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Nor?Azowa?IbrahimEmail author Faraj?Abu-Ilaiwi Mohamad?Zaki?Ab.?Rahman Mansor?B.?Ahmad Khairul?Zaman?M.?Dahlan Wan?Md?Zin?Wan?Yunus 《Journal of Polymer Research》2005,12(3):173-179
Grafting of acrylamide (AAm) onto oil palm empty fruits bunch fiber using hydrogen peroxide as initiator and methyl acrylate as comonomer was investigated. The amount of comonomer needed to make grafting of acrylamide possible was determined. The percentage of poly(acrylamide) and the comonomer in the final graft copolymer was estimated by elemental analysis. Results obtained indicated that methyl acrylate facilitated the incorporation of acrylamide monomer onto OPEFB. The reactivity ratios for both monomers were determined by using Fineman–Ross plot. The effects of reaction temperature and period as well as amount of the initiator, solvent, monomer and comonomer on the percentage of grafting at fixed amount of comonomer (11 mmol) were studied. Maximum percentage of grafting was achieved when the amount of initiator and solvent 3.98×10−3 mol and 50 mL respectively. The optimum reaction temperature was 50 ○C and the reaction period was 90 min. Highest percentage of grafting was 232% when 25.6 mmol of acrylamide was used under these optimum conditions. The presence of functional group in the grafted polymer is characterized by infrared spectroscopy and the surface morphology is observed by scanning electron microscopy. Thermoanalytic investigation on OPEFB and OPEFB-g-PAAM were carried out to evaluate the thermal stability and respective activation energy of the materials. 相似文献
3.
Khamirul Amin Matori Loy Chee Wah Mansor Hashim Ismayadi Ismail Mohd Hafiz Mohd Zaid 《International journal of molecular sciences》2012,13(12):16812-16821
We report on a recycling project in which α-Al2O3 was produced from aluminum cans because no such work has been reported in literature. Heated aluminum cans were mixed with 8.0 M of H2SO4 solution to form an Al2(SO4)3 solution. The Al2(SO4)3 salt was contained in a white semi-liquid solution with excess H2SO4; some unreacted aluminum pieces were also present. The solution was filtered and mixed with ethanol in a ratio of 2:3, to form a white solid of Al2(SO4)3·18H2O. The Al2(SO4)3·18H2O was calcined in an electrical furnace for 3 h at temperatures of 400–1400 °C. The heating and cooling rates were 10 °C/min. XRD was used to investigate the phase changes at different temperatures and XRF was used to determine the elemental composition in the alumina produced. A series of different alumina compositions, made by repeated dehydration and desulfonation of the Al2(SO4)3·18H2O, is reported. All transitional alumina phases produced at low temperatures were converted to α-Al2O3 at high temperatures. The X-ray diffraction results indicated that the α-Al2O3 phase was realized when the calcination temperature was at 1200 °C or higher. 相似文献
4.
Engineering with Computers - Vast research works implementing feature-based technology have successfully been devoted. However, work on recognition of revolved regular-freeform surfaces is still... 相似文献
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Ismayadi Ismail Mansor Hashim Khamirul Amin Matori Rosidah Alias Jumiah Hassan 《Journal of Superconductivity and Novel Magnetism》2012,25(1):71-77
In this paper the effect of sintering temperature on Ni0.5Zn0.5Fe2O4 is examined closely. The evolution of toward magnetically ordered materials was to be tracked with the parallel evolving
microstructure subjected to sintering temperatures in an ascending order. The starting powder of Ni0.5Zn0.5Fe2O4 was prepared via mechanical alloying and later molded into toroidal samples. After each sintering, we observed the resulting
changes in the materials. The XRD data showed a single phase being formed as early as 600 °C and the peak intensity was increasing
with the sintering temperature indicating an increase in the degree of crystallinity. The BH hysteresis loops showed the evolution
from paramagnetism to moderate ferromagnetism to strong ferromagnetism with microstructural changes. For lower sintering temperatures,
the samples showed paramagnetic behavior dominating the samples. As sintering temperature increased, paramagnetic states decreased
and, at 900 °C, a moderately ferromagnetic state appeared. Sintering at 1000 °C produced a strongly ferromagnetic state giving
a well-formed sigmoid-shape hysteresis loop. 相似文献
7.
I. E. Samy M. Shattri B. K. H. Bujang R. M. Ahmed I. Sharharin 《International journal of remote sensing》2013,34(10):3176-3196
Subsurface geological fractures in karst terrain are often associated with unpredictable environmental and geotechnical engineering problems. This requires precise mapping and an understanding of the distribution of geological fractures on multi-scales. To extract and investigate surface and subsurface geological fractures on such scales, multi-scales, this study presents two approaches. The first involves geological prediction and visual interpretation of terrain parameters using a digital elevation model (DEM). The second is an automatic detection method using a topographical fabric algorithm that uses a DEM to create a map of ridges, which represent the footwalls of geological fractures, and valleys (channels), which reflect geological fracture zones. Unlike wavelet analysis and the Fourier transform, which use optical remote-sensing images, the integration of visual interpretation and a topographical fabric algorithm is capable of the extraction and spatial correlation of subsurface geological fractures. This method was applied to Kuala Lumpur limestone bedrock in Malaysia, by focusing on the adjacent mountainous areas and the geometries of ex-opencast mining ponds. The spatial correlation of the extracted surface geological fractures was clarified by rose diagrams and semivariogram models. Spatial correlation shows that the Malaysian peninsula, surface and subsurface geological fractures and the geometry of ex-opencast mining ponds share similar trends. The results obtained using this methodology is compared to those of subsurface geological fractures reported by means of geophysical surveying and field investigation. This proposed method may be useful for mapping geological fractures in areas of high soil moisture, where geophysical surveying is difficult and/or not available, and is also highly applicable in other parts of Malaysia or Southeast Asia, permitting a better understanding of the geotectonics and geotechnical engineering setting of the study area. 相似文献
8.
Noraini Nordin Samikannu Kanagesan Nur Rizi Zamberi Swee Keong Yeap Nadiah Abu Subramani Tamilselvan Mansor Hashim Noorjahan Banu Alitheen 《IET nanobiotechnology / IET》2017,11(3):343
In this study, nanocrystalline magnesium zinc ferrite nanoparticles were successfully prepared by a simple sol–gel method using copper nitrate and ferric nitrate as raw materials. The calcined samples were characterised by differential thermal analysis/thermogravimetric analysis, Fourier transform infrared spectroscopy and X‐ray diffraction. Transmission electron microscopy revealed that the average particle size of the calcined sample was in a range of 17–41 nm with an average of 29 nm and has spherical size. A cytotoxicity test was performed on human breast cancer cells (MDA MB‐231) and (MCF‐7) at various concentrations starting from (0 µg/ml) to (800 µg/ml). The sample possessed a mild toxic effect toward MDA MB‐231 and MCF‐7 after being examined with MTT (3‐[4, 5‐dimethylthiazol‐2‐yl]‐2, 5 diphenyltetrazolium bromide) assay for up to 72 h of incubation. Higher reduction of cells viability was observed as the concentration of sample was increased in MDA MB‐231 cell line than in MCF‐7. Therefore, further cytotoxicity tests were performed on MDA MB‐231 cell line.Inspec keywords: sol‐gel processing, nanoparticles, nanofabrication, magnesium compounds, zinc compounds, toxicology, biological organs, cancer, cellular biophysics, nanomedicine, calcination, differential thermal analysis, Fourier transform infrared spectra, X‐ray diffraction, transmission electron microscopy, particle size, organic compoundsOther keywords: sol‐gel method, cytotoxic effects, breast cancer cell line, MDA MB‐231 in vitro, nanocrystalline magnesium zinc ferrite nanoparticles, copper nitrate, ferric nitrate, raw materials, calcined samples, differential thermal analysis, thermogravimetric analysis, Fourier transform infrared spectroscopy, X‐ray diffraction, transmission electron microscopy, average particle size, cytotoxicity testing, human breast cancer cells, mild toxic effect, 3‐[4,5‐dimethylthiazol‐2‐yl]‐2,5 diphenyltetrazolium bromide) assay, cell viability, MCF‐7, MDA MB‐231 cell line, size 17 nm to 41 nm 相似文献
9.
The present paper illustrates the development of generative surface recognition for regular and freeform. To obtain the final form of product, material removal volume generation from a stock model is also discussed. Only a few studies integrated the regular and freeform surfaces to provide a comprehensive definition of surface recognition as well as for the volumetric estimation of removal material in finishing and roughing operations. The current research deploys a comprehensive surface recognition approach that can recognise both regular and freeform surfaces based on the geometry as well as loop entity of a face. In contrast to the regular surface that can be categorised into a particular group of geometrical shape, such as cylindrical shape, the proposed approach enables the recognition of a freeform surface that cannot be defined as a generic geometrical shape. In addition, the new method also simplifies the existing surface recognition for regular surfaces. The material removal volumes created consist of machining volumes for finishing and roughing operations needed to be machined to obtain the final form of the product. The present research provides a unique user customisation feature that enables user to specify the volumetric thickness for material removal volume in the finishing operation as well as the size for the stock model. These estimated volumes are prepared for subsequent manufacturing applications, such as sequencing of machining operation. 相似文献
10.
Alireza Hamedianfar Shattri Mansor Noordin Ahmad 《International journal of remote sensing》2013,34(5):1876-1899
Urbanization is commonly accepted as an important contributor to the growth of man-made structures and as a rapid convertor of natural environments to impervious surfaces. Roofs are one class of impervious surface whose materials can highly influence the quality of urban surface water. In this study, two data sources, WorldView-2 (WV-2) imagery and a combination of WV-2 and lidar data, were utilized to map intra-urban targets, with 13 classes. Images were classified using object-based image analysis. Pixel-based classifications using the support vector machine (SVM) and maximum likelihood (ML) methods were also tested for their abilities to use both lidar data and WV-2 imagery. ML and SVM classifications yielded overall accuracies of 72.46% and 75.69%, respectively. The results of these classifiers exhibited mixed pixels and salt-and-pepper effects. Spectral, spatial, and textural attributes as well as various spectral indices were employed in the object-based classification of WV-2 imagery. Feature classification of WV-2 imagery resulted in 85% overall accuracy. Lidar data were added to WV-2 imagery to assist in the spatial and spectral diversities of urban infrastructures. Classified image made from WV-2 imagery and lidar data achieved 92.84% overall accuracy. Rule-sets of these fused datasets effectively reduced the spectral variation and spatial heterogeneities of intra-urban classes, causing finer boundaries among land-cover classes. Therefore, object-based classification of WV-2 imagery and lidar data efficiently improved detailed characterization of roof types and other urban surface materials. 相似文献