氨精制装置运行问题分析及改造措施

通过分析中国石油兰州石化分公司炼油厂氨精制装置存在的运行问题,提出了相应的改造措施,包括在分凝器脱液管线上新增隔离阀门、更换三级冷凝冷却器、更换氨压缩机及采用低温结晶脱硫工艺等。改造后装置运行结果表明:三级分凝器出口温度由70℃降至小于35℃,压缩机吸气量由5 m3/m in提高至74 m3/m in,原料酸性水中硫化氢质量分数下降45.5%,氨质量分数下降55.5%,净化水合格率达100%,氨精制塔塔顶温度下降5~20℃,液氨中氨质量分数由97.05%上升至99.60%,液氨产量达0.125 t/h,实现了装置的长周期运行。     

汽车自动传动液的研制

介绍了自动传统液的分类规格、自动传动液的特性和相关的评定方法；研制了无锌和低锌配方的两种产品，经评定试验和实机使用，符合ＤｅｘｒｏｎⅡＤ、Ｍｅｒｃｏｎ和ＡｌｌｉｓｏｎＣ－４的规格要求，达到了国外同类产品的质量水平。     

对交替工作式氧化沟几个技术问题的探讨

从交替工作式氧化沟处理城市污水实例的运行资料出发 ,并在着重分析COD ,SS的超标原因及影响因素的基础上 ,提出了达标排放改进技术及完善工艺建议。     

二辊轧机轧辊堆焊新技术应用

介绍了二辊粗轧机轧辊利用堆焊新技术开展堆焊修复试验与应用，并介绍了堆焊材料的选择、堆焊工艺以及取得的良好效果。     

MPaaS: Mobility prediction as a service in telecom cloud

Mobile applications and services relying on mobility prediction have recently spurred lots of interest. In this paper, we propose mobility prediction based on cellular traces as an infrastructural level service of telecom cloud. Mobility Prediction as a Service (MPaaS) embeds mobility mining and forecasting algorithms into a cloud-based user location tracking framework. By empowering MPaaS, the hosted 3rd-party and value-added services can benefit from online mobility prediction. Particularly we took Mobility-aware Personalization and Predictive Resource Allocation as key features to elaborate how MPaaS drives new fashion of mobile cloud applications. Due to the randomness of human mobility patterns, mobility predicting remains a very challenging task in MPaaS research. Our preliminary study observed collective behavioral patterns (CBP) in mobility of crowds, and proposed a CBP-based mobility predictor. MPaaS system equips a hybrid predictor fusing both CBP-based scheme and Markov-based predictor to provide telecom cloud with large-scale mobility prediction capacity.     

First-Principles Study of the High-Temperature Behaviors of the Willemite-Ⅱ and Post-Phenacite Phases of Silicon Nitride

The structural and elastic properties of the recently-discovered wⅡ- and δ-Si_3N_4 are investigated through the plane-wave pseudo-potential method within ultrasoft pseudopotentials.The elastic constants show that wⅡ- and δ-Si_3N_4 are mechanically stable in the pressure ranges of 0-50 GPa and 40-50 GPa,respectively.The α→wⅡ phase transition can be observed at 18.6 GPa and 300 K.The β→δ phase transformation occurs at pressures of 29.6,32.1,35.9,39.6,41.8,and 44.1 GPa when the temperatures are100,200,300,400,500,and 600 K,respectively.The results show that the interactions among the N-2s,Si-3s,3p bands(lower valence band) and the Si-3p,N-2p bands(upper valence band) play an important role in the stabilities of the wⅡ and S phases.Moreover,several thermodynamic parameters(thermal expansion,free energy,bulk modulus and heat capacity) of δ-Si_3N_4 are also obtained.Some interesting features are found in these properties.δ-Si_3N_4 is predicted to be a negative thermal expansion material.The adiabatic bulk modulus decreases with applied pressure,but a majority of materials show the opposite trend.Further experimental investigations with higher precisions may be required to determine the fundamental properties of wⅡ- andδ-Si_3N_4.     

原位模板法在铝基底上制备TiO2纳米管阵列薄膜

采用液相沉积法，将铝基多孔阳极氧化铝（AAO）模板浸入到（NH4）2TiF6溶液中，制备出高度有序的TiO2纳米管阵列薄膜，并在不同的温度下进行了热处理。用场发射扫描电子显微镜、透射电子显微镜和X射线衍射仪等手段对试样的微观形貌、结构及物相进行了表征。结果表明，TiO2纳米管的形貌依赖于AAO的特征，薄膜是由外径大约200nm，壁厚约40nm的TiO2纳米管阵列组成，薄膜厚度约25μm。原位模板法制备的TiO2纳米管阵列薄膜为非晶态，在400℃空气中焙烧2h转变为锐钛矿相TiO2。经过650℃焙烧仍保持纳米管结构，表现出较好的热稳定性。     

电脉冲孕育处理Al-22Si合金衰退性的研究

研究了电脉冲孕育处理后不同静置时间对Al-22Si合金凝固组织中初生相形态、大小、分布的影响。结果表明，电脉冲处理后立刻浇注对Al-22Si合金有较明显的变质作用，初生Si相形态由粗大板条状变为块状，其平均尺寸由153．15μm降至77．35μm，分布也较均匀；但电脉冲处理也存在着较明显的衰退性，即随着熔体静置时间的延长孕育效果逐渐消失，当静置时间为80min时，其组织形态与未经电脉冲处理的组织相似，其平均尺寸由77．35μm升至143．67μm。     

Effect of electric pulse treatment on solidification structure of an A1-15%Si alloy

The effect of electric pulse modifying on the solidification structure of an Al-15%Si alloy was investigated. The result shows that the primary silicon disappears sometimes and the eutectic phase is refined after the treatrnent of EP （electric pulse） though there are different modalities in different treating durations. DSC （differential scanning calorimetry） analysis indicates that the super-cooling texture decreases and the freezing range narrows evidently after the electric pulse treatment.     

电脉冲孕育处理对Al-5Cu合金热裂的影响

研究了不同电脉冲孕育处理参数对Al-5Cu合金热裂倾向的影响.结果表明,不同电脉冲孕育处理参数均可降低Al-5Cu合金的热裂倾向,处理后该合金热裂临界应力比未处理试样提高了约3倍.合金热裂倾向改善的原因是,电脉冲孕育处理细化了Al-5Cu合金组织,减少了共晶相的数量,缩短了合金凝固温度区间.