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1.
2.
Three-dimensional (3D) YBO3:Tb3+ flower-like and dense flower-like hierarchitecture constituted of nanoflakes are solvothermally synthesized in the presence of polyborate precursors in the mixture of ethanol and water. The growth process of the YBO3:Tb3+ flowers and dense flowers was explored based on the time-dependent experiment and the results showed that the growth mechanism follows an in situ growth rather than self-assembly process as reported previously. YBO3:Tb3+ morphologies composed of nanoflakes are achieved by controlling the concentration of ethanol and dependence of photoluminescence on morphology was studied. Remarkable photoluminescence enhancement was observed for YBO3:Tb3+ with flower-like morphology demonstrating the potential of the microstructure in future applications as a green phosphor. Such a synthetic method and growth mechanism may be applied to fabricate complex 3D architectures of other materials. 相似文献
3.
A crack-tip screening analysis of cleavage fracture of steel is developed. The analysis incorporates evidence that reinitiation
of an arrested cleavage crack requires less stress intensity than cleavage initiation from a fatigue precrack. Fractographic
evidence as well as metallographic sectioning of arrested cracks have previously shown that the mechanism of rapid crack propagation
by cleavage is affected strongly by partial crack-plane deflection which leaves unbroken ligaments in its wake. The tearing
of these ligaments by dimple rupture is the dominant energy-absorbing mechanism. Earlier etch-pit experiments using an Fe-Si
alloy showed that the crack-tip stress intensity based on plastic zone size is extremely low. These observations are incorporated
into a model in which cleavage crack reinitiation is analyzed using a sharp crack that is shielded by a distribution of pinching
forces along its faces. During reloading of the arrested crack, the ligaments restrict crack-tip blunting, leading to higher
local stresses. As a result, lower stress intensities are needed for reinitiation than for initiation from a fatigue precrack. 相似文献
4.
5.
Satisfaction of twin objectives of maximization of Mn along with minimization of PDI do not necessarily guarantee the maximization of concentration of desired species in a semibatch epoxy polymerization process. As the final product consists of a number of polymer species, a need is felt to perform an advanced optimization study to come up with such process conditions for which the selective growth of a particular polymer species is maximized in minimum possible processing time and the population of other species should be at their lowest values. These above-mentioned conflicting objectives frame the platform for a multi-objective optimization problem, which is solved here using a real-coded non-dominated sorting genetic algorithm or NSGA II and Pareto optimal solutions are obtained. The decision variables are discrete addition rates of various ingredients, e.g. the amount of addition of bisphenol-A (a monomer), sodium hydroxide and epichlorohydrin at different time steps. All species balance equations, bounds on Mn, PDI and addition amounts are treated as constraints. Results are very promising in terms of optimized operations for selective enhancement of desired polymer species for the epoxy polymerization process. Total additions are kept very close to available experimental conditions to minimize probable extrapolation errors. It has been observed that preferential oligomer production is extremely difficult for epoxy polymerization. Lower chain polymers are the only choice for a good quality, stable polymer product. 相似文献
6.
7.
JA Moshier E Malecka-Panas H Geng J Dosescu J Tureaud M Skunca AP Majumdar 《Canadian Metallurgical Quarterly》1995,55(22):5358-5365
Ornithine decarboxylase (ODC) has been shown to be oncogenic in transfected NIH/3T3 cells overexpressing the enzyme from a heterologous promoter. These cells, designated as NODC-2 cells, acquire proliferative properties associated with tumorigenic transformation such as loss of contact inhibition, decreased population doubling time, anchorage-independent growth, and tumor production in nude mice. At least one of these parameters, loss of contact inhibition, remains dependent on elevated ODC levels. We have used these cells to investigate the molecular mechanisms by which ODC overexpression drives cell transformation and to examine the involvement of other proto-oncogene products in this process. An interaction between ODC overexpression and the epidermal growth factor receptor (EGF-R) was suggested initially by the elevation of both basal (300%) and ligand-induced (457%) EGF-R tyrosine kinase activities in NODC-2 cells compared to similarly treated control NLK cells. Disruption of EGF-R mediated signal transduction in NODC-2 cells both by treatment with tyrphostin-25 or by transfection with a vector expressing a dominant negative EGF-R mutant resulted in reacquisition of contact-inhibited growth and suppression of anchorage-independent, clonogenic growth in soft agar. We conclude that ODC-induced transformation of NIH/3T3 cells is mediated, at least partly, by alterations in EGF-R signal transduction activity. 相似文献
8.
When a circuit is tested using random or pseudorandom patterns, it is essential to determine the amount of time (test length) required to test it adequately. We present a methodology for predicting different statistics of random pattern test length. While earlier methods allowed estimation only of upper bounds of test length and only for exhaustive fault coverage, the technique presented here is capable of providing estimates of all statistics of interest (including expected value and variance) for all coverage specifications.Our methodology is based on sampling models developed for fault coverage estimation [1]. Test length is viewed as awaiting time on fault coverage. Based on this relation we derive the distribution of test length as a function of fault coverage. Methods of approximating expected value and variance of test length are presented. Accuracy of these approximations can be controlled by the user. A practical technique for predicting expected test length is developed. This technique is based on clustering faults into equal detectability subsets. A simple and effective algorithm for fault clustering is also presented. The sampling model is applied to each cluster independently and the results are then aggregated to yield test lengths for the whole circuit. Results of experiments with several circuits (both ISCAS '85 benchmarks and other practical circuits) are also provided.This work was done while the author was with the Department of Electrical Engineering, Southern Illinois University, Carbondale, IL 62901. 相似文献
9.
A high power, mid-infrared (/spl lambda/=3.8 /spl mu/m) lead-salt vertical-cavity surface-emitting laser (VCSEL) operating at 325 K is demonstrated. The laser emission is generated in a half-wavelength microcavity consisting of seven pairs of PbSe/PbSrSe multiple-quantum-wells embedded in two mirrors and optically pumped with 5 ns laser pulses. 相似文献
10.
N Majumdar P Bhattacharya DC Biswas RK Choudhury DM Nadkarni A Saxena 《Canadian Metallurgical Quarterly》1995,51(6):3109-3115