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1.
Since the discovery in 1922 of 2,2-diphenyl-1-(2,4,6-trinitrophenyl) hydrazyl stable free radical (DPPH·), the chemistry of such open-shell compounds has developed continuously, allowing for both theoretical and practical advances in the free radical chemistry area. This review presents the important, general and modern aspects of the chemistry of hydrazyl free radicals and the science behind it. 相似文献
2.
Petre Badica Dan Batalu Mihail Burdusel Mihai A. Grigoroscuta Gheorghe V. Aldica Monica Enculescu Raluca A. Gabor Zhiyong Wang Ruoxuan Huang Peifeng Li 《Ceramics International》2018,44(9):10181-10191
Pristine and (SiC+Te)-added MgB2 powders, green and spark plasma sintered (SPS) compacts were investigated from the viewpoint of quasi-static and dynamic (Split-Hopkinson Pressure Bar, SHPB) compressive mechanical properties The amount of the additive (SiC+Te) was selected to be the optimum one for maximization of the superconducting functional parameters. Pristine and added MgB2 show very similar compressive parameters (tan δ, fracture strength, Vickers hardness, others) and fragment size in the SHPB test. However, for the bulk SPSed samples the ratio of intergranular to transgranular fracturing changes, the first one being stronger in the added sample. This is reflected in the quasi-static KIC that is higher for the added sample. Despite this result, sintered samples are brittle and have roughly similar fragmentation behavior as for brittle engineering ceramics. In the fragmentation process, the composite nature of our samples should be considered with a special focus on MgB2 blocks (colonies) that show the major contribution to fracturing. The Glenn-Chudnovsky model of fracturing under dynamic load provides the closest values to our experimental fragment size data. 相似文献
3.
C. Busuioc C.D. Ghitulica A. Stoica M. Stroescu G. Voicu V. Ionita L. Averous S.I. Jinga 《Ceramics International》2018,44(8):9433-9441
Bacterial cellulose membranes were employed as templates for calcium phosphates deposition by successive immersion in solutions of Ca(NO3)2·4H2O and (NH4)2HPO4, under ultrasonication. During the wet chemical reaction, mineral phases were loaded on bacterial cellulose fibrils, leading to precursor hybrid composites. These were subjected to a lyophilisation procedure in order to preserve the 3D porous aspect and afterwards to a thermal treatment with the aim of removing the polymeric phase and generating well crystallized structures. Different types of morphologies were achieved by varying the heating rate, as well as the calcination temperature and period. The as-prepared samples and the final ones were investigated from compositional and structural point of view through X-ray diffraction and Fourier-transform infrared spectroscopy and morphologically concerning by scanning electron microscopy. The magnetic properties were also evaluated in order to demonstrate the suitability of the obtained materials for the development of magnetic scaffolds dedicated to hard tissue applications. 相似文献
4.
This paper considers the estimation of the parameters of a linear discrete-time system from noise-perturbed input and output measurements. The conditions imposed on the system are fairly general. In particular, the input and output noises are allowed to be auto-correlated and they may be cross-correlated as well. The proposed method makes use of an instrumental variable (IV)-vector to produce a covariance matrix that is pre- and postmultiplied by some prechosen weights. The singular vectors of the so-obtained matrix possess complete information on the system parameters. A weighted subspace fitting (WSF) method is then applied to the aforementioned singular vectors to consistently estimate the parameters of the system. The IV-WSF technique suggested herein is noniterative and easy to implement, and has a small computational burden. The asymptotic distribution of its estimation errors is derived and the result is used to motivate the choice of the weighting matrix in the WSF step and also to predict the estimation accuracy. Numerical examples are included to illustrate the performance achievable by the method.This work has been supported by the Swedish Research Council of Engineering Sciences under contract 93-669 and by the Göran Gustafsson Foundation. 相似文献
5.
An asymptotically efficient autoregressive moving-average (ARMA) spectral estimator is presented, based on the sample covariances of observed time series. The estimate of the autoregressive (AR) part is shown to be identical to the optimal instrumental variable (IV) estimator in [7] although derived here using a different approach. The moving-average (MA) spectral parameter estimate is new. 相似文献
6.
Mats Cedervall Petre Stoica Randolph Moses 《Circuits, Systems, and Signal Processing》1997,16(3):349-362
We propose a new algorithm for estimating the parameters of damped, undamped, or explosive sinusoidal signals. The algorithm resembles the MODE algorithm, which is commonly used for direction of arrival estimation in the array signal processing field. It is derived as a natural approximation to an asymptotically (high-SNR) optimal parameter estimator and has excellent statistical accuracy. Nevertheless, it is computationally simple and easy to implement. Numerical examples are included to illustrate the performance of the proposed method.This work has been supported by the Swedish Research Council for Engineering Sciences (TFR). 相似文献
7.
8.
Hidden-Action in Network Routing 总被引:1,自引:0,他引:1
Feldman M. Chuang J. Stoica I. Shenker S. 《Selected Areas in Communications, IEEE Journal on》2007,25(6):1161-1172
In communication networks, such as the Internet or mobile ad-hoc networks, the actions taken by intermediate nodes or links are typically hidden from the communicating endpoints; all the endpoints can observe is whether or not the end-to-end transmission was successful. Therefore, in the absence of incentives to the contrary, rational (i.e., selfish) intermediaries may choose to forward messages at a low priority or simply not forward messages at all. Using a principal-agent model, we show how the hidden-action problem can be overcome through appropriate design of contracts in both the direct (the endpoints contract with each individual router directly) and the recursive (each router contracts with the next downstream router) cases. We further show that, depending on the network topology, per-hop or per-path monitoring may not necessarily improve the utility of the principal or the social welfare of the system. 相似文献
9.
We consider a special growth-curve (SGC) model with a known steering matrix and generalized waveform in the presence of unknown interference and noise. Several estimators of the complex amplitude based on this model are derived, including the methods of approximate maximum likelihood (AML), minimum variance distortionless response (MVDR), and amplitude and phase estimation (APES). We analyze the statistical properties of these estimators and show that in the presence of temporally white but spatially correlated noise and interference, AML is asymptotically statistically efficient for a large snapshot number while MVDR and APES are asymptotically equivalent but not statistically efficient. Via several numerical examples, we also show that when the noise and interference are both spatially and temporally correlated, the APES estimator can achieve better estimation accuracy and exhibit greater robustness than the other methods. 相似文献
10.
Orthogonal space-time block codes: maximum likelihood detection for unknown channels and unstructured interferences 总被引:3,自引:0,他引:3
Space-time coding (STC) schemes for communication systems employing multiple transmit and receive antennas have been attracting increased attention. The so-called orthogonal space-time block codes (OSTBCs) have been of particular interest due to their good performance and low decoding complexity. In this paper, we take a systematic maximum-likelihood (ML) approach to the decoding of OSTBC for unknown propagation channels and unknown noise and interference conditions. We derive a low-complexity ML decoding algorithm based on cyclic minimization and assisted by a minimum amount of training data. Furthermore, we discuss the design of optimal training sequences and optimal information transfer to an outer decoder. Numerical examples demonstrate the performance of our algorithm. 相似文献