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1.
The three-dimensional morphology of polyethylene single crystals grown from dilute solution has been examined by atomic force microscopy. Single crystals were deposited on a soft ground of aqueous solution of poly(vinyl alcohol) (PVA) to avoid the collapse of thin lamellar crystals with thickness of 10 nm. The observation of single crystals on dried PVA clarifies the morphology of a chair type crystal as well as well-known hollow pyramidal type. It has been confirmed that the screw dislocations in the chair type follow a selection rule of the handedness in a manner to relieve the distortion in the chair type. 相似文献
2.
Takeshi Kondo Hiroyuki Ito Kazuhide Kusakabe Kazuhiro Ohkawa Kensuke Honda Yasuaki Einaga Akira Fujishima Takeshi Kawai 《Diamond and Related Materials》2008,17(1):48-54
The effect of CF4 plasma etching on diamond surfaces, with respect to treatment time, was investigated using scanning electron microscopy (SEM), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), and electrochemical measurements. SEM observations and Raman spectra indicated an increase in surface roughening on a scale of 10–20 nm, and an increase in crystal defect density was apparent with treatment time in the range of 10 s to 30 min. In contrast, alteration of the diamond surface terminations from oxygen to fluorine was found to be rather rapid, with saturation of the F/C atomic ratio estimated from XPS analysis after treatment durations of 1 min and more. The redox kinetics of Fe(CN)63−/4− was also found to be significantly modified after 10 s of CF4 plasma treatment. This behavior shows that C–F terminations predominantly affect the redox kinetics compared to the effect on the surface roughness and crystal defects. The double-layer capacitance (Cdl) of the electrolyte/CF4 plasma-treated boron-doped diamond interface was found to show a minimum value at 1 min of treatment. These results indicate that a short-duration CF4 plasma treatment is effective for the fabrication of fluorine-terminated diamond surfaces without undesirable surface damage. 相似文献
3.
The lateral crystal habits ofn-alkanes (n-C
n
H2n+2) have been observed just below the melting points by optical microscopy forn=18, 19, 20, 22, 24, 34, 44, 50 and 65. The shape of the crystals depends on the crystal phase: circular in the rotator phase,
lenticular in phase C, and diamond in the low-temperature phase. The rounding of the lateral shape can be explained in terms
of thermal roughening of the lateral faces in the disordered phases at high temperature. 相似文献
4.
Yoshiyuki Uno Akira Okada Kensuke Uemura Purwadi Raharjo Toshihiko Furukawa Kosaku Karato 《Precision Engineering》2005,29(4):171-455
A new finishing process for metal molds by large-area electron beam (EB) irradiation is proposed in this study. In the large-area EB irradiation equipment used here, an EB with high-energy density is irradiated without focusing the beam, and so the EB with a maximum diameter of 60 mm can be used for melting or evaporating metal surface instantly. Experimental results show that the surface roughness decreases from 6 μmRz to less than 1 μmRz in just a few minutes under proper machining conditions. The corrosion resistance of metal mold surface also could be greatly improved by large-area EB irradiation. Furthermore, the surface roughness of tilting surface close to 90° could be well improved. Therefore, large-area EB irradiation method has a possibility to become a high-efficiency finishing process for metal molds. 相似文献
5.
We first demonstrate an integrated-optic device for a fibre laser Doppler velocimeter, which consists of a waveguide interferometer and a frequency shifter in z-propagation Ti-diffused LiNbO3. The device is also pigtailed with a single-mode fibre to pick up a Doppler-shifted signal. Using the fabricated device, the velocity of a moving object was successfully heterodyne-detected with a signal/noise ratio of 30dB. 相似文献
6.
T Kimura I Haruta Y Isobe E Ueno J Toda Y Nemoto K Ishikawa Y Miyazono K Shimizu K Yamauchi N Hayashi 《Canadian Metallurgical Quarterly》1997,92(5):883-886
We present a patient with continuous melena, diagnosed as rectal varices bleeding. She had a history of esophageal varices, which was treated by endoscopic ligation therapy. Eight years after the treatment of esophageal varices, the continuous melena began. Colonoscopic examination showed that the melena was caused by rectal varices, which were so severe that they could not be treated by either endoscopic sclerotherapy or surgical devascularization. Taking into considering the overall risk of treating rectal varices, we chose the approach of double balloon-occluded embolotherapy (DBOE) with 5% ethanolamine oleate with iopamodol as a liquid embolic material. DBOE is one of the interventional radiology techniques (Morita et al., Acta Hepatol Jpn 1994;35:109-120), but in this case was a completely new and novel clinical procedure for rectal varices. After the DBOE therapy, the condition of rectal varices was markedly improved. Thus, DBOE might be a new tool for treating inoperable rectal varices. 相似文献
7.
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9.
H. Toda Y. Mochizuki T. Kawanishi H. Kawashima 《Nutrient Cycling in Agroecosystems》2002,63(2-3):167-173
In a coastal agricultural area in the central part of Japan (Shizuoka), we found decreasing nitrate concentration with depth in a shallow groundwater, where the depth to water table varied between 0.6 and 1.2 m below ground surface. High nitrate concentrations (5–29 mg N L–1) were often observed in the upper layer (0–2 m) of the groundwater, but the concentration decreased to less than 1 mg N L–1 in the deeper layer. Ammonium was scarcely detected, and the concentration of dissolved oxygen was usually low (< 1 mgO2 L–1) in the groundwater. Nitrate in the groundwater often had very heavy nitrogen stable isotope ratios (>20{}). There was a negative relationship between nitrogen stable isotope ratio of nitrate and its concentration. When nitrate was injected into the groundwater with acetylene and bromide (a conservative tracer), nitrate concentration decreased to 20% of the initial level within 5 days, accompanied by the increase in nitrite and nitrous oxide concentration and a little change in bromide concentration. These results indicate that microbial denitrification plays a potential role in the decrease of nitrate in shallow groundwater at the study site. 相似文献
10.
The structure of internal oxide layers in decarburized sheet was studied using a newly developed electrochemical method. Dissolving
potential profiles indicated the amount of fayalite (Fe2SiO4) and silica (SiO2) in the layers. The quantitative data for the contents of fayalite and silica in the internal oxide layers can be easily
obtained by this method. 相似文献