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排序方式: 共有790条查询结果,搜索用时 15 毫秒
1.
Antonio Sanchez‐Solis Andres Garcia‐Rejon Mirna Estrada Antonio Martinez‐Richa Guadalupe Sanchez Octavio Manero 《Polymer International》2005,54(12):1669-1672
The production and properties of blends of poly(ethylene terephthalate) (PET) and poly(ethylene naphthalene 2,6‐dicarboxylate) (PEN) with three modified clays are reported. Octadecylammonium chloride and maleic anhydride (MAH) are used to modify the surface of the montmorillonite–Na+ clay particles (clay–Na+) to produce clay–C18 and clay–MAH, respectively, before they are mixed with the PET/PEN system. The transesterification degree, hydrophobicity and the effect of the clays on the mechanical, rheological and thermal properties are analysed. The PET–PEN/clay–C18 system does not show any improvements in the mechanical properties, which is attributed to poor exfoliation. On the other hand, in the PET–PEN/clay–MAH blends, the modified clay restricts crystallization of the matrix, as evidenced in the low value of the crystallization enthalpy. The process‐induced PET–PEN transesterification reaction is affected by the clay particles. Clay–C18 induces the largest proportion of naphthalate–ethylene–terephthalate (NET) blocks, as opposed to clay–Na+ which renders the lowest proportion. The clay readily incorporates in the bulk polymer, but receding contact‐angle measurements reveal a small influence of the particles on the surface properties of the sample. The clay–Na+ blend shows a predominant solid‐like behaviour, as evidenced by the magnitude of the storage modulus in the low‐frequency range, which reflects a high entanglement density and a substantial degree of polymer–particle interactions. Copyright © 2005 Society of Chemical Industry 相似文献
2.
M. Delgado-Pinar J. Mora A. Diez J.L. Cruz M.V. Andres 《Photonics Technology Letters, IEEE》2005,17(3):552-554
We report a wavelength-switchable fiber ring laser that includes a Bragg grating-based acoustooptic superlattice modulator. Wavelength switching of the laser emission is achieved by controlling the peak reflectivity of the different reflection bands that appear on both sides of the Bragg wavelength when a longitudinal acoustic wave propagates along the grating. 相似文献
3.
Stakeholder involvement is essential to the development of a total maximum daily load (TMDL) and its implementation plan. A tool, beyond a simulation model, is needed to support the decision making process that requires negotiation and compromise among stakeholders. The decision support system (DSS) described herein has a TMDL module to calculate various combinations of point and nonpoint loads that can meet the water quality criteria. Its Consensus module allows stakeholders to formulate, evaluate, modify, and vote for alternatives. The DSS displays bar charts for pollution loads from various subwatersheds and attributes the nonpoint loads to land uses. The water quality consequence of the pollution loads is output in maps, which shows sections meeting criteria in green and those not in red. The DSS requires a front end effort of site specific adaptation and model calibration. An Internet-based stakeholder process was developed to allow more concerned citizens to participate in management decisions. 相似文献
4.
G Charach PD Rabinovich FM Konikoff I Grosskopf MS Weintraub T Gilat 《Canadian Metallurgical Quarterly》1998,29(3-4):125-136
In most patients with atherosclerosis, the underlying metabolic derangement remains undefined. Animal experiments have suggested that the ability to produce and excrete large amounts of bile acids may be an adaptation mechanism to cholesterol overload protecting against the atherogenic effects of cholesterol. However, there are very few data on bile acid excretion in human atherosclerosis. In the present study, we have investigated fecal bile acid secretion in subjects with and without coronary artery disease. The target group consisted of 30 patients with proven coronary artery disease and the control group consisted of 27 matched subjects without clinical or laboratory evidence of coronary atherosclerosis. Fecal bile acids were measured by gas-liquid chromatography from 24-hr stool collections under a controlled diet. The patients excreted significantly less bile acids than the controls (325+/-135 vs. 592+/-223 mg/day, respectively, p < 0.0001). The difference was primarily due to a reduced excretion of secondary bile acids. Less than 50% of deoxycholate was excreted by patients (180+/-81 mg/day) as compared to controls (367+/-168 mg/day, p < 0.0002), while lithocholic acid excretion was 111+/-62 mg/day in patients vs. 190 +/-70 mg/day in controls (p < 0.005). The fecal output of the two primary bile acids, cholic and chenodeoxycholic acid, did not differ significantly between patients and controls. The fecal output of total bile acids correlated with that of both secondary bile acids in patients as well as in controls. These findings suggest that patients with coronary heart disease are unable to excrete adequate amounts of bile acids to rid themselves of excess cholesterol, even if they are able to maintain a plasma cholesterol level comparable to that of healthy controls. 相似文献
5.
An experimental study of the effects produced by different parameters of the heat-quenching cycle permitted the optimization of the properties typical of these martensitic stainless steels: hardness and corrosion resistance. The results obtained demonstrate that the heating temperatures currently used in industrial quenching treatment of these steels should be modified. 相似文献
6.
7.
A simple and accurate analysis of a single-mode optical fibre interferometric displacement detection technique is resented. This analysis is in good agreement with experimental measurements, and shows that angular alignment between the fibre and the sensor is the most critical parameter. 相似文献
8.
9.
Mait Lang Tiit Nilson Andres Kuusk Andres Kiviste Maris Hordo 《Remote sensing of environment》2007,110(4):445-457
Several published foliage mass and crown radius regression models were tested on the preparation of the input for the reflectance model of Kuusk and Nilson [Kuusk, A. and Nilson, T. (2000), A directional multispectral forest reflectance model. Remote Sensing of Environment, 72(2):244–252.] for 246 forest growth sample plots in Estonia. In each test, foliage mass and crown radius for trees in the sample plots were predicted with a particular pair of allometric regression models. The forest reflectance model was then run using the estimated foliage mass and crown radius values. Reflectance factors were simulated and compared with the reflectance values obtained from three atmospherically corrected Landsat 7 Enhanced Thematic Mapper (ETM+) scenes. The statistics of linear regression between the simulated and measured reflectance factors were used to assess the performance of foliage and crown radius models. The hypothesis was that the best allometric regression models should provide the best fit in reflectance. The strongest correlation between the simulated and measured reflectance factors was found in the short-wave infrared band (ETM + 5) for all the images. The highest R2 = 0.71 was observed in Picea abies dominated stands. No excellent combination of foliage mass and crown radius functions was found, but the ranking based on determination coefficients showed that some linear crown radius models are not applicable to our data. Processing of raster images, reflectance measurement for small sample plots, usage of tree-species-specific fixed parameters (specific leaf area, etc.), and the ignored influence of phenology introduced additional variation into the relationships between simulated and measured reflectance factors. Further studies are needed, but these preliminary results demonstrate that the proposed method could serve as an effective way of testing the performance of foliage mass and canopy cover regressions. 相似文献
10.
Nowadays, cities are the most relevant type of human settlement and their population has been endlessly growing for decades. At the same time, we are witnessing an explosion of digital data that capture many different aspects and details of city life. This allows detecting human mobility patterns in urban areas with more detail than ever before. In this context, based on the fusion of mobility data from different and heterogeneous sources, such as public transport, transport‐network connectivity and Online Social Networks, this study puts forward a novel approach to uncover the actual land use of a city. Unlike previous solutions, our work avoids a time‐invariant approach and it considers the temporal factor based on the assumption that urban areas are not used by citizens all the time in the same manner. We have tested our solution in two different cities showing high accuracy rates. 相似文献