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1.
Mechanical properties of high density polyethylene (HDPE) extended to draw ratios in the 20–40 range have been determined and compared with corresponding properties of the polymers containing particulates including rutile, carbon black, iron oxide, and mica. Shrinkage of drawn structures was studied to temperatures near the fusion of the polymer host. The degree of interaction at polymer/additive interfaces was varied by surface coating certain of the solids with standard coupling agents. Solids were found to increase tensile moduli and to decrease shrinkage, particularly at higher exposure temperatures. The magnitude of changes due to the presence of solids was shown to depend on the apparent interaction at contacts between host and additive. In a dispersion–force matrix, like HDPE, benefits were optimized when the particulates were amphoteric or neutral, rather than having pronounced acid or base interaction potentials. 相似文献
2.
In a pot culture experiment, the effect of gypsum (50% of soil requirement), pyrites (equivalent to gypsum), farmyard manure (0.5 g per 100g soil) and Zn (10mg Zn kg–1 soil) on Zn equilibria in Ghabdan and Langrian series of sodic soils was studied. The equilibrium soil solutions collected anaerobically after 1, 14, 28, 42, 56, 70 and 84 days of submergence were analysed for pH, EC, HCO3 and Zn. Submergence markedly decreased soil solution pH and Zn up to 14 days and thereafter, the former slightly increased and the latter continued to decrease. Addition of amendments decreased soil solution pH in the order gypsum, pyrites and farmyard manure (FYM) and increased Zn concentration in the order FYM, gypsum and pyrites. The values of Zn potential (pZn + 2pOH) were within the range of pKsp for Zn(OH)2-Zn2+ (aq) from 16 to 84 days of submergence in Ghabdan soil and from 9 to 42 days of submergence in Langrian soil, where later it shifted to ZnCO3-Zn2+ (aq) system. Addition of FYM, pyrites and gypsum shortened the period of predominant existence of Zn(OH)2-Zn2+ (aq) system to 40, 30 and 12 days in Ghabdan soil and 30, 20 and 6 days in Langrian soil respectively. After these periods the system was saturated with respect to ZnCO3-Zn2+ (aq) except gypsum treatment where Zn-soil (unknown solid phases) -Zn2+ (aq) system controlled the solubility of Zn after 38 and 28 days of submergence of Ghabdan and Langrian soil respectively. 相似文献
3.
This paper presents a 3rd-order two-path continuous-time time-interleaved (CTTI) delta-sigma modulator which is implemented in standard 90 nm CMOS technology. The architecture uses a novel method to resolve the delayless feedback path issue arising from the sharing of integrators between paths. By exploiting the concept of the time-interleaving techniques and through the use time domain equations, a conventional single path 3rd-order discrete-time (DT) ΔΣ modulator is converted into a corresponding two-path discrete-time time-interleaved (DTTI) counterpart. The equivalent CTTI version derived from the DTTI ΔΣ modulator by determining the DT loop filters and converting them to the equivalent continuous-time loop filters through the use of the Impulse Invariant Transformation. Sharing the integrators between two paths of the reported modulator makes it robust to path mismatch effects compared to the typical time-interleaved modulators which have individual integrators in all paths. The modulator achieves a dynamic range of 12 bits with an OverSampling Ratio of 16 over a bandwidth of 10 MHz and dissipates only 28 mW of power from a 1.8-V supply. The clock frequency of the modulator is 320 MHz but integrators, quantizers and DACs operate at 160 MHz. 相似文献
4.
A new practical design approach for minimum-phase FIR or IIR filters, setting out from a high dimensionality FIR linear-phase prototype is described. The novelty of this technique lies in overcoming the inherent problem of finding the roots of a high order polynomial with repeated and/or very closely clustered roots 相似文献
5.
A power-efficient rail-to-rail CMOS analogue voltage buffer is presented. It consists of a complementary pair of super source followers, but a bulk-driven input device with the replica-biased scheme is utilised to eliminate the DC level shift, quasi-floating gate transistors to achieve class-AB performance, and a current switch which shifts between the complementary pair to allow rail-to-rail operation. The proposed buffer has been designed for a 0.35 mum CMOS technology to operate at a 1.8 V supply voltage. Simulated results are provided to demonstrate the total harmonic distortion for a 1.6 Vpp 100 kHz sine wave with a 68 pF load is as low as -46 dB, while the static current consumption remains under 8 muA. 相似文献
6.
G. M. Kale 《Metallurgical and Materials Transactions B》1998,29(1):31-38
Gibbs energy of formation of NiTiO3 (ilmenite) relative to its component oxides, NiO (rock salt) and TiO2 (rutile), has been measured employing the solid-state electrochemical cell,
. between 994 and 1371 K. The open-circuit electromotive force (emf) of the preceding solid-state galvanic cell was found
to be reversible and to vary linearly as a function of temperature in the range of measurement. The results obtained in this
study give for the reaction
. Combining the Gibbs energy of formation of NiTiO3 (ilm) from the component oxides with that for the formation of NiO (rs) from its elements gives for the reaction
. Differential thermal analysis (DTA) of NiTiO3 (ilm) between 373 and 1623 K indicated that NiTiO3 (ilm) undergoes a reversible order-disorder phase transformation between 1540 and 1594 K. Based on the ideal mixing of cations
on the cationic sublattice of NiTiO3 (ilm) and a critical phase transformation of 1568 K obtained from the DTA, the Gibbs energy change for the order-disorder
phase transformation in NiTiO3 (ilm) is obtained as
. 相似文献
7.
Mechanical and thermal properties of wood fibers reinforced poly(lactic acid)/thermoplasticized starch composites 下载免费PDF全文
Thermoplasticized starch (TPS) filled poly(lactic acid) (PLA) blends are usually found to have low mechanical properties due to poor properties of TPS and inadequate adhesion between the TPS and PLA. The purpose of this study was to investigate the reinforcing effect of wood fibers (WF) on the mechanical properties of TPS/PLA blends. In order to improve the compatibility of wood with TPS/PLA blends, maleic anhydride grafted PLA (MA‐g‐PLA) copolymer was synthesized and used. TPS, TPS/PLA blends, and WF reinforced TPS/PLA composites were prepared by twin‐screw extrusion and injection molded. Scanning electron microscope and crystallinity studies indicated thermoplasticity in starch. WF at two different weight proportions, that is, 20% and 40% with respect to TPS content were taken and MA‐g‐PLA at 10% to the total weight was chosen to study the effect on mechanical properties. At 20% WF and 10% MA‐g‐PLA, the tensile strength exhibited 86% improvement and flexural strength exhibited about 106% improvement over TPS/PLA blends. Increasing WF content to 40% further enhanced tensile strength by 128% and flexural strength by 180% with respect to TPS/PLA blends. Thermal behavior of blends and composites was analyzed using dynamic mechanical analysis and thermogravimetric analysis. © 2017 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2018 , 135, 46118. 相似文献
8.
SiO2 thin films are in high demand for wide range of applications including microelectronics, optoelectronics, solar energy conversion, photocatalysis, and self-cleaning coatings. The performance of thin film is strongly influenced by surface properties like surface roughness, thickness, morphology, wetting behavior, and thermal stability. In these applications, the SiO2 sols were prepared using tetraethylorthosilicate as a source of SiO2 and deposited on 100?×?40?×?2?mm3 glass slide using dip-coating method for 2?min and calcined at 250?°C for 30?min. The SiO2 thin films were obtained using DTAB, SDS, and Tween 20 (Tw 20) surfactants with the thickness of 36.92, 47.15, and 52.39?nm, respectively. Surface morphology was studied with AFM and surface roughness was depicted with 0.9528, 3.6534, and 0.9294?nm. Contact angle measurements have been performed with goniometer to evaluate the wetting behavior of the film. The contact angle of 58.01°, 48.40°, and 37.88° was observed with SDS, DTAB, and Tw 20 film, respectively. The SiO2 thin films with SDS showed more surface roughness and water repelling ability when compared to DTAB and least with Tw 20. 相似文献
9.
Experiments have been carried out with jet mixers to study the solid suspension characteristics. The jet velocities required for solid suspension in 0.5 and 1 m ID tanks were measured experimentally. The nozzle diameter was varied from 0.0156 to 0.05 m. The nozzle clearance from the tank bottom was varied from 0.1 to 0.9 m. Tap water and sand of average sizes 100, 300, and 500 µm were used. The solid loading was varied from 1 to 5% (wt.). The effect of nozzle angle was also studied. A semi‐empirical model has been developed to predict the jet velocity needed to achieve a certain degree of suspension. 相似文献
10.
Phillip Masimba Toperesu Girish M. Kale Jafar Daji David E. Parkinson Simon Parkinson 《International Journal of Applied Ceramic Technology》2022,19(2):1160-1170
The corrosion behavior of a tin IV oxide-doped AZS-refractory, subject to static and dynamic corrosion testing at 1370˚C in soda-lime-silica glass, was studied considering the effect of the microstructural features on corrosion. The refractory was synthesized by slip cast methods through reaction sintering of alumina and zircon raw materials using SnO2 as a sintering agent. SnO2 had a considerable influence in the enhanced alumina/zircon reaction sintering and the subsequently evolved microstructures of an interlocked Zr(1-x)Sn(x)O2 solid solution reinforced alumina-mullite composite. The process kinetics of the refractory corrosion followed reasonably well the predicted dependence on the square root of angular velocity under forced convection corrosion. Glass chemical corrosion and erosion of the refractory, under static and dynamic glass conditions, respectively, revealed the Zr(1-x)Sn(x)O2 solid solution-rich mullite matrix as providing the most corrosion resistance and glass compatibility. 相似文献