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1.
Determination of dislocation densities in HCP metals from X-ray diffraction line-broadening analysis
Griffiths M. Sage D. Holt R. A. Tome C. N. 《Metallurgical and Materials Transactions A》2002,33(13):859-865
X-Ray diffraction (XRD) line-broadening analysis has been performed on highly textured Zr-2.5Nb specimens which had been deformed
in tensile tests to produce well-controlled dislocation structures. An iterative deconvolution method has been applied to
extract the broadening function for the material, using as standards, a Zr single crystal and a 0 pct deformed specimen. In
both cases, for specific tensile tests, a significant contribution to the basal line braodening was observed, which was clearly
not directly related to the dislocation structure generated by the deformation, i.e., so-called c-component dislocations having a component of their Burgers vectors perpendicular to the basal plane. Calculations showed
that the extent of basal line broadening cannot be attributed to the secondary effect of strain from a-type dislocations, i.e., dislocations with Burgers vectors parallel with the basal plane. It is concluded that most of the line broadening observed
was the result of intergranular strain distributions. These distributions are most prominent for grains oriented with their
c-axes perpendicular to the tensile-deformation axis and resulted in basal-plane line broadening even when there were few,
if any, c-component dislocations present.
This article is based on a presentation made in the symposium entitled “Defect Properties and Mechanical Behavior of HCP Metals
and Alloys” at the TMS Annual Meeting, February 11–15, 2001, in New Orleans, Louisiana, under the auspices of the following
ASM committees: Materials Science and Critical Technology Sector, Structural Materials Division, Electronic, Magnetic & Photonic
Materials Division, Chemistry & Physics of Materials Committee, Joint Nuclear Materials Committee, and Titanium Committee. 相似文献
2.
C. G. Gwie R. J. Griffiths D. T. Cooney M. L. Johns D. I. Wilson 《Journal of the American Oil Chemists' Society》2006,83(12):1053-1062
The spray-freezing of two food fats, tripalmitin (PPP) and cocoa butter (CB) and mixtures thereof, has been modeled experimentally
using a novel single droplet freezing apparatus configured so that temperature profiles or samples for microstructure analysis
can be obtained. For 2 mm diameter droplets suspended in a cold air flow at temperatures around 2–15°C, initial cooling rates
were on the order of 10 K s−1 and the temperature profiles could be correlated directly to DSC data collected at 20 K min−1, indicating that minimal supercooling of the materials occurred in the droplet form. Microstructure analysis confirmed that
PPP crystallized preferentially in mixtures, and that the surface structure was very sensitive to storage conditions. The
bulk structure was much less sensitive, and the internal microstructure of the PPP droplets revealed distinct nucleation sites,
which were absent from the CB: These persisted in the mixtures up to 50 wt%. X-ray analysis indicated that the fats crystallized
in their more stable forms, namely, β for PPP and Form V/V1 in CB. 相似文献
3.
Beta-COP is essential for biosynthetic membrane transport from the endoplasmic reticulum to the Golgi complex in vivo 总被引:2,自引:0,他引:2
R Pepperkok J Scheel H Horstmann HP Hauri G Griffiths TE Kreis 《Canadian Metallurgical Quarterly》1993,74(1):71-82
Experimental glomerulonephritis was induced in rats to investigate the consequence of the antigen-antibody interaction on the surface of glomerular endothelial cells (GENs). A lectin, Lens culinaris hemoagglutinin (LCH), was first planted in the left kidney by isolated perfusion of a left kidney, and then the circulation was reestablished. Rabbit anti-LCH antibodies were injected from the tail vein 3 minutes after the recirculation of the left kidney, and acute glomerulonephritis ensued. Fifteen minutes after the injection, rabbit immunoglobulin G (IgG), rat C3, and LCH were observed exclusively on the surface of GENs. Accumulation of platelets was prominent. Three hours later, the immune deposits were seen in the subendothelial space, and the polymorphonuclear cells were the dominant infiltrate in the glomeruli. Up to the seventh day, immune deposits were seen in the subendothelial space, and the widening of this area was increasingly observed. Fourteen days later, immune deposits containing rat IgG were observed in the subepithelial area, but they were only occasionally seen in the subendothelial space and in the mesangial area. No crescent formation was seen at day 14, but the mesangial area was expanded, with an increased number of cells. The number of nuclei in the cross-section of a glomerulus increased after the induction of glomerulonephritis, but the number of leukocyte common antigen-positive cells (infiltrating cells) decreased gradually from day 4 to day 14. The staining of Thy-1.1, a marker of mesangial cell, was markedly enlarged in the glomerulus at day 14. These data suggest that mesangial proliferative glomerulonephritis can be induced by the antigen-antibody interaction on the surface of GENs. 相似文献
4.
This experiment was designed to use the graded dose-related amnesia produced by the benzodiazepine lorazepam (1.0, 2.0 mg/70 kg, oral) and the anticholinergic scopolamine (0.3, 0.6 mg/70 kg, subcutaneous) as a tool to explore the cognitive and neurochemical mechanisms underlying metamemory in the judgment of learning paradigm, with a placebo-controlled independent groups design in healthy volunteers (n=12/group). Results provide evidence for a pharmacological dissociation between effects on memory versus metamemory (relative accuracy of item-by-item monitoring) across a range of levels of memory performance and suggest that the drugs selectively impair those aspects of metamnemonic monitoring that require participants' awareness of their overall current state of functioning (absolute accuracy of prospective item-by-item monitoring, prospective global monitoring) but not those that rely solely on assessment of individual item characteristics (relative accuracy of item-by-item monitoring). (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
5.
Entrained double oxide films have been held responsible for reductions in mechanical properties in aluminum casting alloys.
However, their behavior in the liquid metal, once formed, has not been studied directly. It has been proposed that the atmosphere
entrapped in the double oxide film defect will continue to react with the liquid metal surrounding it, perhaps leading to
its elimination as a significant defect. A silicon-nitride rod with a hole in one end was plunged into liquid aluminum to
hold a known volume of air in contact with the liquid metal at a constant temperature. The change in the air volume with time
was recorded by real-time X-ray radiography to determine the reaction rates of the trapped atmosphere with the liquid aluminum,
creating a model for the behavior of an entrained double oxide film defect. The results from this experiment showed that first
oxygen, and then nitrogen, was consumed by the aluminum alloy, to form aluminum oxide and aluminum nitride, respectively.
The effect of adding different elements to the liquid aluminum and the effect of different hydrogen contents were also studied.
This article is based on a presentation made in the John Campbell Symposium on Shape Casting, held during the TMS Annual Meeting,
February 13–17, 2005, in San Francisco, CA. 相似文献
6.
The rôle of saponins in the undesirable sensory properties of the dried pea P sativum is reported. The sensory properties of isolated soyasaponin I are defined and described as bitter, astringent and metallic. The distribution of saponin in various air-classified pea flour fractions shows that the protein-rich fraction may contain sufficient saponin to cause undesirable tastes. 相似文献
7.
8.
9.
Schulz Laura E.; Bonawitz Elizabeth Baraff; Griffiths Thomas L. 《Canadian Metallurgical Quarterly》2007,43(5):1124
Causal learning requires integrating constraints provided by domain-specific theories with domain-general statistical learning. In order to investigate the interaction between these factors, the authors presented preschoolers with stories pitting their existing theories against statistical evidence. Each child heard 2 stories in which 2 candidate causes co-occurred with an effect. Evidence was presented in the form: AB→E; CA→E; AD→E; and so forth. In 1 story, all variables came from the same domain; in the other, the recurring candidate cause, A, came from a different domain (A was a psychological cause of a biological effect). After receiving this statistical evidence, children were asked to identify the cause of the effect on a new trial. Consistent with the predictions of a Bayesian model, all children were more likely to identify A as the cause within domains than across domains. Whereas 3.5-year-olds learned only from the within-domain evidence, 4- and 5-year-olds learned from the cross-domain evidence and were able to transfer their new expectations about psychosomatic causality to a novel task. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
10.
H King MC McCulloch JA Barrie E Kyriakides CV Beechey BM Cattanach IR Griffiths 《Canadian Metallurgical Quarterly》1997,26(8):557-566
Animals with spontaneous mutations affecting myelin formation have provided useful information about the genetic and cellular mechanisms regulating normal and abnormal myelination. In this paper we describe a novel murine mutation termed hindshaker (hsh), which is inherited in an autosomal recessive manner. Affected mice are characterised by a variable tremor of the hind end which commences at about 2 weeks of age and largely disappears in animals older than 6 weeks. There is hypomyelination affecting predominantly the spinal cord, although the optic nerves and brain are involved to a much lesser degree. The defect of thinly myelinated and naked axons is maximal at 20 days of age and largely resolves with time so that in the adult most axons are myelinated. The myelin structure appears normal and immunostains for the major proteins. Although the distribution of oligodendrocytes in the spinal cord is similar to normal during the period of hypomyelination, there are fewer mature cells. The hsh mutation appears to delay the maturation of oligodendrocytes, particularly in the spinal cord. Additionally, there is a considerable variation in phenotypic expression and in penetrance when the mutation is expressed on different genetic backgrounds, suggesting the hsh locus is subject to the influence of modifying gene(s). Identification of the hsh gene should identify a factor important in the development of oligodendrocytes, particularly those in the spinal cord. 相似文献