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排序方式: 共有93条查询结果,搜索用时 15 毫秒
1.
Mingjun Li Kosuke Nagashio Ph.D. Kazuhiko Kuribayashi 《Metallurgical and Materials Transactions A》2002,33(8):2677-2683
A mullite (3Al2O3·2SiO2) sample has been levitated and undercooled in an aero-acoustic levitator, so as to investigate the solidification behavior
in a containerless condition. Crystal-growth velocities are measured as a function of melt undercoolings, which increase slowly
with melt undercoolings up to 380 K and then increase quickly when undercoolings exceed 400 K. In order to elucidate the crystal
growth and solidification behavior, the relationship of melt viscosities as a function of melt undercoolings is established
on the basis of the fact that molten mullite melts are fragile, from which the atomic diffusivity is calculated via the Einstein-Stokes equation. The interface kinetics is analyzed when considering atomic diffusivities. The crystal-growth
velocity vs melt undercooling is calculated based on the classical rate theory. Interestingly, two different microstructures are observed;
one exhibits a straight, faceted rod without any branching with melt undercoolings up to 400 K, and the other is a feathery
faceted dendrite when undercoolings exceed 400 K. The formation of these morphologies is discussed, taking into account the
contributions of constitutional and kinetic undercoolings at different bulk undercoolings. 相似文献
2.
F. Onishi T. Miyake Y. Inatomi K. Kuribayashi 《Microgravity science and technology》2006,18(3-4):86-90
Application of a uniform magnetic field is expected to be a promising substitute for utilization of the microgravity environment from the view point of damping of convection in electrically conductive fluid. Measurements of interdiffusion coefficients in In80Sn20, Sn95Pb5, and Ge97.5Si2.5 melts were performed in a wide temperature range up to 1473 K under a uniform and horizontal static magnetic field of 1 T by utilizing the magnetohydrodynamics effect in these melts. 相似文献
3.
R. Ueyama K. Kamada M. Harada T. Ueyama T. Yamamoto K. Kuribayashi K. Koumoto T. Shiosaki 《Journal of Materials Science》2001,36(2):371-379
Physical and electrical properties of three types of Ag-Pd pastes, which consist of different metal fine powders, i.e., a coprecipitated powder, an agglomerated alloy powder made by heat treatment and a pulverized alloy powder produced by improved pulverization method, have been studied. The paste prepared from pulverized alloy powder showed a higher film packing density (6.3 g/cm3) than those made of the other powders. The film consisting of pulverized alloy powder showed a lower expansion at around 500 °C, a lower shrinkage from 700 °C to 1100 °C and a lower electric resistivity. The results indicated that the paste which consists of an pulverized Ag-Pd alloy powder was superior in performance to the other two pastes for an internal electrode material of multilayer ceramic device. 相似文献
4.
5.
This paper reports work on complex formation from ZDP and various aliphatic amines, and their equilibrium states in oil, adsorptivities and antiwear properties are investigated. Complex formation from ZDP and amine was proven by isolation and identification of solid crystals, and various complexes were found from mono- and diamines. The complex from monoamine has lower adsorptivity than free ZDP, while the poorer adsorptivity of ZDP/monoamine complex makes its antiwear property worse. 相似文献
6.
Ryosuke Ueyama Masahiro Harada Tamotu Ueyama Takashi Yamamoto Tadashi Shiosaki Kiyoshi Kuribayashi Kunihito Koumoto Won Son Seo 《Journal of Materials Science: Materials in Electronics》2000,11(2):139-143
Ultrafine BaTiO3 particles were prepared by a micro-emulsion charring (MEC) method. The MEC method consisted of two steps. The first step is the preparation of a water/oil micro-emulsion with BaTiO3 elements, and the second is a low temperature firing process in N2 atmosphere, which includes charring of oil in an emulsion and powdering BaTiO3 particles with the char. The char formed around BaTiO3 particles prevents an agglomeration of BaTiO3 particles during firing. In the present experiment, the W/O ratio and the amount of emulsifier greatly influenced the size of droplets of the emulsion. The charring temperature was another important experimental factor in order to obtain the desired BaTiO3 particles. The finally obtained BaTiO3 charring powders were monodispersed spherical particles and the particle size was 0.1 m to 0.5 m. 相似文献
7.
E. Sato H. Morioka K. Kuribayashi D. Sundararaman 《Journal of Materials Science》1999,34(18):4511-4518
The effect of Al2O3 doping of around 0.1 wt% on superplastic behavior was studied in 3 mol% yttria-stabilized tetragonal zirconia polycrystal (TZP) which was free from SiO2 contamination and had a grain size of 0.4 m. Compression creep tests revealed that high-purity TZP with less than 0.07 wt% Al2O3 had two deformation regions: the low stress region had a stress exponent of three and an apparent activation energy of 640 kJ/mol, and the high stress region had two and 460 kJ/mol. On the other hand, TZP containing more than 0.12 wt% Al2O3 had only one region which had a stress exponent of two and an activation energy of 480 kJ/mol. The region of diffusion control with a stress exponent of one was not observed in any samples. High resolution transmission electron microscopy revealed that no amorphous grain boundary phase was produced even with 0.18 wt% Al2O3 doping. Energy dispersive X-ray spectroscopy near grain boundaries revealed that yttrium was segregating at the grain boundaries with denuded zones of 30 nm width, which were created during slow cooling from the sintering temperature. 相似文献
8.
Zengyun Jian Kosuke Nagashio Kazuhiko Kuribayashi 《Metallurgical and Materials Transactions A》2002,33(9):2947-2953
Using an electromagnetic levitation facility with a laser heating unit, silicon droplets were highly undercooled in the containerless
state. The crystal morphologies on the surface of the undercooled droplets during the solidification process and after solidification
were recorded live by using a high-speed camera and were observed by scanning electron microscopy. The growth behavior of
silicon was found to vary not only with the nucleation undercooling, but also with the time after nucleation. In the earlier
stage of solidification, the silicon grew in lateral, intermediary, and continuous modes at low, medium, and high undercoolings,
respectively. In the later stage of solidification, the growth of highly undercooled silicon can transform to the lateral
mode from the nonlateral one. The transition time of the sample with 320 K of undercooling was about 535 ms after recalescence,
which was much later than the time where recalescence was completed. 相似文献
9.
H. Matsushima T. Nishida Y. Konishi Y. Fukunaka Y. Ito K. Kuribayashi 《Electrochimica acta》2003,48(28):2446-4125
Water electrolysis was conducted in both alkaline (25 wt.% KOH, 2 wt.% KOH) and acid (0.1N H2SO4) solutions for 8 s under microgravity environment realized in a drop shaft. The gas bubble formation of hydrogen and oxygen on platinum electrodes was observed by CCD camera. In alkaline solutions, a bubble froth layer grew on the electrode surface. Hydrogen bubble size was smaller than that of oxygen. The current density at constant potential decreased continually with time. In spite of the growth of a bubble froth layer on the electrode, the electrolysis never stopped, apparently because fresh electrolyte is supplied to the electrode surface by microconvection induced by the gas bubble evolution. In acid solution, hydrogen gas bubbles frequently coalesced on the cathode surface, yielding a larger average bubble than that of oxygen. The current density did not vary at constant potentials from –0.4 to −0.8 V versus reversible hydrogen electrode (RHE), because the effective electrode surface area was significantly reduced by the larger bubble size compared to alkaline electrolyte. The present experiments indicate that, especially in a microgravity environment, the bubble evolution behavior and the resultant current–potential curves are significantly influenced by the wettability of the electrode in contact with the electrolyte. 相似文献
10.
Measuring accurate deformation distribution of large-scale structures inexpensively and efficiently is a crucial challenge of structural health monitoring. Phase-based imaging technique has great potential for accurate and robust multipoint displacement measurement in the field. In this study, the sampling Moiré method—one of the promising optical techniques—was applied to the displacement measurement of a concrete bridge for the high-speed railway in Japan. Using retroreflective Moiré markers, the two-dimensional in-plane displacements at multiple locations could be easily measured from recorded digital images at a distance of 20 m regardless of day and night. Results of the dynamic deflection obtained from the sampling Moiré method were in good agreement with those from a conventional laser Doppler vibrometer. The time series of two-dimensional displacement analyses when the outbound or inbound trains passed at the speed of 150 or 320 km/h through the bridge revealed that the points at the centre and the quarter of the bridge span demonstrated complex deformation behaviour showing elliptical rotation. The effects of random noise of the recorded image were quantitatively investigated, and the air fluctuation was discussed from the field experiments. We proved that measurements using the sampling Moiré method could be more stable at night than daytime. 相似文献