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ZnO单晶的KOH碱液法生长和表征(英文) 总被引:2,自引:1,他引:1
采用自发成核方法,以KOH碱液作助熔剂,在银、镍和铁坩埚中分别生长了透明、棕绿色和棕色的纤维锌矿氧化锌单晶。X射线衍射和电感耦合等离子体原子发射光谱分析表明:晶体的颜色与所含的杂质有关,这些杂质来源于所使用的坩埚。采用光致发光(photoluminescence,PL)光谱对所生长的晶体进行了表征,结果显示,从银坩埚中生长的氧化锌晶体质量较高,其室温下用325nm波长光激发的PL光谱显示381nm强的紫外发射峰。在此基础上,从200mL银坩埚中生长出了尺寸为φ3mm×34mm氧化锌晶体。 相似文献
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探讨子用界面聚合法制备尼龙包油胶囊的实验条件,研究了不同配料比对胶囊性质的影响,得到制备稳定包油胶囊的最佳实验条件。 相似文献
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沸石负载TiO2光催化剂的制备及其性能研究 总被引:1,自引:0,他引:1
以钛酸四丁酯和乙醇为原料,采用溶胶-凝胶(sol-gel)法制备以天然沸石为载体的负载型TiO2光催化剂,并利用X射线衍射(XRD)和扫描电镜(SEM)等对其进行结构表征.通过自行设计的光催化反应器,考查溶胶-凝胶体系的组成、焙烧温度及焙烧时间等因素对光催化剂降解造纸废水性能的影响,同时讨论该催化剂的可重复利用性,确定制备天然沸石负载型二氧化钛光催化剂的最佳实验条件:无水乙醇与钛酸四丁酯的体积比为4.0,冰醋酸与钛酸四丁酯的体积比为0.1,水与钛酸四丁酯的体积比为0.15,硝酸与钛酸四丁酯的体积比为0.1,焙烧温度为300℃,焙烧时间为4 h,造纸废水COD去除率可达81.93%. 相似文献
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Pure and different content europium(Eu) doped mesoporous titania were prepared by template method using Eu(NO3)3.6H2O andTi(OC4H9)4 as precursors and Pluronic P123 as template and characterized with X-ray diffraction(XRD),N2 adsorption-desorption measurements,and ultraviolet-visible diffuse absorption spectra.Their photocatalytic activities were studied by photodegradation phenol in water under visible light irradiation.The results showed that Eu doping restrained the growth of grain size and extended the p... 相似文献
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TiO_2 nanoparticles coated cotton fiber composite was successfully prepared by using a sol-gel method at low temperature(about 100℃) using tetrabutyl-titanate [Ti(OBu)_4] as raw material.The preparation of the TiO_2 colloid and the composite were described.The properties of resulting materials were characterized by SEM and XRD,the photocatalytic degradation performance was tested using methylene blue(MB) as the target pollutant in aqueous solution.The results showed that the amorphous TiO_2 nanoparticles were distributed evenly on the outer surfaces of cotton fibers,which shows efficient photocatalytic properties when exposed to UV light,the degradation rate of MB reached 95.35% under the conditions of catalyst dosage 2.5 g/L,MB concentration 50 mg/L,irradiation time 120 min,and pH 10,and the photocatalytic activity of TiO_2/cotton fibers remained above 90% of its activity as-prepared after being used four times,the degradation rate of MB could reach 88.78% when irradiation time was 120 min.The photocatalytic degradation of MB could be properly described by the first-order kinetic law.By comparison of the removal rates of MB with and without UV light,it could be affirmed that the disappearance of MB was due to photodegradation rather than adsorption on cotton fibers. 相似文献
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采用MNDO、一维紧束缚CNDO/2-CO方法研究聚并苯(PAS)、聚并吡啶(PPyPy)及多聚氰(PC)的分子结构,揭示结构稳定性和电荷分布的变化规律。能带结构分析指出:N原子的引入改变分子结构,增加亲电和亲核掺杂反应的活性点,但本征电导率并没有增加。 相似文献
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若干新型热电材料的热输运调控及热逻辑器件 总被引:1,自引:0,他引:1
随着电子和能源科技的发展,基于纳米结构调控的新型热电材料以及热逻辑器件研究正受到越来越多的关注。本工作围绕几种具有应用潜力的热电材料,利用项目团队自主开发的微纳尺度热输运测试系统,从理论和实验上研究了原子及纳米尺度结构对热输运特性的调控机制,包括:全组分Si1–xGex合金薄膜的原子合金化,Bi2Ca2Co2Oy层状结构单晶的错配界面,超离子导体A0.5Rh O2 (A=K,Rb,Cs)单晶的离子局域共振,准一维结构Zr Te5/Hf Te5单晶中的疏松微结构,以及Sn Se单晶中的Sn Se2原子级插层,总结了不同尺度结构和原子间作用力对热传导性质的影响规律,为探索低热导率、高热电转换性能的新型热电材料提供有效的调控方案。最后,介绍了利用相变转换机制实现热导率高效动态调控的实验结果,及其在热逻辑器件方面的潜在应用。 相似文献