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D. C. Peets R. Liang C. Stock W. J. L. Buyers Z. Tun L. Taillefer R. J. Birgeneau D. A. Bonn W. N. Hardy 《Journal of Superconductivity and Novel Magnetism》2002,15(6):531-534
We have grown cubic centimeter-size crystals of YBa2Cu3O x suitable for neutron studies, by a top-seeded melt-growth technique. Growth conditions were optimized with an eye toward maximizing phase purity. It was found that the addition of 2% Y2BaCuO5 and 0.5% Pt (by mass) were required to prevent melt loss and to obtain the highest crystallinity. A neutron diffraction study on a mosaic of six such crystals found that the final Y2BaCuO5 concentration was 5%, while other impurity phases comprised less than 1% by volume. The oxygen content was set to x = 6.5, the crystals were detwinned, and then carefully annealed to give the well-ordered ortho-II phase. The neutron study determined that 70% of the mosaic's volume was in the majority orthorhomic domain. The neutron (006) and (110) rocking curve widths were ~1° per crystal and ~2.2° for the mosaic, and the oxygen chain correlation lengths were >100 Å in the a- and b-directions and ~50 Å in the c-direction. 相似文献
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The latest developments and in particular important synthetic aspects for the preparation of modern poly(styrene‐divinylbenzene) (PS‐DVB) based liquid chromatography (LC) supports are reviewed. In this context, the chemistry of particular porous and nonporous, functionalized, monolithic, coated silica and more specialized mixed organic PS‐DVB media is covered. Special consideration is given to modern approaches such as micro‐(μ)‐HPLC and coating techniques and their most important applications. Synthetic particularities relevant to the corresponding applications are outlined. 相似文献
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Ferdinand P. Ferragu O. Lechien J.L. Lescop B. Magne S. Marty V. Rougeault S. Kotrotsios G. Neuman V. Depeursinge Y. Michel J.B. Van Uffelen M. Varelas D. Berthou H. Pierre G. Renouf C. Jarret B. Verbandt Y. Stevens W. Voet M.R.H. Toscano D. 《Lightwave Technology, Journal of》1995,13(7):1303-1313
Recent developments of stability control in mines, essentially based on Ge-doped fiber Bragg gratings (FBG) are reported including results about the different aspects of the system: accurate characterizations of FBG, sensor network topology and multiplexing method, user interface design and sensor packaging 相似文献
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G. L. Chen C. Guyon Z. X. Zhang B. Da Silva P. Da Costa S. Ognier D. Bonn M. Tatoulian 《Microfluidics and nanofluidics》2014,16(1-2):141-148
In this paper, tricobalt tetraoxide (Co3O4) catalyst was coated on the polydimethylsiloxane microchannel by the plasma-enhanced metal-organic chemical vapor deposition technology. The obtained Co3O4 film was characterized by SEM, XRD, XPS, and TEM, and the results show that the as-deposited Co3O4 film was initially composed of many cauliflowers-shaped microclusters. Also, the microcauliflower was transformed from an amorphous phase to a crystal phase when the Co3O4 film was treated by Ar and O2 plasma for more than 20 min, and the crystal lattice line occurred on the surface of nano-sized-Co3O4 particles. Meanwhile, the interface of Co3O4 particles with diameter between 3 and 12 nm became obvious and some nano-catkin structures were also formed on the Co3O4 film. The ratio of Co3+/Co2+ in the spinel-type Co3O4 was nearly 2, and the nano-particles predominantly expose their {311}, {111}, and {220} planes. These morphologies and structure characteristics were found to be ideal for increasing the catalytic activity efficiency of Co3O4 for CO oxidation, and the catalytic stability of Co3O4 coated on the organic microreactor lasted nearly 85 h for trace CO oxidation at room temperature. 相似文献
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Integrating products and services to customized solutions can help firms to differentiate from their competitors. In practice, however, various companies fall short in extracting value from their customers. Therefore this paper focuses on pricing aspects as central means for value appropriation in the context of solutions. Following the resource-based view of the firm, we adopt a process-oriented perspective on pricing practices in order to identify crucial factors and activities. Based on 15 in-depth interviews with practitioners from various industries we derive six steps of a price management process for value appropriation in the context of solution selling and present critical activities and routines within each step. 相似文献
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Ferdinand Verhulst 《Journal of Engineering Mathematics》2005,53(3-4):349-358
Stable normal-mode vibrations in engineering can be undesirable and one of the possibilities for quenching these is by embedding
the oscillator in an autoparametric system by coupling to a damped oscillator. There exists the possibility of destabilizing
the undesirable vibrations by a suitable tuning and choice of nonlinear coupling parameters. An additional feature is that,
to make the quenching effective in the case of relaxation oscillations, one also has to deform the slow manifold by choosing
appropriate coupling; this is illustrated for Rayleigh and van der Pol relaxation. 相似文献