assisted Pyrolysis of a Polysilazane 总被引:1,自引:0,他引:1
Weiyou Yang Zhipeng Xie Hezhuo Miao Ligong Zhang Hang Ji Linan An 《Journal of the American Ceramic Society》2005,88(2):466-469
Recently, one-dimensional nanostructures have attracted extensive attention since they are potentially important for both applications and fundamental research. In this paper, we report the synthesis of ultra-long single crystal Si3 N4 nanobelts via catalyst-assisted pyrolysis of polymeric precursors. The obtained products contain both α- and β-Si3 N4 nanobelts, which are 50–100 nm in thickness, 400–1000 nm in width, and a few hundreds of micrometers to several millimeters in length. Different from previous techniques for synthesizing one-dimensional structures, the current nanobelts are synthesized through confined crystallization of an amorphous phase. A solid–liquid–gas–solid reaction/crystallization growth mechanism is proposed. The formation of nanobelts instead of nanowires is attributed to the anisotropy growth at an earlier stage. 相似文献
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Zhenyu Zhu Zihan Sun Shudong Zhou Shang Xu Xiaoxiao Li Weijun Li Lin Wang Weiyou Yang Fengmei Gao Shanliang Chen 《Journal of the American Ceramic Society》2022,105(2):806-814
Low turn-on field (Eto) and stable electron emission are two of key parameters for reliable application of field emission (FE) cathodes. In the present work, we developed a novel high-performance integrated field emission cathode based on well-aligned SiC nanocone arrays via an electrochemical etching approach. The etched SiC nanocone emitters and the underlying remaining SiC wafer are designed into a single-crystalline integrated architecture without interfaces, which favors cathodes with a sturdy configuration to resist Joule heat during long period electron emission process and structural failure caused by the existed strong electrostatic forces. Accordingly, the Eto of the integrated SiC cathode is reduced to 0.32 V/μm, which is the lowest value among all the previously reported SiC nanostructured emitters. In addition, the integrated cathode presented superior stability with an electron emission fluctuation of 3.3% over 10 h. This work provides a new perspective for designing and fabricating advanced FE cathodes for further promising applications in harsh working conditions with high performance. 相似文献
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水力机组振动监测与故障诊断 总被引:4,自引:1,他引:4
针对水力机组运行过程中因振 动而引起故障并造成经济损失这一问题,开发了一套新型的振动监测及故障诊断系统,它以 工业PC 机为主体,与摆度、振动传感器及有关功能模块和信号预处理器共同组成机组振动 在线监测分析系统。利用该系统对机组振动的周期性监测,能够在线监测机组缺陷的缓慢变 化过程,为视情检修提供良好的依据,同时也为机组运行调度提供可靠的信息。介绍了该系 统的硬件及软件组成、原理及功能,并结合实例运用小波分析与傅里叶分析相结合的信号分 析方法,对机组故障进行了分析诊断,找出了故障原因。 相似文献
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Polygonal Single-Crystal Aluminum Borate Microtubes 总被引:1,自引:0,他引:1
Weiyou Yang Zhipeng Xie Jingtao Ma Hezhuo Miao Jiesheng Luo Ligong Zhang Linan An 《Journal of the American Ceramic Society》2005,88(2):485-487
In this paper we report the synthesis of polygonal single-crystal aluminum borate microtubes by the direct calcination of alumina and boron nitride powders in air. The diameters of the obtained tubes vary between 1 and 15 μm; and the lengths are in the range of tens to hundreds of micrometers. The cross-sections of the microtubes are in the shapes of rectangular, hexagonal, and quasi-circle. A new solid–liquid–solid growth mechanism was proposed to account for the formation of microtubes instead of whiskers. 相似文献
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Weiyou Yang Huatao Wang Xiaomin Cheng Zhipeng Xie Linan An 《Journal of the American Ceramic Society》2008,91(8):2732-2735
We report the synthesis of perfect single-crystal Al2 O3 microspheres via direct thermal decomposition of aluminum isopropoxide in air without any template or catalyst. The obtained microspheres were characterized using scanning electron microscopy, X-ray diffraction, transmission electron microscopy, and selective area electron diffraction. The results suggested that the formation of the spheres can be attributed to a transition from polycrystalline to single-crystalline symmetry during high-temperature annealing. The obtained microspheres could be useful for many applications such as lubricants and polishing mediums. 相似文献