DNNSA反胶团萃取净化电镀废水中镍的动力学

采用恒界面池研究了二壬基萘磺酸－煤油体系萃取废水中镍离子的动力学。考察了搅拌转速,界面积,DNNSA 浓度,镍离子浓度,温度对萃取速率的影响。实验结果表明：溶液中镍离子的萃取速率在200 rpm时出现与搅拌强度无关的化学反应动力学“坪区”,此时镍离子萃取速率与两相接触面积成正比,说明萃取过程为界面化学反应控制过程。在动力学“坪区”,镍离子萃取速率正比于萃取剂浓度,而与水相中的镍离子浓度无关,且随着温度升高,萃取速率增加,萃取活化能为31.56 kJ•mol-1。得到了DNNSA萃取废水中镍离子的萃取动力学方程并对萃取机理进行了探讨。     

An orthogonal analysis method for decoupling the nozzle geometrical parameters of microthrusters

This paper proposes an orthogonal analysis method for decoupling the multiple nozzle geometrical parameters of microthrusters, thus an reconfigured design can be implemented to generate a proper thrust. In this method, the effects of various nozzle geometrical parameters, including throat width W _t , half convergence angle θ _in , half divergence angle θ _out , exit-to-throat section ratio W _e /W _t and throat radius of the curvature R _t /W _t , on the performance of microthrusters are sorted by range analysis. Analysis results show that throat width seriously affects thrust because range value of 67.53 mN is extremely larger than the range value of other geometry parameters. For average specific impulse (ASI), the range value of exit-to-throat section ratio W _e /W _t and half divergence angle θ _out are 4.82 s and 3.72 s, respectively. Half convergence angle with the range value of 0.39 s and throat radius with 0.32 s have less influence on ASI compared with exit-to-throat section ratio and half divergence angle. When increasing the half convergence angle from 10° to 40° and throat radius of the curvature from 3 to 9, average specific impulse initially decreases and then increases. A MEMS solid propellant thruster (MSPT) with the reconfigured geometrical parameters of nozzle is fabricated to verify the feasibility of the proposed method. The thrust of the microthruster can reach 25 mN. Power is estimated to be 0.84 W. This work provides design guideline to reasonably configure geometry parameters of microthruster.     

A quantitative optimisation model for a horizontal MEMS solid propellant thruster with experimental verification

This paper studies the effect of multiple geometric parameters of a micronozzle on a MEMS solid propellant thruster (MSPT) and establishes a quantitative optimisation model. Influences of the structural parameters of the micronozzle on performance are accurately calculated. The significance and contribution ratio of each parameter are evaluated by F distribution. Correspondingly, a horizontal MSPT is fabricated and tested to prove the optimisation model. In the implementation, a complete microigniter is formed by a single layer of Au, achieving an ultra-low ignition voltage of 2.1 V with an extremely low ignition resistance of 4 Ω.     

基于Σ-Δ调制技术的微加速度计系统研究

论述了Σ-Δ调制器的基本原理,将Σ-Δ调制技术应用于微加速度计系统,设计了一种新型的微加速度计,建立了系统模型。并对系统的频率特性进行了分析,表明基于该技术的微加速度计系统在工作频段内噪声能够得到有效的消除,且具有近似的线性相位。     

Fabrication of ZnS/C microsphere composites with enhanced electromagnetic wave absorption properties

Journal of Materials Science: Materials in Electronics - For electromagnetic wave-absorbing materials, organic-derived carbon materials and metal sulfides are highly preferred. In this paper, ZnS/C...     

Effects of garlic oil on milk fatty acid profile and lipogenesis‐related gene expression in mammary gland of dairy goats

BACKGROUND: Garlic oil (GO) has blood lipid‐lowering effects. Milk fatty acid (FA) originates partly from plasma, and can be affected by the mammary lipogenesis. This study aimed to investigate GO effects on milk FA profile and mammary lipogenesis‐related gene expression. Early‐lactation goats were randomly allocated to four treatments with six goats each, and offered corn silage ad libitum and fixed amount of 0.79 kg day^?1 dry matter (DM) concentrate mixed with GO (0, 0.57, 1.14, 1.71 g kg^?1 DM) for 30 days consisting of 26‐day adaptation. RESULTS: Intake of corn silage reduced (P≤0.05) as GO level increased in the concentrate. Lipase activity and lactose content linearly increased, while non‐esterified FA concentration quadratically decreased with increasing GO level (P≤0.05). The proportions of short‐ and medium‐chain (C14:0, C15:0 and C16:0) and saturated FA decreased, whereas C18, cis9 trans11 conjugated linoleic acid (c9t11 CLA), t10c12 CLA, monounsaturated and polyunsaturated FA, and some ≥ C20 FA proportions increased in a linear manner with increasing GO level (P≤0.05). The mRNA abundance of genes remained unchanged (P > 0.1) as GO level increased. CONCLUSION: Garlic oil altered milk FA profile and these effects may not be related to the mammary lipogenesis‐related genes expression. © 2012 Society of Chemical Industry     

用于CARS激发源的全光纤窄线宽皮秒脉冲种子源的研究

进行了窄线宽、低重复频率和无色散管理的全光纤皮秒脉冲种子源的研究。数值仿真分析了腔内脉冲的演化过程,研究了腔长和光纤光栅带宽对脉冲稳定性和脉冲宽度的影响。搭建实验系统,对腔长和抽运功率的影响进行了实验研究,在腔长为24.1 m时,成功产生86 ps的稳定光脉冲,其线宽为0.04 nm,重复频率为4.3 MHz。当将此脉冲放大用于相干反射托克斯拉曼散射(CARS)光谱探测,理论光谱分辨率可达0.3 cm-1。     

煤泥型煤燃烧特性的实验研究

以5种煤泥型煤为原料进行燃烧实验,研究煤泥型煤的燃烧特性及影响因素.结果表明,成型过程及黏结剂等对煤泥的燃烧性能基本无影响;煤泥型煤燃烧初期主要为挥发分的析出和燃烧,火焰旺盛火力强;型煤中后期燃烧为焦炭的燃烧,燃烧由型煤表面不断深入内部进行,氧气要扩散到焦炭表面会受到灰壳及其内部产生的挥发分和燃烧产物等扩散阻力.型煤挥发分越高,灰分越低,其燃烧速率越大,且易于燃尽.     

喷涂技术在烟草薄片生产中的应用研究

分析了烟草薄片原生产涂布系统的不足,对原涂布系统进行改造,新增涂布装置,将柠檬酸钾单独施加到烟草薄片上,研究了新喷涂技术对涂布液和烟草薄片质量的影响。结果表明,应用新喷涂技术时,涂布液的黏度降低了17.78%、含渣量降低了24.52%,涂布液渗透性提高;在未影响产品物理指标、化学指标、感官质量的基础上,烟草薄片中钾离子横幅分布均匀性提升了68.49%。     

车门玻璃下位振动传递路径建模及优化分析

阐述了传递路径分析(transfer path analysis,简称TPA)方法的基本理论,对某车型左前车门玻璃下位关门过程中玻璃振动异常进行了传递路径分析,并针对该车门结构设计特点,提出了基于传递路径分析方法的二级TPA分析模型,分别为锁机、密封条-玻璃一级传递路径模型和导轨接附点-玻璃二级传递路径模型.通过常用关...