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1.
Graft copolymers of sodium alginate (NaAlg) with N‐vinyl‐2‐pyrrolidone were prepared using azobisisobutyronitrile as initiator. The graft copolymers (NaAlg‐g‐PVP) were characterized with Fourier transform infrared spectroscopy, elemental analysis, and differential scanning calorimetry. Polymeric hydrogel beads of NaAlg and NaAlg‐g‐PVP were prepared by crosslinking method using glutaraldehyde (GA) as a crosslinker in the hydrochloric acid catalyst (HCl) and these beads were used to deliver anti‐inflammatory drug, indomethacin (IM). Chemical stability of the IM after encapsulation into beads was confirmed by FTIR. Preparation conditions of the NaAlg‐g‐PVP beads were optimized by considering the percentage entrapment efficiency, particle size, swelling capacity and their release data. In vitro release studies were performed in simulated gastric fluid (pH 1.2) for the initial 2 h, followed by simulated intestinal fluid (pH 7.4) for 4 h. Effects of GA concentration, exposure time to GA, drug/polymer (d/p) ratio, and concentration of HCl on the release of IM were discussed. It was observed that IM release from the beads decreased with increasing GA concentration and exposure time. IM release also decreases with increasing d/p ratio and HCl concentration. The highest IM release was obtained to be 77% for beads crosslinked with 0.027M GA. Swelling experiments were also performed to compute molecular mass between crosslinks of the beads. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
2.
Bilal Demirel Nihat B. İnaner Derya U. Gezer Fugen Daver Ali Yaras Fatih Akkurt 《Polymer Engineering and Science》2021,61(7):2043-2054
Polyethylene terephthalate (PET)/nano-hydroxyapatite (nHAp) composite granules were obtained using twin-screw extruder. Preforms were prepared by injection molding and then PET/nHAp bottles were produced by blow molding. For PET bottles with nHAp, the migration amounts of carboxylic acid (COOH), acetaldehyde (AA), diethylene glycol (DEG), and isophthalic acid (IPA); glass transition temperature (Tg); melting temperature (Tm); and the maximum crystallization temperature (Tcry) were measured. The load-carrying capacity, burst strength, stress cracking, and regional material distribution tests were carried out on the bottles. X-ray diffraction, scanning electron microscopy, Fourier transform infrared spectroscopy, differential scanning calorimetry, and ultraviolet transmittance analyses were conducted to explain the changes in mechanical, chemical, physical properties, and light transmission of bottles. It was found out that the COOH amount increased and the AA content decreased with increasing nHAp amount. On the other hand, no change was observed in the amounts of DEG and IPA. Although the mechanical properties such as load-carrying capacity and burst strength of the bottles have improved, it has been determined that the standard environmental stress crack resistance test procedure cannot be applied to such a composite. Experimental findings indicate that nHAp disrupts the chemical structure of PET and it isolates harmful chemicals such as AA by forming intermolecular bonds. Moreover, with the addition of up to 0.8% nHAp, PET bottles block the light transmission approximately 80% within 400–700 nm wave length zone. The study demonstrates that the PET/nHAp composite bottles can be used in the food industry, particularly in the packaging of milk and milk products which are vulnerable to light exposure. 相似文献
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Assignment of referees to football games is an important problem faced in professional football leagues. Despite its importance, the problem has received limited academic attention. This paper presents a model and analysis of the problem for fair referee assignments, and develops a constructive heuristic and a local search procedure for its solution. Results from an extensive computational study show that the methods are effective in solving the problem in a second of computation time and yielding an excellent solution quality. 相似文献
5.
A new image segmentation system is presented to automatically segment and label brain magnetic resonance (MR) images to show normal and abnormal brain tissues using self-organizing maps (SOM) and knowledge-based expert systems. Elements of a feature vector are formed by image intensities, first-order features, texture features extracted from gray-level co-occurrence matrix and multiscale features. This feature vector is used as an input to the SOM. SOM is used to over segment images and a knowledge-based expert system is used to join and label the segments. Spatial distributions of segments extracted from the SOM are also considered as well as gray level properties. Segments are labeled as background, skull, white matter, gray matter, cerebrospinal fluid (CSF) and suspicious regions. 相似文献
6.
Can an electronic portfolio that is both a multimedia container for student work and a tool to support key learning processes have a positive impact on the literacy practices and self-regulated learning skills of students? This article presents the findings of a yearlong study conducted in three Canadian provinces during the 2007–2008 school year initially involving 32 teachers and 388 students. Due to varying levels of implementation our final data set included 14 teachers and 296 students. Using a non-equivalent pre-test/post-test design, we found that grade 4–6 students who were in classrooms where the teacher provided regular and appropriate use of the electronic portfolio tool ePEARL (i.e., medium–high implementation condition, n = 7 classrooms and 121 students), compared to control students (n = 7 classrooms and 175 students) who did not use ePEARL, showed significant improvements (p < .05) in their writing skills on a standardized literacy measure (i.e., the constructed response subtest of the Canadian Achievement Test-4th ed.) and certain metacognitive skills measured via student self-report. The results of this study indicate that teaching with ePEARL has positive impacts on students’ literacy and self-regulated learning skills when the tool is used regularly and integrated into classroom instruction. 相似文献
7.
İbrahim Büyükyazıcı 《Computers & Mathematics with Applications》2010,59(1):274-282
In this paper, we investigate convergence and approximation properties of a Chlodowsky type generalization of Stancu polynomials (we called Stancu–Chlodowsky polynomials).The rates of convergence of this generalization are obtained by means of modulus of continuity and by using the -functional of Peetre. We also present and prove theorems on weighted approximation and the order of approximation of continuous functions by these operators on all positive semi-axis. 相似文献
8.
?smail Dinçer 《Advances in Engineering Software》2011,42(4):160-171
Determination of deformation modulus and coefficient of subgrade reaction of soils have major importance, whether the projects are in design, and construction or compaction assessment stage of earth filling structures. Plate load test is one of the frequently used method to directly determine the parameters but the method is both costly and time consuming. For this reason, this paper is concerned with the applications of artificial neural networks (ANN) and simple-multiple regression analysis to predict deformation modulus and coefficient of subgrade reaction of compacted soils from compaction parameters (such as maximum dry density (MDD) and optimum moisture content (OMC), field dry density (FDD), and field moisture content (FMC)). Regression analysis and artificial neural network estimation indicated that there are acceptable correlations between deformation modulus and coefficient of subgrade reaction and these parameters. Artificial neural networks model exhibits higher performance than traditional statistical model for predicting deformation modulus and coefficient of subgrade reaction. 相似文献
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Mustafa Turan Ferhat Gunay Adil Aslan 《Journal of Intelligent and Robotic Systems》2012,65(1-4):73-91
Unmanned Aircraft (UA) have become an integral part of the present-day joint air operations. UA have potential to be employed across the full spectrum of Air Force functions. On the other hand, UA technology could be a subject of an asymmetric use by state actors in high or low density conflict, and/or by non-state actors in many ways including terrorism, drug smuggling, and limited attack with unconventional payloads i.e. biological or chemical agents. Therefore countering the threat associated with the hostile UA use could be necessary in the future. First part of the research revealed that UA can be a threat in the future. In the second part of the research, the SWOT (Strengths-Weaknesses-Opportunities-Threats) analysis supplemented with the Tree analysis (SWOT+Tree) provided a broader look for investigating the factors related to hostile UA use analytically. In literature, there is little information about the concepts for CUAOPS. The final goal of the paper is to find possible solutions and means for a better understanding of the nature of CUAOPS. 相似文献