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1.
Kumari Asha Neeraj Kumar Biswas Sakshi Saxena Vibha Rani Satsangi Rohit Shrivastav Rama Kant Sahab Dass 《International Journal of Hydrogen Energy》2021,46(40):20858-20870
The present study attempts quantitative determination of changes in the morphological surface features viz. fractal dimension, lower and upper cut off length scale through Power Spectral Density analysis prior to and after irradiation of 100 KeV Ar+ ion beam at incidence angles of 0°, 40° and 60° on ZnO thin films. All the unirradiated and irradiated samples are subjected to photoelectrochemical characterization and a correlation between photoelectrochemical performance and morphological parameters is established. Sample irradiated at 40° angle at the fluence of 5 × 1016 ions/cm2 is found to possess maximum fractal dimension of 2.72, lower and upper cut off length scale of 3.16 nm and 63.00 nm respectively. This sample exhibits maximum photocurrent density of 3.19 mA/cm2 and applied bias photon-to-current efficiency of 1.12% at 1.23 V/RHE. Hydrogen gas collected for duration of 1 h for the same sample was ~4.83 mLcm?2. 相似文献
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In a prospective study of layered versus mass closure of abdominal incisions in infants and children, 34 cases underwent wound closure by layered and mass closure technique on an alternate basis. All the patients were assessed for their nutritional status and haemoglobin level pre-operatively, and wound complications were compared with respect to closure technique, nutritional status and normal haemoglobin level. Presence of protein energy malnutrition and anaemia did not increase the risk of wound complications with either of the technique. 相似文献
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The present study was aimed at understanding the response of 2014 Al alloy dispersed with graphite particles in various corrosive environments. Marine (sodium chloride) as well as acidic media were selected for the purpose with a view to widen the range of utility of the composite for applications where such environments may be encountered. Studies were also extended to characterize the corrosion resistance of the composite in fresh as well as used lubricating oils to explore the possibilities of using it in bearing, bushing and such other applications. The corrosion behaviour of the base alloy processed under identical conditions was also examined in the above media to see the influence of graphite addition in the alloy. In order to assess the role of the matrix microstructure, the composite as well as the base alloy was subjected to corrosion in heat-treated as well as-cast conditions. It was observed that the specimens suffered from the maximum rate of corrosion in acid, while sodium chloride produced the minimum corrosion rate. Oil in both used and fresh conditions revealed a negligibly small extent of corrosion. The composite was found to show a higher rate of corrosion than the base alloy under identical test conditions. This was attributed to the dispersoid/matrix interfacial corrosion in the case of the graphitic aluminium alloy. Heat treatment of the composite and the base alloy was found to lower the rate of corrosion in the environments tested. Microstructural modifications of the matrix and possible relief of residual stresses were thought to be responsible for the lower rate of corrosion in the heat-treated condition. 相似文献
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We analyze and numerically study the code-matching logic module that is the central element in a proposed soliton-based ring network system running at peak rates of 100 Gb/s. The proposed network is packet-switched, and fast logic is required to route each packet. That is the function of the code-matching logic module, and four soliton logic gates that can perform fast logic are the key devices in its design. The behavior of the code-matching logic module is governed by a large set of parameters, and we simulate it by varying many of these parameters. The physical effects that occur in these devices and their significance are analyzed. The results indicate that the logic module will work but within a restricted parameter range 相似文献
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Conducting composites of polythiophene (PTP) and polyfuran (PF) with acetylene black (AB) were prepared via chemical oxidative polymerization of thiophene and furan in a suspension of AB in CHCl3 at room temperature using anhydrous FeCl3 as the oxidant. Formation of PTP and PF and their subsequent incorporation in PTP–AB and PF–AB composite systems were confirmed by FTIR analysis. Scanning electron microscope analysis showed the presence of compact clusters of particles in both composites. Transmission electron micrographs of PTP–AB and PF–AB composites showed formation of globular polymer encapsulated AB particles with average diameters of the order of ~100 nm in both systems. Thermogravimetric analysis revealed that the overall thermal stability varied in the order: AB > PTP–AB > PTP and AB > PF–AB > PF. DC conductivity values for the PTP–AB and PF–AB composites were of the order of 10?2 and 10?3 S cm?1, respectively. Copyright © 2004 Society of Chemical Industry 相似文献
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N‐vinylcarbazole (NVC) was polymerized by 13X zeolite alone in melt (65°C) or in toluene (110°C) and a poly(N‐vinylcarbazole) (PNVC)‐13X composite was isolated. Composites of polypyrrole (PPY) and polyaniline(PANI) with 13X zeolite were prepared via polymerization of the respective monomers in the presence of dispersion of 13X zeolite in water (CuCl2 oxidant) and in CHCl3 (FeCl3 oxidant) at an ambient temperature. The composites were characterized by Fourier transform infrared analyses. Scanning electron microscopic analyses of various composites indicated the formation of lumpy aggregates of irregular sizes distinct from the morphology of unmodified 13X zeolite. X‐ray diffraction analysis revealed some typical differences between the various composites, depending upon the nature of the polymer incorporated. Thermogravimetric analyses revealed the stability order as: 13X‐zeolite > polymer‐13X‐zeolite > polymer. PNVC‐13X composite was essentially a nonconductor, while PPY‐13X and PANI‐13X composites showed direct current conductivity in the order of 10?4 S/cm in either system. However, the conductivity of PNVC‐ 13X composite could be improved to 10?5 and 10?6 S/cm by loading PPY and PANI, respectively. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 913–921, 2006 相似文献
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