羰基镍粉末生产中羰基镍测定的发展状况与应用

阐述了国内外羰基镍测定的各种方法以及在工业与环境保护等领域的应用状。     

Interactive key frame selection model

Video summarization can provide a fine representation of the content of video stream and reduce a large amount of data involved in video indexing, browsing, and retrieval. Moreover, Key frame selection is an important step in the research of content-based video analysis and retrieval. Although there exist a variety of methods for key frame selection, they are heuristic and closed systems, which cannot dynamically generate video summary with user’s preference. In this paper, an M-estimator and epipolar line distance constraint camera motion estimation algorithm is introduced as camera parameters is an important motion feature for key frame selection, and Broyden-Fletcher-Goldfarb-Shanno (BFGS) method is applied to optimize estimated parameters. Moreover, since Interactive Computing is a novel-computing model that represents the transition of algorithm to interaction, an interactive model of key frame selection (IKFS) is presented as a result of improving the model of key frame selection (KFS). The model of KFS and IKFS are proved to satisfy the criterion of induction and coinduction, respectively. Experimental results show that the processing scheme generates flexible and desirable summarizations whose distortion rate is lower than current method. Above all, IKFS is an extension to KFS.     

核电三级设计计划编制分析

核电作为安全、稳定、高效的清洁能源,在世界范围内近年来呈现出快速发展的趋势。目前国家全力以赴推进三代核电建设,因为设计是建设的龙头,因此制定一个科学的、详尽的、切实可行的三级设计计划,对核电站的设计、乃至整个建设工作非常重要和必要。对采购、施工、调试均有举足轻重的影响。     

Preparation and characterization of PEGDE crosslinked silk fibroin film

To obtain water-insoluble silk fibroin(SF) materials, polyethylene glycol diglycidyl ether(PEG-DE) was selected as a crosslinking agent to prepare SF films(blends). The reaction conditions were optimized for the crosslinking of the SF molecules. The hot water stability of the blends was measured using BCA protein assay and gravimetric analysis. The molecular conformation and crystalline structure of the blends were analyzed by FTIR and XRD, respectively. When the mass ratio of SF:PEG-DE was 1.0:0.8, the hot water loss rate of the SF blends was minimized. PEG-DE could induce SF molecules to form β-sheets during the gel reaction process, resulting in improved crystallinity and hot water dissolved resistance of the blend films. In order to demonstrate the cytotoxicity of the chemical reagents used to crosslink SF, L929 cells were seeded on the blend film(SF:PEG-DE = 1:1) and cultured for 3 days. Cells of L929 readily adhered and spread in the fusiform on the blend film resulting in high cell viability. The extracted liquid from the SF porous film did not inhibit cell proliferation, as estimated by the MTT assay.     

Effect of pre-annealing on thermal stability of amorphous Zr-Cu-Ni alloy

The influence of pre-annealing on thermal stability of the amorphous Zr70Cu20Ni10 alloy was reported by em-ploying the differential scanning calorimetry (DSC) and high-resolution transmission electron microscopy (HRTEM) tech-niques. It has been observed that the supercooled liquid region decreases with increasing the annealing time under isothe-mal conditions, indicating that the thermal stability of the amorphous Zr70Cu20Ni10 alloy decreases gradually. HRTEM ob-servations reveal that there exist some ordered atomic clusters in the amorphous matrix at the relaxation stage. These or-dered atomic clusters can be regarded as precursors for the precipitation of the crystalline phases in the subsequent crystal-lization process. The reasons resulting in the decrease in thermal stability of the amorphous Zr70Cu20Ni10 alloy with anneal-ing time are discussed through the Gaussian decomposition for the radial distribution function of the amorphous Zr70Cu20Ni10 alloy.     

二维土壤水中溶质运移问题的全离散混合元法研究

本文建立了二维非粘性土壤水中溶质运移问题的混合元格式,讨论了混合元解的存在唯一性,并分析了误差估计.最后给出数值算例,数值模拟结果表明,用该方法模拟溶质运移问题是合理有效的.     

半焦成型技术及型焦应用研究进展

半焦孔隙结构发达,具有良好的吸附能力,但由于机械强度较低及耐热和耐水性能较差等原因,半焦的大规模应用受到了极大限制,不仅造成半焦资源大量浪费,也导致严重的环境污染问题。成型半焦机械强度高,耐热和耐水性能得到显著改善,可以广泛用作吸附剂或催化剂载体,具有很好的经济价值。综述半焦成型的主要工艺,阐明半焦成型机理,介绍有黏结剂冷压成型、无黏结剂冷压成型和热压成型等半焦成型工艺的特点以及产品型焦的主要应用领域,并提出半焦成型技术和型焦应用的主要发展方向。     

宜春单站短时强降水统计和分析

通过使用宜春2005～2012年3～9月的单站气象要素资料,对40个短时强降水个例进行逐5min数据的统计和分析,提出了10min降水量≥10mm的"超短时强降水"概念;了解到≥10mm/10min的超短时强降水不仅在历年的短时强降水中出现频率最高,同时常伴随出现在≥30mm/h和≥50mm/2h的短时强降水中;当短时强降水发生时,会出现气压上升、温度下降、湿度上升、雨量骤大和前导风加大等显著变化;宜春单站短时强降水呈现逐年增多态势,易发时间集中于每年4～8月和每日04:00～05:00和14:00～20:00。     

共晶Ga—In合金的液态结构与粘度研究

利用液态金属X射线衍射仪测试了室温下Ga-24.6%In共晶合金的强度曲线、结构因子、双体分布函数以及原子间最近邻距离。结果表明,液态共晶Ga-In合金结构因子的第一峰呈明显的不对称。表明熔体中仍保留有部分Ga的共价键。,建立了共晶Ga-In合金的结构模型。利用此模型计算所得结果与用Gauss分解所得结果吻合良好;利用回转振动粘度仪进行了粘度测量。结果表明,共晶Ga-In合金的粘度值在100－600℃范围内满足指数关系,表明熔体中没有发生结构转变。并给出了其粘度与温度的关系式。     

水流含沙量对磨蚀的影响

在前人进行的基础上，分析了含沙量对磨损和气蚀的影响，提出了由湍流猝发现象而引起的扫荡磨损的概念，认为含沙量的增加将增加小角度微切削破坏作用和扫荡磨损，降低单颗粒泥沙的破坏作用，含沙量小时促进气蚀，而含沙量大时则制约气蚀，提出了临界含沙量SCr有可能不存在的情况，解释了文献[1],[2]的结论。