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微波烧结W-Ni-Fe高密度合金的变形现象及显微组织 总被引:3,自引:0,他引:3
以还原钨粉、羰基镍粉和羰基铁粉为原料,采用微波烧结和常规液相烧结法制备90W-7Ni-3Fe高密度合金,对比研究该合金的变形现象及相对密度和硬度,并对合金样品顶部和底部区域的SEM照片进行分析。结果表明:在温度1 500℃和保温10 min的条件下,经微波烧结的合金变形现象得到有效控制,垂直收缩率偏差和水平收缩率偏差分别为0.21%和0.72%,而常规烧结的垂直收缩率偏差和水平收缩率偏差分别为1.23%和3.25%;微波烧结样品的相对密度为99.88%,略高于常规烧结的99.48%;微波烧结合金的硬度(HRC)比常规烧结高2.3,平均晶粒尺寸比常规烧结低5.88μm;并且,微波烧结样品顶部与底部的液相含量、接触度、晶粒尺寸以及硬度的差异均较小,表明微波烧结的合金晶粒细小、组织均匀。 相似文献
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C掺杂Mg(B1-xCx)2的电子结构和弹性性质的第一性原理研究 总被引:1,自引:0,他引:1
利用基于密度泛函理论(Density functional theory,DFT)的广义梯度近似(Generalized gradient approximation,GGA)研究C掺杂Mg(B(1-x)Cx)2晶体的电子结构和弹性性质.计算所得晶格参数和平衡态体积与实验结果符合较好.能带结构和态密度的研究结果表明,随... 相似文献
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分析了圆片冲击法硅片强度测试中简支半径对动载荷挠度及强度测试值的影响,实验求得直径50.8mm硅片抗弯强度测试值的校正系数为0.8。 相似文献
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The green and sintered densities,and tensile strength of sintered P/M steels produced by cold compaction,warm compaction,warm compaction combined with die wall lubrication(DWL)were measured under various compaction pressures using polytetrafluoroethylene(PTFE)emulsion as the die wall lubricant.The effects of warm compaction on the mechanical properties were studied.The tensile fracture behaviors of cold compaction and warm compaction were studied using scanning electron microscope(SEM).The results show that the density of sintered P/M steel prepared by warm compaction or warm compaction with DWL is higher than that by cold compaction under all compaction pressures.Meanwhile,the highest tensile strength is obtained by combination of warm compaction and die wall lubrication under all compaction pressures.The SEM results show that the fracture modes of the sintered samples prepared by cold compaction and warm compaction at 700 MPa are the mixed mode of ductile fracture and brittle fracture,and obvious dimples can be found in some regions.The fracture of sample prepared by cold compaction is uneven and has irregular and big pores,but that by warm compaction is relatively even and the pores are round mostly,and the samples have many obvious dimples on the whole fracture surface. 相似文献
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压制压力对微波烧结W-Ni-Fe高密度合金性能的影响 总被引:1,自引:0,他引:1
以还原钨粉、羰基镍粉和羰基铁粉为原料,研究了压制压力对微波烧结90W-7Ni-3Fe高密度合金性能的影响,并对分别在1 480℃和1460℃烧结的合金性能进行对比分析.实验结果表明:微波烧结W-Ni-Fe高密度合金的密度和力学性能随压制压力升高而升高,在600 MPa时达到最大,随后迅速下降.在1 480℃进行微波烧结的合金,其各项性能明显高于在1 460℃烧结的,例如,在600 MPa时,前者的相对密度为97.5%,而后者为96.3%;前者的断口存在穿晶断裂,后者则沿晶断裂明显. 相似文献
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