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K2NiF4-type CaLnCoO4 (Ln = Sm and Gd) has been synthesized at 1173 or 1223 K in air using citric acid (CA) and ethylene glycol (EG). CaLnCoO4 (Ln = Sm and Gd) has an orthorhombic structure with the space group Bmab. The average particle sizes are approximately 300 nm for CaSmCoO4 and approximately 170 nm for CaGdCoO4, respectively. The global instability index (GII) indicates that the crystal structure of CaGdCoO4 is more stable than that of CaSmCoO4. CaLnCoO4 (Ln = Sm and Gd) is a p-type semiconductor and shows paramagnetic behavior above 5 K. The 1/χ-T curve of CaSmCoO4 deviates from the Curie-Weiss law, whereas the 1/χ-T curve of CaGdCoO4 follows the Curie-Weiss law in the temperature range of 5 ≤ T ≤ 300 K. From the values of the observed effective magnetic moment (μeff) of CaLnCoO4 (Ln = Sm and Gd), it is considered that the spin state of the Co3+ ion is low. 相似文献
3.
Monodispersed ellipsoidal hematite particles were synthesized and coated with silicone using a silane-coupling agent, phenyltriethoxysilane.
The thickness of the silicone shell was controlled by the concentration of phenyltriethoxysilane and the presence of n-hexadecyltrimethylammonium chloride, which was thought to modify the surface properties of the hematite particles to be organophilic.
The hematite/silicone core-shell particles were strongly hydrophobic and had a good dispersibility and stability in toluene.
Hollow ellipsoidal silicone particles were obtained by the dissolution of hematite with hydrochloric acid from the core-shell
particles. 相似文献
4.
Hideki Taguchi Katsuyuki Nakade Masashi Yosinaga Masaki Kato Ken Hirota 《Journal of the American Ceramic Society》2008,91(1):308-310
X-ray photoelectron spectroscopy was performed to elucidate the catalytic activity of CH4 oxidation on perovskite-type Ca(Mn1− x Ti x )O3−δ synthesized at 1173 K in a flow of oxygen from a gel with citric acid and ethylene glycol. The Mn ion content decreases and the ratio of the Mn3+ ion in the Mn ion increases with increases in x . Ca(Mn1− x Ti x )O3−δ has a high catalytic activity of CH4 oxidation at x =0.4. These results indicate that the catalytic activity strongly depends on the Mn3+ ion content of the surface. 相似文献
5.
In a conveyor system for mass production as in the Ford system, each station processes just one item in one cycle time, where the cycle time is the time-interval between two successive outputs. In a Just-In-Time production system, a single-unit production and conveyance system is applied to a part production line without conveyors, and multi-function workers and a U-shaped layout of machines have been introduced. The multi-function worker takes charge of multiple machines. In this paper, we consider a U-shaped line with multiple multi-function workers, each of which is responsible for several machines. We formulate it into a marked Petri net, which has a convex property of a generalized semi-Markov process. This shows that the cycle times of two different systems are comparable in the sense of an increasing convex order. We also show the reversibility of the system, that is, the expected cycle time of the reversed system where each worker operates items and walks in the reversed order of stations is the same as that of the original system. 相似文献
6.
E Hamada T Nakajima S Ota A Terano M Omata S Nakade K Mikoshiba Y Kurachi 《Canadian Metallurgical Quarterly》1993,102(4):667-692
The effects of acetylcholine (ACh) and histamine (His) on the membrane potential and current were examined in JR-1 cells, a mucin-producing epithelial cell line derived from human gastric signet ring cell carcinoma. The tight-seal, whole cell clamp technique was used. The resting membrane potential, the input resistance, and the capacitance of the cells were approximately -12 mV, 1.4 G ohms, and 50 pF, respectively. Under the voltage-clamp condition, no voltage-dependent currents were evoked. ACh or His added to the bathing solution hyperpolarized the membrane by activating a time- and voltage-independent K+ current. The ACh-induced hyperpolarization and K+ current persisted, while the His response desensitized quickly (< 1 min). These effects of ACh and His were mediated predominantly by m3-muscarinic and H1-His receptors, respectively. The K+ current induced by ACh and His was inhibited by charybdotoxin, suggesting that it is a Ca(2+)-activated K+ channel current (IK.Ca). The measurement of intracellular Ca2+ ([Ca2+]i) using Indo-1 revealed that both agents increased [Ca2+]i with similar time courses as they increased IK.Ca. When EGTA in the pipette solution was increased from 0.15 to 10 mM, the induction of IK.Ca by ACh and His was abolished. Thus, both ACh and His activate IK.Ca by increasing [Ca2+]i in JR-1 cells. In the Ca(2+)-free bathing solution (0.15 mM EGTA in the pipette), ACh evoked IK.Ca transiently. Addition of Ca2+ (1.8 mM) to the bath immediately restored the sustained IK.Ca. These results suggest that the ACh response is due to at least two different mechanisms; i.e., the Ca2+ release-related initial transient activation and the Ca2+ influx-related sustained activation of IK.Ca. Probably because of desensitization, the Ca2+ influx-related component of the His response could not be identified. Intracellularly applied inositol 1,4,5-trisphosphate (IP3), with and without inositol 1,3,4,5-tetrakisphosphate (IP4), mimicked the ACh response. IP4 alone did not affect the membrane current. Under the steady effect of IP3 or IP3 plus IP4, neither ACh nor His further evoked IK.Ca. Intracellular application of heparin or of the monoclonal antibody against the IP3 receptor, mAb18A10, inhibited the ACh and His responses in a concentration-dependent fashion. Neomycin, a phospholipase C (PLC) inhibitor, also inhibited the agonist-induced response in a concentration-dependent fashion. Although neither pertussis toxin (PTX) nor N-ethylmaleimide affected the ACh or His activation of IK,Ca, GDP beta S attenuated and GTP gamma S enhanced the agonist response.(ABSTRACT TRUNCATED AT 400 WORDS) 相似文献
7.
Quantitative detection system for maize sample containing combined-trait genetically modified maize 总被引:4,自引:0,他引:4
Akiyama H Watanabe T Wakabayashi K Nakade S Yasui S Sakata K Chiba R Spiegelhalter F Hino A Maitani T 《Analytical chemistry》2005,77(22):7421-7428
Various countries have established regulations that stipulate the labeling of agricultural commodities, feed, and food products that contain or are made from genetically modified (GM) material or that contain adventitious GM material in amounts that exceed certain threshold levels. While regulations in some countries refer to GM material on a weight per weight (w/w) percentage, the currently applied detection methods do not directly measure the w/w percentage of the GM material. Depending on the particular method and the sample matrix it is applied to, the conversion of analytical results to a w/w percentage is challenging or not possible. The first rapid PCR system for GM maize detection on a single kernel basis has been developed. The equipment for the grinding of individual kernels and a silica membrane-based 96-well DNA extraction kit were both significantly revised and optimized for this particular purpose, respectively. We developed a multiplex real-time PCR method for the rapid quantification of GM DNA sequences in the obtained DNA solutions. In addition, a multiplex qualitative PCR detection method allows for the simultaneous detection of different GM maize traits in each kernel and thereby for identification of individual kernels that contain a combination of two or more GM traits. Especially for grain samples that potentially contain combined-trait GM maize kernels, the proposed methods can deliver informative results in a rapid, precise, and reliable manner. 相似文献
8.
9.
Kenichi Ide Masahiko Nakade Tohru Takahashi Takenori Nakajima 《Electrical Engineering in Japan》2012,178(1):1-10
Much of oil‐filled (OF) cable has been used for a long time as 66‐ to 500‐kV extrahigh‐voltage cable. Sometimes we can see extremely degraded tan δ oil (several tens of percent of tan δ, for example) in joint boxes, etc. The values of tan δ calculated by a simple combination model of paper/oil show that the oil‐impregnated paper with such a high tan δ oil likewise has an extremely high tan δ, which must result in thermal breakdown. However, such an event has not taken place up to the present in actually operated transmission lines. This fact suggests that some mechanism for the suppression of tan δ has acted in the paper insulation impregnated with degraded tan δ oil. Therefore, we investigated in detail the tan δ characteristics of paper impregnated with extremely high tan δ oil. In addition, based on the investigation results, we developed a method for simulation of heat generation by dielectric loss in an OF cable joint (which has degraded tan δ oil). © 2011 Wiley Periodicals, Inc. Electr Eng Jpn, 178(1): 1–10, 2012; Published online in Wiley Online Library ( wileyonlinelibrary.com ). DOI 10.1002/eej.21184 相似文献
10.
Apurv Dash Jürgen Malzbender Robert Vaßen Olivier Guillon Jesus Gonzalez-Julian 《Journal of the American Ceramic Society》2020,103(12):7072-7081
The compressive creep of silicon carbide fiber reinforced Ti3SiC2 MAX phase with both fine and coarse microstructure was investigated in the temperature range of 1000-1300°C. Comparison of only steady-state creep was done to understand the response of fabricated composite materials toward creep deformation. It was demonstrated that the fibers are more effective in reducing the creep rates for the coarse microstructure by an increase in activation energy compared to the variant with a finer microstructure, being partly a result of the enhanced creep rates for the microstructure with larger grain size. Grain boundary sliding along with fiber fracture appears to be the main creep mechanism for most of the tested temperature range. However, there are indications for a changed creep mechanism for the fine microstructure for the lowest testing temperature. Local pores are formed to accommodate differences in strain related to creeping matrix and predominantly elastically deformed fibers during creep. Microstructural analysis was done on the material before and after creep to understand the deformation mechanics. 相似文献