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Journal of Inorganic and Organometallic Polymers and Materials - The silver oxide nanoparticle was successfully synthesized using floral waste by simple one pot, cost effective method. The complete...  相似文献   
3.
Journal of Inorganic and Organometallic Polymers and Materials - Different concentrations of ZnFe2O4 and manganese substituted ZnFe2O4 nanoparticles (10%, 20% and 30%) dispersed...  相似文献   
4.
A new series of liquid crystalline polymers containing aromatic triad ester mesogen and 1,1′‐disubstituted ferrocene as a nonmesogenic unit along with polymethylene spacer was synthesized. The polymer was synthesized by a room temperature polycondensation reaction between bis(4‐chloroformyl phenyloxy alkyl ferrocene dicarboxylate) and quinol. The alkyl groups have been varied by an even number of methylene groups with a range from two to ten groups. All the polymers were found to possess liquid crystalline properties. The identification of the mesophase is more transparent with an increase in the spacer. The thermal characteristics were studied using thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC). The results reveal that the thermal stability of the polymers was decreased with increasing spacer length. The Tg, Tm, and Ti of the polymers decreased with increasing methylene groups. The incorporation of the ferrocene moiety also has a considerable effect on the glass transition temperature. The char yield of the polymer decreases with an increasing methylene chain length. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 86: 3494–3501, 2002  相似文献   
5.
Control chart patterns, besides determining the presence of assignable causes, also provide hints on the nature of assignable cause(s) present. Relating the patterns exhibited on the control chart to assignable causes is an ambiguous and vague task especially when multiple patterns co-exist. In this work, a rule based fuzzy inference system is developed for control chart to prioritize the control chart causes based on the accumulated evidence. When a process goes out of control, search for assignable causes can be assisted by the priorities assigned to the causes. For an in-control process, developing patterns can be tracked and preventive action can be taken to prevent the process from going out of control.  相似文献   
6.
Improvement of tea leaves fermentation with Aspergillus spp. pectinase   总被引:1,自引:0,他引:1  
The pectinase enzymes isolated from Aspergillus spp., A. indicus, A. flavus and A. niveus were used for fermentation of tea leaves. The enzymes were purified and characterized. The effect of both crude enzyme preparation and purified pectinase enzymes on the improvement of tea leaf fermentation were determined in terms of theaflavin, thearubigin, high polymerized substances, total liquor colour, dry matter content and total soluble solids of the tea produced. The crude enzyme preparations obtained from ethanol precipitation were found to be more effective in improving tea leaf fermentation than the purified pectinase enzymes.  相似文献   
7.
Nallusamy  Tamilselvam  Vijayakumar  S. 《SILICON》2022,14(7):3129-3146
Silicon - Recent innovations in materials technology upsurge the use of Al2O3 and SiC based composites in aerospace, automotive, defence, transportation, and sporting industries. The reinforcements...  相似文献   
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12-Tungstophosphoric acid supported on montmorillonite K10 (PWA/mont-K10) catalysed Pechmann condensation reaction was reported. The catalyst was characterized by XRD, FTIR, UV–Vis DRS, surface area and pore size analysis, TGA and acidity by DRIFTS using pyridine. The morphology of the catalyst was studied by SEM. The activity of mont-K10, mont-KSF, \textSO 4 2 - \mathord
/ \vphantom \textSO 4 2 - \textZrO 2 \textZrO 2 {{{\text{SO}}_{ 4}^{{ 2 {-}}} } \mathord{\left/ {\vphantom {{{\text{SO}}_{ 4}^{{ 2 {-}}} } {{\text{ZrO}}_{ 2} }}} \right. \kern-\nulldelimiterspace} {{\text{ZrO}}_{ 2} }} , 12-tungstophosphoric acid, and PWA/mont-K10 was investigated by condensation reaction of resorcinol with ethyl acetoacetate in the absence of solvent. Effect of molar ratio, amount of catalyst, reaction temperature and time on the yield of 7-hydroxy-4-methylcoumarin had been investigated on PWA/mont-K10. PWA/mont-K10 catalysed condensation of ethyl acetoacetate with phenol and a few substituted phenols had also been carried out to yield corresponding coumarins. The recycled catalyst showed reduced activity after single use. 15 wt% PWA on mont-K10 was found to be effective for synthesis of coumarin derivatives without employing any solvent.  相似文献   
10.
The high hydrostatic coefficients of porous piezoelectric materials provide the reduced acoustic impedance for the effective coupling with water medium as well as biological tissues. The hydrostatic strain coefficient (dh), voltage coefficients (gh) and longitudinal piezoelectric coefficient (d33) of porous piezoelectric materials has a strong dependence on processing parameters such as porosity parameter, polymer percentage, density and poling voltage. In this work, a nonparametric regression has been carried out to figure out the nonlinear relationships between the hydrostatic coefficients and its processing parameters. The nonparametric regression has been carried out by artificial neural network. The Network architecture utilized is radial basis function (RBF) which is combined with Fuzzy Clustering Method (FCM) to identify the hidden node numbers and widths. The porosity parameter was calculated from scanning electron micrographs of the porous piezoelectric materials using conventional image processing techniques. The results of the artificial neural network were evaluated against experimental data.  相似文献   
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