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1.
Separation tests using hollow-fibre modules were performed for the difficult selective extraction of trivalent actinides over fission lanthanides from acidic media. This article shows that with 2,6-di(5,6-dipropyl-1,2,4-triazin-3-yl)pyridine as the extractant, up to 94% americium could be extracted from 1.0 kmol/m3 HNO3, with minimal lanthanide co-extraction. Using a synergistic mixture of bis(chlorophenyl)dithiophosphinic acid and tri-n-octyl phosphine oxide, tests were performed on extraction, lanthanide scrubbing and stripping. In the extraction test, up to 99.99% americium could be extracted from 0.5 kmol/m3 HNO3, with approximately one third of the lanthanides being co-extracted. Mass transfer calculations using a consistent set of input data showed good agreement with the experiments. 相似文献
2.
3.
Pyrolysis experiments were performed in high vacuum and under reduced air pressure (100 Pa). The volatile products of pure cellulose and cellulose containing various amounts of flame retardant 2,2′-oxybis (5,5-dimethyl-1,3,2-dioxaphosphorinane-2,2′-disulfide), i.e., Sandoflam 5060 of Sandoz AG, were studied by means of gas chromatography in combination with mass spectroscopy. The volatile products were characterized with infrared spectroscopy. The studied revealed that the incorporation of the flame retardant enhanced the water release and shifted the onset of this reaction to lower temperature. On the basis of these findings an explanation for the mechanism of flame retardancy in generated cellulose fibers modified with this particular flame retardant is attempted. From experiments with different residual air pressure the influence of oxygen on the primary processes of the pyrolytic degradation of cellulose is being discussed. 相似文献
4.
The multi-homogeneous Bezout number is a bound for the number of solutions of a system of multi-homogeneous polynomial equations,
in a suitable product of projective spaces. Given an arbitrary, not necessarily multi-homogeneous, system, one can ask for
the optimal multi-homogenization that would minimize the Bezout number. In this paper it is proved that the problem of computing,
or even estimating, the optimal multi-homogeneous Bezout number is actually NP-hard. In terms of approximation theory for
combinatorial optimization, the problem of computing the best multi-homogeneous structure does not belong to APX, unless P
= NP. Moreover, polynomial-time algorithms for estimating the minimal multi-homogeneous Bezout number up to a fixed factor
cannot exist even in a randomized setting, unless BPP ⫆ NP. 相似文献
5.
Klaus Bauckhage 《化学,工程师,技术》1993,65(10):1200-1205
Utilisation of Different Components of Scattered Light for Particle Size Determination in Dispersed Systems . Light scattered by finely and coarsely dispersed particles can be used in variety of ways for characterization of sprays, emulsions, or suspensions. The characteristic of greatest interest is the particle size or the particle size distribution. While homogeneous, coarsely dispersed particles at sufficient dilutions and randomly distributed in a transparent continuous phase are generally amenable to particle size analysis, finely dispersed particles at higher concentrations or coarsely dispersed particles containing finely dispersed components are often difficult to measure. This article discusses ways of overcoming such difficulties on the basis of examples taken mainly from phase Doppler anemometry. 相似文献
6.
A method for the determination of carbon black fillers in peroxide vulcanizates or sulfur vulcanizates of natural rubber (NR, cis-1,4-polyisoprene) by metathesis degradation with 1-octene was developed using the catalyst WCl6? (C2H5)3Al2Cl3. The carbon black was separated from the reaction mixture by centrifuging and determined by weighing. In this connection, investigations were also performed with the catalyst WCl6? C2H5Al2Cl3 which was less suitable for filler determination. The rate of degradation of crosslinked NR with (E)-4-octene was measured. Metathesis reactions of 2-methyl-2-pentene (low-molecular-weight model compound of NR) with 7-tetradecene showed the importance of double bond shift for the degradation of NR. 相似文献
7.
Aus Betriebsergebnissen bei der Pfannenentschwefelung ist ein negativer Einfluß oxidierender Gasphasen bekannt. Daher war es das Ziel der eigenen Untersuchungen in einer geeigneten Apparatur die Wirkung oxidierender Bedingungen in der Gasphase sowohl auf den Verlauf des Schwefelabbaues in der Schlacke als auch des Schwefeltransportes aus dem Roheisen in die Schlacke zu untersuchen. Oxidierende Gasphasen erwirken bei der Pfannenentschwefelung an der Phasengrenze Schlacke/Gas eine Oxidation des Schwefels aus der Schlacke, ohne jedoch bei ruhender Schlackenschicht ein Oxidationspotential in der Schlacke aufzubauen, das bis zur Phasengrenze Roheisen/Schlacke durchgreift und dort die Entschwefelung des Roheisens durch die Siliciumgehalte stört. Sowohl die Entschwefelung des Roheisens als auch die Oxidation des Schwefels aus der Schlacke werden durch höhere Temperaturen und durch eine Rührwirkung gefördert. Der Schwefeltransport wird bei den ungerührten wie bei den gerührten Schmelzen durch Diffusionsvorgänge gesteuert und auch hier durch steigende Temperaturen und rührende Kräfte begünstigt. 相似文献
8.
9.
Prof. Dr.-Ing. Klaus Gersten 《Forschung im Ingenieurwesen》1992,58(5):113-118
Zusammenfassung Es wird ein allgemeines Widerstandsgesetz für Stufendiffusoren hergeleitet, bei dem die Widerstandszahl den Zusatzverlust
gegenüber den Verlusten der bis zum Kontursprung reichenden fiktiven Kanal- bzw. Rohrstr?mungen in der Zu- und Abstr?mung
beschreibt. Unter vereinfachenden Annahmen reduziert sich dieses Gesetz auf die bekannte Carnot-Formel. Insbesondere wird
dabei der Anteil des Zusatzverlustes, der vom Unterdruck an der Stufe und von der Wandschubspannungs?nderung unmittelbar hinter
der Stufe herrührt, vernachl?ssigt. Die Berücksichtigung dieses Anteils führt zu einem gegenüber der Carnot-Formel verbesserten
Widerstandsgesetz.
Herrn Prof. Dr.-Ing. Martin Fiebig zum 60. Geburtstag 相似文献
10.
Thomas Stieglitz Martin Schuettler Klaus Peter Koch 《IEEE engineering in medicine and biology magazine》2005,24(5):58-65
In the following article, the technologies to fabricate polyimide-based thin and flexible substrates with monolithically integrated electrode arrays and printed circuit boards (PCB) for hybrid electronic assemblies as well as an assembling technique that connects bare electronic dice with flexible PCBs are presented. The concept of modular, flexible biomedical microsystems as neural prostheses is introduced in general and described in detail in three examples. A cuff electrode with integrated multiplexer circuitry and standard implantable cables represents the combination of microtechnology with precision mechanics; a sieve electrode used as an implant in peripheral nerve regeneration studies demonstrates the next level of integration density but still uses a cable connection; and last, joint effort to fabricate the demonstrator of a vision prosthesis that is completely implantable in the eye with a wireless link for energy supply and data transmission is presented. System design, hybrid assembling technology, and flexible multilayer encapsulation using parylene and silicone rubber are the key components for creating a new generation of neural prostheses for complex and challenging new applications. 相似文献