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1.
2.
Ivan Fortelný Monika Lapčíková František Lednický Zdeněk Starý Zdeněk Kruliš 《Polymer Engineering and Science》2008,48(3):564-571
This article is focused on the phase structure development in immiscible polymer blends during melt mixing. Nonuniformity of the phase structure, i.e., the coexistence of areas containing particles with markedly different size distribution, was detected in quenched and compression molded samples of a number of various blends prepared by long and intensive mixing in the chamber of a Plasticorder. The same effect was found also for polystyrene/polyamide blends prepared in a twin‐screw extruder. It was shown that neglecting nonuniformity of the phase structure can lead to considerable error in evaluation of the effect of system parameters on the blend morphology. The reasons for the effect were discussed and it was found that inhomogeneous flow field in mixers is a plausible explanation of the nonuniform phase structure. POLYM. ENG. SCI., 2008. © 2008 Society of Plastics Engineers 相似文献
3.
ZnO-based varistor samples were prepared by the direct mixing of the constituent phases (DMCP) and sintering at 1100 °C for 2 h. The influence of the starting powder mixture's composition – the amounts of the pre-reacted varistor compounds and their composition – and its preparation, either with or without mechano-chemical activation (MCA), on the microstructure, phase composition and electrical characteristics of the varistor samples was studied. It showed that MCA improved the density and microstructural homogeneity of the varistor samples. MCA strongly affected the grain growth: it enhanced the nucleation of inversion boundaries (IBs) in the ZnO grains and the IBs-induced grain-growth mechanism resulted in uniform grain growth and hence a microstructure with smaller ZnO grains and a narrower grain size distribution. The final phase composition of the samples prepared by the DMCP method mainly depended on the presence of varistor dopants that can prevent the formation of the pyrochlore phase, especially Cr2O3, while MCA can affect it mostly by providing a homogeneous distribution of those dopants. The DMCP varistor samples prepared with MCA had much better current–voltage characteristics than the samples of the same composition prepared from unactivated powders. 相似文献
4.
Iv?n Arce of Core Security Technologies looks at the current state of malware and introduces the articles he selected for this special issue. 相似文献
5.
Ivan Hrivňák 《International Journal of Pressure Vessels and Piping》1985,20(3):223-237
This paper deals with the metallurgical changes which occur during heat treatment of welded joints. Stress relieving heat treatment in the temperature range below A1, the normalizing heat treatment and the heat treatment in the intercritical range A1–A3, are all considered. The thermal regime of welding is described. The practice of intercover of the weldment before applying PWHT to ambient temperature is described. It is stressed that the aim of stress-relieving heat treatment is not only to relax internal stresses but also to improve the microstructure and impact properties of HAZ and weld metal, to improve dimensional stability and increase resistance against stress corrosion. Examples are given of the effect of annealing in the intercritical range A1–A3 on the improvement in toughness of electroslag welded joints. Changes in dislocation distribution and density, precipitation processes and grain sizes during PWHT are described. 相似文献
6.
Ivan Cimrák 《Archives of Computational Methods in Engineering》2007,15(3):277-309
The Landau-Lifshitz (LL)equation of micromagnetism governs rich variety of the evolution of magnetization patterns in ferromagnetic
media. This is due to the complexity of physical quantities appearing in the LL equation. This complexity causes also an interesting
mathematical properties of the LL equation: nonlocal character for some quantities,nonconvex side-constraints, strongly nonlinear
terms. These effects influence also the numerical approximations. In this work, recent developments on the approximation of
weak solutions, together with the overview of well-known methods for strong solutions,are addressed.
Author is supported by the Fund for Scientific Research - Flanders FWO (Belgium). 相似文献
7.
Fish oils containing different levels of polymers of triacylglycerols formed during autoxidation were incubated with pancreatic
lipase to establish whether these polymers are substrates for lipase hydrolysis. With oils containing low amounts (less than
4%) of triacylglycerol polymers as substrates, both triacylglycerols and polymers of triacylglycerols were almost completely
hydrolyzed, and fatty acid monomers and monoacylglycerols were the major lipid products. Under the same incubation conditions,
some triacylglycerols remained intact when highly oxidized oils containing 20 or 30% triacylglycerol polymers were the substrate.
The fatty acid composition of these residual triacylglycerols was almost identical to that of triacylglycerols present at
the start of the assay. When fish oil containing 30% triacylglycerol polymers was incubated with the lipase, the component
triacylglycerols and polymers of triacylglycerols were hydrolyzed at similar rates, and fatty acid dimers were detected as
a product. It is concluded that the high molecular weight polymers of triacylglycerols present in oxidized fish oils can be
hydrolyzed by pancreatic lipasein vitro. 相似文献
8.
The polyesterification and isomerization reaction of 1,6-hexane diol and maleic anydride in a melt without catalyst was studied by 13C and 1H n.m.r. spectroscopy. The structure and concentration of oligoester species during the polyesterification and isomerization were determined depending on the reaction temperature and time. According to the number and configuration of repeating units determined from 1H n.m.r. spectra kinetics of both reactions were also considered. The degree of isomerization is continuously increasing in the investigated reaction range. 相似文献
9.
A model employing the correction factors of Marek and Standart, but using a concentration-dependent liquid phase association factor of Jenkins—Robinson, has been used to model vapour—liquid equilibrium data for mixtures of acetic acid with benzene, toluene, o-xylene and p-xylene. With the aim to use systems of acetic acid—benzene and acetic acid—toluene as the test mixtures for distillation columns, the examination of the systems of acetic acid—aromatic hydrocarbons was undertaken. The model promises to be useful in modelling isobaric and isothermal data of acetic acid—benzine, acetic acid—toluene, acetic acid-p-xylene and acetic acid-o-xylene systems. Deviation plots show that the isothermal and isobaric data are represented well. 相似文献
10.
With the help of DTA, DTG elementary analysis of carbonized residues and ESR spectroscopy the influence of anionic form on thermooxidation of trimethylammoniumhydroxyprophyl (TMAHP)–cellulose was studied. At 300°C the percentage of carbon in carbonized residue thermolyzed in oxidative atmosphere is higher than for the sample degraded in inert atmosphere. The percentage of hydrogen decreases simultaneously. The concentration of free radicals in thermolyzed residue also increases due to the presence of oxygen. We propose that oxygen is abstracting the hydrogen atoms from polysaccharide and unpaired electrons on carbon atoms are produced. At 400°C the percentage of carbon in residues prepared at inert atmosphere is higher than for residue formed at oxidative atmosphere. Also the concentration of free radicals in thermolyzed residues obtained in inert atmosphere is greater than for those from oxidative ones. That is why suppose that at this temperature oxygen is bonded to polysaccharide residue and free radicals are terminated. From the semiquantitative DTA we can make the following sequence of samples according to their increasing thermooxidative effect: unmodified cellulose < A–HSO < A–Br? < A–I? < A–NO < A–H2PO < A–CH3COO? < A–HCO < A–F? < A–Cl?1 < A–OHp?. 相似文献