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排序方式: 共有1007条查询结果,搜索用时 31 毫秒
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Manika Chaudhary Milan Singh Ashwani Kumar Yogendra K. Gautam Anil K. Malik Yogesh Kumar Beer Pal Singh 《Ceramics International》2021,47(2):2094-2106
The current research work presents a facile and cost–effective co-precipitation method to prepare doped (Co & Fe) CuO and undoped CuO nanostructures without usage of any type of surfactant or capping agents. The structural analysis reveals monoclinic crystal structure of synthesized pure CuO and doped-CuO nanostructures. The effect of different morphologies on the performance of supercapacitors has been found in CV (cyclic voltammetry) and GCD (galvanic charge discharge) investigations. The specific capacitances have been obtained 156 (±5) Fg?1, 168(±5) Fg?1 and 186 (±5) Fg?1 for CuO, Co-doped CuO and Fe-doped CuO electrodes, respectively at scan rate of 5 mVs?1, while it is found to be 114 (±5) Fg?1, 136 (±5) Fg?1 and 170 (±5) Fg?1 for CuO, Co–CuO and Fe–CuO, respectively at 0.5 Ag-1 as calculated from the GCD. The super capacitive performance of the Fe–CuO nanorods is mainly attributed to the synergism that evolves between CuO and Fe metal ion. The Fe-doped CuO with its nanorods like morphology provides superior specific capacitance value and excellent cyclic stability among all studied nanostructured electrodes. Consequently, it motivates to the use of Fe-doped CuO nanostructures as electrode material in the next generation energy storage devices. 相似文献
3.
The crystallization process of hexagonal boron nitride in the presence of copper has been investigated. The positive effect of copper on the crystallinity of boron nitride was observed in the three studied systems of: nitrided boron, nitrided boron–carbon, and previously prepared turbostratic boron nitride. However, the presence of copper hindered the formation of boron carbonitride and produced graphite and boron nitride phases separately. Poor crystallinity was found as a conditio sine qua non for the existence of such a compound. Well-crystallized boron nitride had a very low spacing parameter 0.3328 nm and a regular hexagonal shape. 相似文献
4.
Apparent carbon aromaticities, fa, of some asphaltenes have been measured by n.m.r. in solution and compared with those obtained by the CP/MAS technique on solid samples. The aromaticities were also measured for several Alberta plains coals. From the 1H solution spectra and 13C solid nmr spectra of asphaltenes, some of their skeletal features, not obtainable from solution spectra only, have been suggested. 相似文献
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6.
A case of using the Semantic Interoperability Framework for custom orthopedic implants manufacturing
Milan Zdravković Miroslav Trajanović Miloš Stojković Dragan Mišić Nikola Vitković 《Annual Reviews in Control》2012,36(2):318-326
The efficiency and effectiveness of the daily practice in orthopedic surgery depend on the availability, interoperability and unique access to a wide set of information, related to the patient’s medical record and diagnosis, domain knowledge and available resources and staff. The most important of the tangible resources, needed for the therapeutic or preventive actions are orthopedic implants. In some cases, the implants may be highly complex and customized products, which need to be manufactured (assembled) on basis of the above information in a shortest possible timeframe. In this paper, the case of the custom orthopedic implants manufacturing is described from the perspective of the collaborative enterprising, with special consideration of the interoperability issues of the involved enterprise collaboration. It is shown how the previously developed Semantic Interoperability Framework can be used to improve the efficiency of the manufacturing and other relevant processes. 相似文献
7.
John P. Hilton ThaiHuu Nguyen Mihaela Barbu Renjun Pei Milan Stojanovic Qiao Lin 《Microfluidics and nanofluidics》2012,13(5):749-760
We present a bead-based approach to microfluidic polymerase chain reaction (PCR), enabling fluorescent detection and sample conditioning in a single microchamber. Bead-based PCR, while not extensively investigated in microchip format, has been used in a variety of bioanalytical applications in recent years. We leverage the ability of bead-based PCR to accumulate fluorescent labels following DNA amplification to explore a novel DNA detection scheme on a microchip. The microchip uses an integrated microheater and temperature sensor for rapid control of thermal cycling temperatures, while the sample is held in a microchamber fabricated from (poly)dimethylsiloxane and coated with Parylene. The effects of key bead-based PCR parameters, including annealing temperature and concentration of microbeads in the reaction mixture, are studied to achieve optimized device sensitivity and detection time. The device is capable of detecting a synthetically prepared section of the Bordetella pertussis genome in as few as 10 temperature cycles with times as short as 15?min. We then demonstrate the use of the procedure in an integrated device; capturing, amplifying, detecting, and purifying template DNA in a single microfluidic chamber. These results show that this method is an effective method of DNA detection which is easily integrated in a microfluidic device to perform additional steps such as sample pre-conditioning. 相似文献
8.
9.
The main aim of this work was to study the effects of particle size, particle volume fraction, and matrix strength on the
long fatigue crack growth resistance of two different grades of Al alloys (Al2124-T1 and Al6061-T1) reinforced with SiC particles.
Basically, it was found that an increase in particle volume fraction and particle size increases the fatigue crack growth
resistance at near threshold and Paris regimen, with matrix strength having a smaller effect. Near final failure, the stronger
and more brittle composites are affected more by static modes of failure as the applied maximum stress intensity factor (K
max) approaches mode I plane strain fracture toughness (K
IC). 相似文献
10.
E. Di Todaro C. T. O. F. Ruckert M. T. Milan W. W. Bose Filho J. R. Tarpani D. Spinelli 《Journal of Materials Engineering and Performance》2006,15(5):608-613
The main goal of this work was to evaluate the effectiveness of Walker’s equation in collapsing the fatigue crack propagation
data of a SAE AMS 7475-T7351 aluminum alloy loaded either longitudinally (L-T) or transversely (T-L) to the rolling direction.
T-L orientation testpieces presented lower ductility and fracture toughness values than L-T orientation. As a consequence,
during the fatigue crack propagation tests, T-L testpieces exhibited a stronger influence of monotonic modes of fracture,
resulting in higher Paris exponent values,m. Walker’s model was able to collapse fatigue crack propagation data of L-T test pieces at different applied stress ratios,R. However, for the T-L orientation, due to theR ratio dependency onm andC, simply averaging ofm values for the calculations of Walker’s exponent proved to be inefficient. A simple analytical procedure was proposed by
the authors to modify Walker’s model to take into account such effect. For T-L test pieces, when Walker’s model is modified
by considering both Paris’s exponent as well the coefficient as a function of theR ratio, the fatigue crack growth data collapses within a narrow band, thus allowing predictions to be made satisfactorily.
The collapsed band is even narrower if the empirical relationm=a+blogC is used instead of simple polynomial equations due to a better correlation coefficient. 相似文献