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排序方式: 共有84条查询结果,搜索用时 15 毫秒
1.
Chun Yang Yin Sharifah Aishah Syed Abdul KadirYing Pei Lim Sharifah Nawirah Syed-AriffinZurinawati Zamzuri 《Fuel Processing Technology》2008
Ash derived from combustion of Malaysian oil palm biomass (empty fruit bunches consisting of fibers) was physically and chemically characterized in order to provide a comprehensive understanding of its specific properties in terms of toxicity, compositions and reusability. Principal analyses conducted include particle size distribution, scanning electron microscopy, elemental dispersive X-ray, elemental analysis, toxicity characteristic leaching procedure (TCLP) as well as thermogravimetric, X-ray diffractometry and Fourier-transform infrared analyses. TCLP result indicated that the oil palm ash (OPA) should not be classified as toxic wastes in terms of heavy metal leachability since leachable copper, cadmium, lead and nickel concentrations were detected below the stipulated leachability limits. It was determined that the OPA contained high amount of potassium as well as presence of silica which implied its suitability to be reused as crude fertilizer or cement replacement material. 相似文献
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3.
Influence of polymer morphology on the adsorption behaviors of molecularly imprinted polymer‐methacrylic acid functionalized β‐cyclodextrin
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The influence of molecularly imprinted polymer‐methacrylic acid functionalized β‐cyclodextrin (MIP(MAA‐β‐CD)) morphology on the adsorption behavior studies towards benzylparaben (BzP) was explored. The effects of time, concentration, and temperature towards BzP uptake were extensively evaluated. The adsorption performance of MIP(MAA‐β‐CD) was compared with that on the molecularly imprinted polymer‐methacrylic acid (MIP(MAA)) synthesized without β‐CD. The MIP(MAA‐β‐CD) was synthesized to obtain a spherical and spongy‐porous texture with a broad pore size distribution. The MIP(MAA‐β‐CD) showed fast kinetic and the intra‐particle diffusion model demonstrated a three step (surface and pore) adsorption process. The Koble‐Corrigan isotherm was the most suitable model for data fitting, which indicated that MIP(MAA‐β‐CD) had homogeneous and heterogeneous surfaces. This finding clearly demonstrated that the large uptake and strong affinity of MIP(MAA‐β‐CD) did not only probably result from the monomer‐template interactions, but also due to the morphological MIP(MAA‐β‐CD) structure. In contrary to MIP(MAA‐β‐CD), MIP(MAA) synthesized with uniform morphology and narrow pore size distribution had lower adsorption capacities and its kinetic data fitted the pseudo‐second order diffusion model, indicating a two‐step (surface only) adsorption process. The MIP(MAA) adsorption process followed the Langmuir isotherm model referred to solely homogeneous uptake. The calculated thermodynamic parameters showed that the BzP uptake was exothermic, spontaneous, and physisorption process onto MIPs, which supported the results of kinetics and isotherm adsorption data. This study clearly revealed that the presence of β‐CD improved the morphology of synthesized MIP, and automatically enhanced the adsorption behavior of MIP. © 2015 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015 , 132, 42720. 相似文献
4.
Sharifah Syed-Abdullah Mike Holcombe Marian Gheorge 《Empirical Software Engineering》2006,11(1):143-167
This paper describes an empirical study, which addresses the aspect of well being amongst members of the software development
teams. The question of interest is whether an agile methodology has any distinct effect on the well being of the software
developers. Both quantitative and qualitative methods were utilised, including the participative observation, focus group
interviews, close-ended questionnaires and simple statistical tests such as Spearman Correlation and Mann–Whitney test. Initial
results showed that an agile methodology (XP) has a positive effect on the level of enthusiasm of the software developers
in the most dynamic project. To understand why XP can increase enthusiasm, results are interpreted with references to cognitive,
affective and managerial properties of the practices studied. This result needs further investigation on the individual effects
of each practice on the wellbeing and attitudes of Software Engineering (SE) teams. 相似文献
5.
Wan Norlinda Roshana Mohd Nawi Sharifah Rafidah Wan Alwi Zainuddin Abdul Manan Jiří Jaromír Klemeš 《Clean Technologies and Environmental Policy》2016,18(6):1769-1777
There has been growing interests to reduce the environmental impact caused by greenhouse gas emissions from process plants through various energy conservation strategies. CO2 emissions are closely linked to energy generation, conversion, transmission and utilisation. Various studies on the design of energy-efficient processes, optimal mix of renewable energy and hybrid power system are driven to reduce reliance on fossil fuel as well as CO2 emissions reduction. This paper presents a systematic technique in the form of graphical visualisation tool for cost-effective CO2 emission reduction strategies in industry. The methodology is performed in four steps. The first step involves calculating the energy consumption of a process plant. This is followed by identification of potential strategies to reduce CO2 emissions using the CO2 management hierarchy as a guide. In the third step, the development of “Investment” versus “CO2 Reduction” (ICO2) plot is constructed to measure the optimal CO2 emission reductions achieved from the implementation of possible CO2 reduction strategies. The Systematic Hierarchical Approach for Resilient Process Screening (Wan Alwi and Manan in AIChE J 11:3981–3988, 2006) method is used in the fourth step via substitution or partial implementation of the various CO2 reduction options in order to meet the cost-effective emission reduction within the desired investment limit or payback period (PP). An illustrative case study on a palm oil refinery plant has been used to demonstrate the implementation of the method in reduction of CO2 emissions. The developed graphical tool provides an insight-based approach for systematic CO2 emission reduction in the palm oil refinery considering both heat and power energy sources. Result shows that 31.2 % reduction in CO2 emissions can be achieved with an investment of USD 38,212 and PP of 10 months based on the present energy prices in Malaysia. 相似文献
6.
Mohamad S Surikumaran H Raoov M Marimuthu T Chandrasekaram K Subramaniam P 《International journal of molecular sciences》2011,12(9):6329-6345
This study focuses on the synthesis and characterization of the inclusion complex of β-Cyclodextrin (β-CD) with dicationic ionic liquid, 3,3'-(1,4-Phenylenebis [methylene]) bis(1-methyl-1H-imidazol-3-ium) di(bromide) (PhenmimBr). The inclusion complex was prepared at room temperature utilizing conventional kneading technique. Proton ((1)H) NMR and 2D ((1)H-(1)H) COSY NMR were the primary characterization tools employed to verify the formation of the inclusion complex. COSY spectra showed strong correlations between protons of imidazolium and protons of β-CD which indicates that the imidazolium ring of PhenmimBr has entered the cavity of β-CD. UV absorption indicated that β-CD reacts with PhenmimBr to form a 2:1 β-CD-PhenmimBr complex with an apparent formation constant of 2.61 × 10(5) mol&(-2) L(2). Other characterization studies such as UV, FT-IR, XRD, TGA, DSC and SEM studies were also used to further support the formation of the β-CD-PhenmimBr inclusion complex. 相似文献
7.
Ahmad M. Rateb Sharifah K. S. Yusof 《International Journal of Communication Systems》2015,28(3):546-559
Compressed sensing is an emerging technique in the field of digital signal acquisition. It promises almost exact recovery of high‐dimensional signals from a very small set of measurements. However, this technique is challenged by the task of recovering signals immersed in noise. In this paper, we derive upper and lower bounds on mean squared recovery error of noisy signals. These bounds are valid for any number of acquired measurements and at any signal‐to‐noise ratio. This work is highly useful for the design of any compressed sensing‐based real world application by quantifying recovery error entailed with realistic digital signal acquisition scenarios. Copyright © 2013 John Wiley & Sons, Ltd. 相似文献
8.
Effect of the activation procedure on the performance of Mo/H-MFI catalysts for the non-oxidative conversion of methane to aromatics 总被引:1,自引:0,他引:1
Sharifah B. Derouane-Abd Hamid J. Ross Anderson Iver Schmidt Christophe Bouchy Claus J. H. Jacobsen Eric G. Derouane 《Catalysis Today》2000,63(2-4):461-469
The effect of pre-treatment on the performance of Mo/H-MFI zeolite catalysts applied to the non-oxidative conversion of methane to aromatics has been investigated. It is demonstrated that catalyst performance depends on activation conditions. Activation of the Mo-oxide/H-MFI precursor with an n-butane/hydrogen mixture results in higher catalyst stability and benzene selectivity which are tentatively attributed to the formation of the -MoC1−x carbide, with f.c.c. structure as revealed by XRD. 相似文献
9.
Syed Adnan Ali Shah Huey Ling Tan Sadia Sultan Muhammad Afifi Bin Mohd Faridz Mohamad Azlan Bin Mohd Shah Sharifah Nurfazilah Munawar Hussain 《International journal of molecular sciences》2014,15(7):12027-12060
Microbial-catalyzed biotransformations have considerable potential for the generation of an enormous variety of structurally diversified organic compounds, especially natural products with complex structures like triterpenoids. They offer efficient and economical ways to produce semi-synthetic analogues and novel lead molecules. Microorganisms such as bacteria and fungi could catalyze chemo-, regio- and stereospecific hydroxylations of diverse triterpenoid substrates that are extremely difficult to produce by chemical routes. During recent years, considerable research has been performed on the microbial transformation of bioactive triterpenoids, in order to obtain biologically active molecules with diverse structures features. This article reviews the microbial modifications of tetranortriterpenoids, tetracyclic triterpenoids and pentacyclic triterpenoids. 相似文献
10.
Hemavathy Surikumaran Sharifah Mohamad Norazilawati Muhamad Sarih 《International journal of molecular sciences》2014,15(4):6111-6136
This work describes methacrylic acid functionalized β-cyclodextrin (MAA-βCD) as a novel functional monomer in the preparation of molecular imprinted polymer (MIP MAA-βCD) for the selective removal of 2,4-dichlorophenol (2,4-DCP). The polymer was characterized using Fourier Transform Infrared (FTIR) spectroscopy, Brunauer-Emmett-Teller (BET) and Field Emission Scanning Electron Microscopy (FESEM) techniques. The influence of parameters such as solution pH, contact time, temperature and initial concentrations towards removal of 2,4-DCP using MIP MAA-βCD have been evaluated. The imprinted material shows fast kinetics and the optimum pH for removal of 2,4-DCP is pH 7. Compared with the corresponding non-imprinted polymer (NIP MAA-βCD), the MIP MAA-βCD exhibited higher adsorption capacity and outstanding selectivity towards 2,4-DCP. Freundlich isotherm best fitted the adsorption equilibrium data of MIP MAA-βCD and the kinetics followed a pseudo-second-order model. The calculated thermodynamic parameters showed that adsorption of 2,4-DCP was spontaneous and exothermic under the examined conditions. 相似文献