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排序方式: 共有151条查询结果,搜索用时 671 毫秒
1.
Andrea Mariela Araya-Sibaja Valdir Soldi Carlos Eduardo Maduro Campos Simone Gonçalves Cardoso 《Drug development and industrial pharmacy》2015,41(5):851-858
Progesterone is a natural hormone steroid used in humans for several treatments and in livestock for artificial insemination, which exhibits two polymorphic forms at ambient conditions: form 1 and form 2. Form 2 is metastable and more soluble than form 1; however, it is not suitable to use as powder raw material because it transforms into form 1 by the effects of grinding. A polymorphic screening of progesterone based on polymer-induced heteronucleation method was performed as an alternative to prepare the metastable form. Polyvinyl alcohol, hydroxypropyl methylcellulose (HPMC), dextran, gelatin, polyisoprene (PI) and acrylonitrile-butadiene (NBR) copolymer were used. Crystals were prepared from 0.5, 10 and 40?mg/mL solutions in acetone at room temperature by solvent evaporation. The samples were characterized by X-ray powder diffraction, differential scanning calorimetry (DSC), scanning electron microcopy and attenuated total reflectance infrared Fourier transform spectroscopy. Form 1 was nucleated from 40?mg/mL solutions on the six polymers and from 10?mg/mL solutions on PI and NBR. The mixture of form 1 and form 2 was obtained from 10?mg/mL solution on HPMC, dextran and gelatin and from 0.5?mg/mL solution crystallizations. Therefore, the polymeric devices, which crystallized the metastable and more soluble polymorph (2) of progesterone, would be a promissory alternative for the pharmaceutical applications. 相似文献
2.
Vanesa Rodríguez-Amor Juan P. Fernández-Blázquez Antonio Bello Ernesto Pérez María L. Cerrada 《Polymer Bulletin》2008,60(1):89-96
Summary The effect of molecular weight on the uniaxial orientation process has been analyzed in two samples of thermotropic poly(diethylene
glycol p,p′-bibenzoate), evaluating the influence of that parameter on the type of orientation obtained. Several strain rates and deformation
temperatures have been tested in order to map out the conditions for obtaining the two different kinds of orientation. The
results show that in the lower molecular weight PDEB sample (Mw=31200) it is rather easy to get exclusively perpendicular “anomalous” orientation, with the molecular axes aligned transversely
to the stretching direction. However, it is extremely difficult to obtain 100% parallel “normal” orientation. On the contrary,
either type of orientation or a mixture of them can be easily developed for the higher molecular weight PDEB sample (Mw=102900). 相似文献
3.
The effective thermal diffusivity of foodstuffs was estimated from time-temperature histories in the geometric center of samples exposed to heating and cooling processes.Transfer functions methodology was used as an alternative method to estimate the thermal diffusivity assuming that conduction was the main heat transfer mechanism. The samples were characterized as delayed first-order systems with unit gain, dead time (L) and time constant (τ).The results were compared with those obtained from the fh value and with results reported in the literature. 相似文献
4.
Mariela Hristova 《国际互联网参考资料服务季刊》2013,18(2):45-64
This study explores citation management usage patterns of undergraduate students, graduate students, and faculty. We analyze the temporal use of RefWorks with an eye toward informing reference services and instruction initiatives. The frequency and intensity of use allow us to glean an understanding of user groups on campus. While our findings for undergraduates and faculty conform to general assumptions, graduate students emerge as a group more similar to faculty than anticipated. Graduate students’ use of RefWorks is characterized by steady logins and large amounts of references; thus, suggesting that personalized instruction might benefit graduate students more than scheduled workshops. 相似文献
5.
Irena Borovanska María L. Cerrada Peter Zipper 《Polymer-Plastics Technology and Engineering》2016,55(5):486-497
The purpose of this study is to investigate the effect of treated natural zeolite on the flow behavior, morphology, thermal, and mechanical properties in recycled polyolefin blends. A model polymer blend consisting of 95 wt% polyolefines and 5 wt% polystyrene was studied. Compositions from this recycled blend and dehydrated zeolite in a narrow concentration range (0–5 wt%) were treated with maleic anhydride-grafted polypropylene and initiator dicumyl peroxide. The compositions were characterized by capillary rheometry, wide-angle X-ray scattering, differential scanning calorimetry, scanning electron microscopy, and mechanical tests. The results show a compatibilizing effect of treated zeolite expressed by increase of shear viscosity and improvement of interfacial interactions and impact strength. The results can open wide possibilities for utilization of treated zeolite in recycling of unsorted polymer wastes. 相似文献
6.
Mariela Cerrada René-Vinicio Sánchez Fannia Pacheco Diego Cabrera Grover Zurita Chuan Li 《Applied Intelligence》2016,44(3):687-703
Feature selection is an important aspect under study in machine learning based diagnosis, that aims to remove irrelevant features for reaching good performance in the diagnostic systems. The behaviour of diagnostic models could be sensitive with regard to the amount of features, and significant features can represent the problem better than the entire set. Consequently, algorithms to identify these features are valuable contributions. This work deals with the feature selection problem through attribute clustering. The proposed algorithm is inspired by existing approaches, where the relative dependency between attributes is used to calculate dissimilarity values. The centroids of the created clusters are selected as representative attributes. The selection algorithm uses a random process for proposing centroid candidates, in this way, the inherent exploration in random search is included. A hierarchical procedure is proposed for implementing this algorithm. In each level of the hierarchy, the entire set of available attributes is split in disjoint sets and the selection process is applied on each subset. Once the significant attributes are proposed for each subset, a new set of available attributes is created and the selection process runs again in the next level. The hierarchical implementation aims to refine the search space in each level on a reduced set of selected attributes, while the computational time-consumption is improved also. The approach is tested with real data collected from a test bed, results show that the diagnosis precision by using a Random Forest based classifier is over 98 % with only 12 % of the attributes from the available set. 相似文献
7.
Luiz Antonio Joia Mariela Fontenelle Sily de Assis 《Information Systems Management》2019,36(3):228-242
ABSTRACTIn this paper, we use the Delphi method to identify the main motivations that have led IT professionals to intend to move to another area. We found that the pursuit of career growth and the quest for acquiring new experiences and abilities have a marked impact on the IT professional turnaway intention. Moreover, female IT professionals and IT professionals oriented by the career advancement paradigm have a higher propensity to abandon the IT area. 相似文献
8.
Alberto García‐Peñas José M Gómez‐Elvira María U de la Orden María L Cerrada Ernesto Pérez 《Polymer International》2016,65(5):596-604
The influence of crystallization rate on the interesting polymorphism of random isotactic poly(propylene‐co‐1‐heptene) copolymers was studied, with particular attention to the conditions for obtaining the mesomorphic phase. Owing to the important decrease of cooling rate involved as the 1‐heptene content increases, the mesophase can be clearly observed by DSC for co‐unit contents above about 5 mol%. Furthermore, only the mesophase (or the amorphous phase) was found for the copolymer with 13.9 mol% 1‐heptene at common cooling rates of the calorimeter. Additionally, the copolymer with 21.4 mol% co‐units was found to be completely amorphous under any thermal treatment analyzed. Variable‐temperature diffraction experiments were carried out to ascertain unambiguously the nature of the phases involved. Finally, a remarkable transparency was attained (above 80% transmittance in the visible light region) at intermediate and high 1‐heptene contents, using easily accessible cooling rates. © 2016 Society of Chemical Industry 相似文献
9.
Benítez B Archile A Rangel L Bracho M Hernández M Márquez E 《Archivos latinoamericanos de nutrición》2002,52(3):307-312
The purpose of this research was to evaluate the nutritional quality and acceptability of a meat product formulated with mechanically deboned poultry meat (40%), bovine plasma (40%) and bovine red cells (3%) as major ingredients. Proteins, fat, humidity and ash were determined by AOAC procedure, iron and calcium by Atomic Absorption Spectrometry and essential amino acids by HPLC. Biological evaluation was performed using digestibility and PER procedures. To evaluate the acceptability (flavor, color and odor) of the product were used 277 children. Results indicated that 100 g of the formulated meat product contain 10.7 g of proteins, 4.4 g of fat, 68.6 g of humidity, 2.9 g of ash, 4.9 mg of iron, 46.6 mg of calcium. Essential amino acids are above the FAO requirements for a highly nutritional protein digestibility (92.4%) and PER (2.18). Acceptability was 91.3% for flavor, 81.2% for color and 92.4% for odor. The high nutritional quality and acceptability along with the low cost make this meat product suitable for government social programs. 相似文献
10.
In this work we report the results of a combined biochemical and electrochemical study aimed to analyze both the growth of biofilms of Pseudomonas fluorescens on copper samples and its possible role in the instability of the metal/electrolyte interface.DNA and RNA were quantified along the time for biofilms grown on copper and glass to estimate both the growth of the bacterial population and its metabolic state (through the RNA/DNA ratio). The expression and specific activity of catalase were also determined to gain insight into their possible role in corrosion acceleration. The electrochemical behavior of the biofilm/copper interface was monitored by Linear Polarization Resistance (Rp) and electrochemical impedance spectroscopy (EIS) along the experiments.Results showed a longer lag phase for biofilms developing on copper that included a period of high metabolic activity (as measured by the RNA/DNA ratio) without biomass growth. Biological activity introduced a new time constant at intermediate frequencies in EIS spectra whose capacitive behavior increased with the biofilm development. The increment in this biofilm-related signal was accompanied by a strong limitation to charge transfer through a diffusion controlled process probably due to oxygen exhaustion by cells respiration, while the resistance of the interface decreased presumably due to oxide dissolution by local acidification under the colonies. In addition, catalase activity was found to be high in mature copper-tolerant biofilms, which differentially express a catalase isoform not present in biofilms growing on glass. 相似文献