Formation of Zr-contained Amorphous Alloy Films by Magnetron Co-sputtering

In order to explore the application of magnetron co-sputtering in fabricating the amorphous alloy, Zr-contained amorphous films were prepared by this technique and investigated by scanning electron microscope, energy disperse spectroscopy and X-ray diffraction. The results show that the co-sputtered films are in fully amorphous state or with amorphous-nanocrystalline structure. The XRD patterns of the Zr-Cu and Zr-Ni amorphous films exhibit a double-peak phenomenon. There is a shift of diffusive peak with changing the sputtering current which is possibly attributed to the change of Zr-Ni and Zr-Cu intermetallic like short range orders. In addition, Zr-Cu-Ni ternary co-sputtered films have a sharper peak at high angle. The sputtering yield of element during co-sputtering ranks as CuNiZr, which can be ascribed to the contribution of melting and boiling temperature, atomic size and electrical conductivity of elements.     

用萃取—火焰原子吸收光谱法测定金属钛中微量铜和镍

1 试剂所用全部试剂都是试剂纯的.水是重蒸馏水.用纯度为99.99%的Cu和Ni配制标准贮备液,酸度调至0.1M盐酸.用FeC1_3.6H_2O配制Fe(Ⅲ)溶液(Fe0.4mg/m1).所用全部溶剂均未进一步提纯.2 样品制备     

Engineering Geological Problems of Levee Along Middle and Lower Reaches of Yangtze River

1　ＩｎｔｒｏｄｕｃｔｉｏｎＢｅｃａｕｓｅｏｆｔｈｅｃｏｍｐｌｉｃａｔｅｄｓｕｂｓｏｉｌｐｒｏｆｉｌｅ ,ｔｈｅｌｅｖｅｅａｌｏｎｇｍｉｄｄｌｅａｎｄｌｏｗｅｒｒｅａｃｈｅｓｏｆＹａｎｇｔｚｅ ,ａｂｏｕｔ 36 0 0ｋｍｌｏｎｇ ,ｈａｓｍａｎｙｈｉｄｄｅｎｐｅｒｉｌｓ .Ａｍｏｎｇｔｈｅｄａｎｇｅｒｏｕｓｅｖｅｎｔｓｄｕｒｉｎｇ 1998’ｓｆｌｏｏｄｓｅａｓｏｎｉｎｔｈｅｗｈｏｌｅｖａｌｌｅｙ ,12 .7%ｏｃ ｃｕｒｒｅｄａｌｏｎｇｔｈｅｔｒｕｎｋｓｔｒｅａｍｄｙｋｅｓ,ｏｆｗｈｉｃｈ 6 98ｗｅｒｅｔｈｅｍｏｓｔｄ…     

Thermal Expansion Behavior of La1—xSrxMn1—yCoyO3—δ Perovskites

The thermal expansion behavior of La1-xSrxMn1-yCoyO3-δ (x=0.2-0.4, y=0.1-0.3) perovskites in air has been investigated. The average linear thermal expansion coefficients increased with increasing Sr content up to 40 mole fraction or Co content up to 30 mole fraction. The expansion is generally attributed to an increase in the average cation radius as some of the cations in the perovskite are reduced in valence when oxygen ions are removed from the structure.     

从奥林匹亚难处理砷黄铁矿精矿中提金的细菌氧化条件

本文着重研究了从奥林匹亚难处理砷黄铁矿精矿中提取金的细菌氧化条件，其中包括ｐＨ值，矿浆密度，滞留时间等因素的影响，试验选用的细菌为氧化铁硫杆菌。     

Measurement System of Uniformity between Breech Horizontal Platform and Datum Tube Axis of Rocket Artillery

The purpose of this development is to detect the parallelism between the breech horizontal platform and the datum tube axis of the rocket artillery. The located aiming mechanism at the muzzle and located adjustment mechanism at the breech are designed in the system. Besides those, the system also uses an autocollimator with accuracy of 1″ and a collimating mirror together to determine the axis of the datum tube. An electronic level with accuracy of 2″ is employed to measure and display the value of the included angle and the parameter of the inclined direction. The entire accuracy of this system is σ≤± 9.1″. This paper describes the composition and the operating principle of the system and analyzes the accuracy. The development of this system supplies reliable measurement method for new rocket artilleries and artilleries, and this technology is of a good application prospect.     

Enhancement Effect of Gold Nanoparticles on the Bioactivity of Hydrogen-producing Microbe

1 IntroductionGold nanoparticles have attracted considerable atten-tionin manyfields duetotheir some special properties al-though goldis very popularfor beingchemicallyinert[1-3].For example ,gold nanoparticles as amplificationtags havebeenthe subject of research directed at gene analysis[4]and antibody or antigen detection[5-7]due to the large di-electric constant ,ease of preparation,andits biocompati-bility[8].Nanoparticles in the range of 1-10 nmin diameterwould display electronic structur…