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排序方式: 共有538条查询结果,搜索用时 31 毫秒
1.
Brian Lawn David Marshall Rishi Raj Greg Hirth Trevor Page Julie Yeomans 《Journal of the American Ceramic Society》2021,104(1):23-26
Crystalline quartz has long been identified as among the weakest of abundant crustal minerals. This weakness is particularly evident around the α–β phase inversion at 573°C, in which Si–O bonds undergo a displacive structural transformation from trigonal to hexagonal symmetry. Here we present data using indentation testing methodologies that highlight the precipitous extent of the transformational weakening. Although the indentations are localized over relatively small specimen contact areas, the data quantify the essential deformation and fracture properties of quartz in a predominantly (but not exclusively) compressive stress field, at temperatures and pressures pertinent to conditions in the earth's crust. 相似文献
2.
Kumari Asha Neeraj Kumar Biswas Sakshi Saxena Vibha Rani Satsangi Rohit Shrivastav Rama Kant Sahab Dass 《International Journal of Hydrogen Energy》2021,46(40):20858-20870
The present study attempts quantitative determination of changes in the morphological surface features viz. fractal dimension, lower and upper cut off length scale through Power Spectral Density analysis prior to and after irradiation of 100 KeV Ar+ ion beam at incidence angles of 0°, 40° and 60° on ZnO thin films. All the unirradiated and irradiated samples are subjected to photoelectrochemical characterization and a correlation between photoelectrochemical performance and morphological parameters is established. Sample irradiated at 40° angle at the fluence of 5 × 1016 ions/cm2 is found to possess maximum fractal dimension of 2.72, lower and upper cut off length scale of 3.16 nm and 63.00 nm respectively. This sample exhibits maximum photocurrent density of 3.19 mA/cm2 and applied bias photon-to-current efficiency of 1.12% at 1.23 V/RHE. Hydrogen gas collected for duration of 1 h for the same sample was ~4.83 mLcm?2. 相似文献
3.
Volatilization resulting from the thermal decomposition of Si3 N4 causes the large weight loss and desintering phenomenon observed during pressureless sintering of Si3 N4 -5% MgO and sialon (z =2)-5% MgO. The addition of a few weight percent of Si to the powder suppresses this volatilazation and helps to achieve fully dense Si3 N4 components. 相似文献
4.
Crystallization of Polymer-Derived Silicon Carbonitride at 1873 K under Nitrogen Overpressure 总被引:1,自引:0,他引:1
Martin Friess Joachim Bill Jerzy Golczewski re Zimmermann Fritz Aldinger Ralf Riedel Rishi Raj 《Journal of the American Ceramic Society》2002,85(10):2587-2589
The chemical stability of an amorphous silicon carbonitride ceramic, having the composition 0.57SiC·0.43Si3 N4 ·0.49C is studied as a function of nitrogen overpressure at 1873 K. The ceramic suffers a weight loss at p N2 < 3.5 bar (1 bar = 100 kPa), does not show a weight change from 3.5 to 11 bar, and gains weight above 11 bar. The structure of the ceramic changes with pressure: it is crystalline from 1 to 6 bar, amorphous at ∼10 bar, and is crystalline above ∼10 bar. The weight-loss transition, at 3.5 bar, is in excellent agreement with the prediction from thermodynamic analysis when the activities of carbon, SiC, and Si3 N4 are set equal to those of the crystalline forms; this implies that the material crystallizes before decomposition. The amorphous to crystalline transition that occurs at ∼10 bar, and which is accompanied by weight gain, is likely to have taken place by a different mechanism. A nucleation and growth reaction with the atmospheric nitrogen is proposed as the likely mechanism. The supersaturation required to nucleate α-Si3 N4 crystals is calculated to be 30 kJ/mol. 相似文献
5.
6.
Hou V.T. Kant K. Ramaswami V. Wang J.L. 《Selected Areas in Communications, IEEE Journal on》1994,12(3):456-467
Motivated by field data which showed a large number of link changeovers and incidences of link oscillations between in-service and out-of-service states in common channel signalling (CCS) networks, a number of analyses of the link error monitoring procedures in the SS7 protocol were performed by the authors. This paper summarizes the results obtained thus far and include the following: (a) results of an exact analysis of the performance of the error monitoring procedures under both random and bursty errors; (b) a demonstration that there exists a range of error rates within which the error monitoring procedures of SS7 may induce frequent changeovers and changebacks; (c) an analysis of the performance of the SS7 level-2 transmission protocol to determine the tolerable error rates within which the delay requirements can be met; (d) a demonstration that the tolerable error rate depends strongly on various link and traffic characteristics, thereby implying that a single set of error monitor parameters will not work well in all situations; and (e) some recommendations on a customizable/adaptable scheme of error monitoring with a discussion on their implementability. These issues may be particularly relevant in the presence of anticipated increases in SS7 traffic due to widespread deployment of advanced intelligent network (AIN) and personal communications service (PCS) as well as for developing procedures for high-speed SS7 links currently under consideration by standards bodies 相似文献
7.
Planning collision-free trajectories in time-varying environments: a two-level hierarchy 总被引:1,自引:0,他引:1
We propose a two-level hierarchy for planning collision-free trajectories in time varying environments. Global geometric algorithms for trajectory planning are used in conjunction with a local avoidance strategy. Simulations have been developed for a mobile robot in the plane among stationary and moving obstacles. Essentially, the robot has a global geometric planner that provides a coarse global trajectory (the path and velocity along it), which may be locally modified by the low-level local avoidance module if local sensors detect any obstacles in the vicinity of the robot. This hierarchy makes effective use of the complementary aspects of the global trajectory planning approaches and the local obstacle avoidance approaches. 相似文献
8.
Name resolution using the Domain Name System (DNS) is integral to today’s Internet. The resolution of a domain name is often dependent on namespace outside the control of the domain’s owner. In this article we review the DNS protocol and several DNS server implementations. Based on our examination, we propose a formal model for analyzing the name dependencies inherent in DNS. Using our name dependency model we derive metrics to quantify the extent to which domain names affect other domain names. It is found that under certain conditions, more than half of the queries for a domain name are influenced by namespaces not expressly configured by administrators. This result serves to quantify the degree of vulnerability of DNS due to dependencies that administrators are unaware of. When we apply metrics from our model to production DNS data, we show that the set of domains whose resolution affects a given domain name is much smaller than previously thought. However, behaviors such as using cached addresses for querying authoritative servers and chaining domain name aliases increase the number and diversity of influential domains, thereby making the DNS infrastructure more vulnerable. 相似文献
9.
Influence of Grain Size on Ferroelastic Toughening and Piezoelectric Behavior of Lead Zirconate Titanate 总被引:1,自引:0,他引:1
Lead zirconate titanate specimens, at composition Zr48.9+- 1.0 / Ti51.1+-1.0 of grain sizes ranging from 0.5 to 15 (μm were prepared by hot pressing. The fracture toughness showed a 40% increase in the fine-grained specimens. Poling produced anisotropy in the fracture toughness. A tensor representation for the fracture toughness, now a function of the crack plane normal and the poling direction, is developed. The maximum and minimum values in the toughness tensor are shown to be related to the unpoled toughness by a simple phenomenological relationship. We also find that the piezoelectric coefficient, d33 , shows a slight increase for the fine-grained specimens, which is in conflict with the general view that smaller-grained materials can sustain vanishingly small values of spontaneous polarization. 相似文献
10.
The effect of the reaction conditions on the grafting parameters during grafting of 2‐acrylamido‐2‐methyl‐1‐propanesulfonic acid onto sodium carboxymethylcellulose using H2O2/Fe+2 redox pair are studied at 30°C. The grafting ratio, add on, and conversion initially increase with the H2O2 concentration in the range of (10.0–15.0) × 10?2 mol dm?3. Thereafter, these parameters decrease with the H2O2 concentration. The grafting ratio, add on, and conversion increase when increasing the ferrous ion concentration from (0.5 to 4.0) × 10?2 mol dm?3 and decrease with a further increase in the concentration. It is observed that the grafting ratio and add on increase with the monomer concentration, whereas the conversion decrease. The hydrogen ions seem to be facilitating the grafting reaction up to a certain concentration and after this concentration seem to be retarding the process. The grafting ratio, add on, and conversion decrease with the sodium carboxymethylcellulose concentration. When increasing the time period from 60 to 90 min, the grafting parameters increase but decrease thereafter. Similarly, when increasing the temperature from 25 to 30°C, the grafting parameters increase and decrease thereafter. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 4819–4825, 2006 相似文献