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1.
Poly(ethylene aspartate) [PEA] was synthesized by the melt condensation of D,L-aspartic acid and ethylene glycol. PEA containing pendent amino and carbonyl groups in its repeating chain was used as the polymeric ligand for complexation with transition metal ions, viz. Co(II), Ni(II), Cu(II), Mn(II), Zn(II), Cd(II), Ca(II), Mg(II), Pb(II) and Hg(II). Complexation was found to be most effective in DMSO. The resulting polyester-metal complexes were solid coloured materials which have been characterized by IR spectroscopy, elemental analysis and magnetic susceptibility measurements. The thermal stability of the polyester-metal complexes was investigated by thermogravimetric analysis (TGA). On the basis of the physico-chemical studies, an oxygen and nitrogen coordinated structure for the polyester-metal complexes is proposed. 相似文献
2.
3.
4.
The counter current heat exchanger theory with periodic inlet temperatures has been applied to analyze the thermal performance of a water heating system. The theoretical results obtained are in agreement with the experimental data reported in the literature. 相似文献
5.
A decision aid for scheduling production in glass fiber manufacturing industry is described. The methodology combines a linear programming (LP) optimization model with a heuristic model. The LP model determines production goals; the heuristic model then uses the LP output to incorporate system-specific constraints in developing processing sequences. 相似文献
6.
7.
The nonlinear Boussinesq equation is used to understand water table fluctuations in various ditch drainage problems. An approximate solution of this equation with a random initial condition and deterministic boundary conditions, recharge rate and aquifer parameters has been developed to predict a transient water table in a ditch-drainage system. The effects of uncertainty in the initial condition on the water table are illustrated with the help of a synthetic example. These results would find applications in ditch-drainage design.Notation
A
/ tanh t
-
a
lower value of the random variable representing the initial water table height at the mid point
-
a+b
Upper value of the random variable representing the initial water table height at the midpoint
-
B
tanh t
-
C
4/
-
h
variable water table height
- h
mean of the variable water table height
-
h
m
variable water table height at the mid point
- h
m
mean of the variable water table height at the mid point
-
K
hydraulic conductivity
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L
half spacing between the ditches
-
m
0
initial water table height at the mid point
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N
Uniform rate of recharge
-
S
specific yield
-
t
time of observation
-
x
distance measured from the ditch boundary
-
(4/SL)(NK)1/2
-
(L/4)(N/K)1/2
-
dummy integral variable 相似文献
8.
B. N. Rai A. K. Sinha U. K. Ghosh S. N. Gupta S. N. Upadhyay 《Chemical Engineering Communications》1988,68(1):15-30
Mass transfer in annuli has been critically examined for various flow situations. The overall mass transfer rate depends on the hydrodynamic regions prevailing in the annular channel as well as on its dimensions. Theoretically consistent correlations are proposed and recommended for both developed and developing boundary layers under laminar and turbulent flow conditions. 相似文献
9.
Sorption of sulfur dioxide (SO2) was carried out on calcium‐based sorbents under dynamic conditions in a fixed bed. The experimental conditions were reaction temperature (700 to 1000°C), SO2 concentration (1000‐10 000 ppm), sorbent particles size (1 to 2 mm) and the types of sorbents (hydroxide or carbonate). The sorption process was found to be effective at low concentration levels (less than 10 000 ppm) as the breakthrough time significantly decreased with increase in concentration. The maximum removal of SO2 was observed at a reaction temperature of 950°C. The hydroxide‐based sorbents of relatively smaller particle size were found to exhibit superior sorption performance in terms of longer breakthrough time and higher sulfate conversion. A mathematical model developed, assuming a porous structure of the sorbent materials, attributed the low sulfation conversion during SO2 sorption due to a pore diffusion mechanism. 相似文献
10.
Flyash, a waste product generated in large quantities in thermal power plants, has been posing problems of disposal. The purpose of the present work was to make a meaningful utilization of flyash as filler in neat epoxy resin matrix and 2% Polybutyleneterepthalate (PBT)/epoxy blend matrix. For this purpose, the tensile, flexural, compression, impact, chemical resistance, and water absorption properties were studied. Composites were made with varying proportion of flyash in epoxy resin and 2% PBT/epoxy blend matrix. Tensile, flexural, and compression properties were measured on a computerized universal testing machine, according to ASTM procedures. Impact strength was determined using izod impact tester for un‐notched specimens. PBT (2%)/epoxy blend matrix composites showed improved mechanical properties over neat epoxy flyash composites. All the composites were found to have good chemical resistance toward acids, solvents, and alkalies. These composites showed better water resistance over neat epoxy flyash composites. POLYM. ENG. SCI. 46:946–953, 2006. © 2006 Society of Plastics Engineers 相似文献