有源电光调制式高功率瞬态电场传感器的研制

瞬态电场防护及应用技术的研究离不开瞬态电场测试系统;文中基于有源电光调制法,研制了一种高功率瞬态电场传感器;通过建立该传感器的等效电路模型,并借助CST仿真建模,分别从频域和时域角度分析了传感器的接收特性,并得到了一致的结果;最后利用脉冲噪声模拟器和吉赫兹横电磁波小室对研制的传感器性能进行了测试;结果表明:接收天线为单极子天线,天线负载采用高阻时响应电压与被测电场场强成正比;研制的传感器带宽为10kHz～314MHz,可用于纳秒级高功率瞬态电场的时域测试。     

基于径向基的瓦斯涌出量灰色预测模型

为了进一步预防煤层瓦斯突出,实现准确、快速预测煤矿瓦斯涌出量的大小,首先采用1-AGO对样本数据进行处理,建立灰色(GM)预测模型,再利用径向基(RBF)神经网络对灰色预测模型结果进行预测,以作为其最终的预测值;采用阜新煤矿某工作面瓦斯涌出量的历史数据进行建模,实验结果表明,GM-RBF组合模型在预测精度及训练误差方面均优于单一的GM模型和RBF神经网络预测模型;算法计算简便,减弱了数据的随机性及模型误差,煤矿瓦斯涌出量的预测平均误差减小到1.57%。     

基于混沌序列的跳频信号源FPGA设计与实现

提出了一种基于混沌序列的跳频信号源的设计及硬件实现方法;该方法基于FPGA技术,以Logistic混沌映射电路作为跳频序列发生器,以直接数字频率合成器作为跳频信号源的基础;在FPGA上完成数字频率合成,并利用高性能的AD9777实现数模转换;实验测试结果表明,该信号源在2MHz～32MHz频率范围内,实现了16个频点的跳变频率且性能良好,能够满足实际工程的需要。     

PVP-assisted Sn-Ti microspheres for the efficient B–V oxidation of cyclohexanone

Journal of Porous Materials - New Sn-Ti microspheres were first successfully synthesized by a PVP-assisted sol-gel method in this paper, and their performance in the B–V oxidation of...     

Preparation of Iron Filler-Based Photocomposites and Application in 3D Printing

The introduction of metallic fillers to polymers via the photopolymerization approach can endow the composite materials with some unique properties, but the relevant research is still scarce due to the issue of light penetration and inner filter effect. Herein, for the first time the fabrication of photocomposites based on fine iron powder (i.e., a typical kind of metallic filler) is reported in this work. The free radical polymerization of two different acrylate monomers, poly(ethylene glycol) diacrylate and trimethylolpropane triacrylate, is performed in the presence of iron filler under mild conditions (i.e., light emitting diode (LED)@405 nm irradiation at room temperature under air). And the real-time Fourier transform infrared spectroscopy reveals remarkable photopolymerization kinetics of acrylates with high final conversions and fast polymerization rates despite the increasing contents of iron filler in the composites. Interestingly, the 3D printing technique is applied to the iron filler-based composites to produce tridimensional patterns with excellent spatial resolution. This work not only paves the way for the investigation of photocomposites based on metallic fillers through photochemical methods, but also broadens the potential application prospects.     

BiOI/g-C3N4光催化降解甲基橙研究

以三聚氰胺为前驱物采用热聚合法制备了石墨相氮化碳（g-C₃N₄）,并在其表面原位合成了碘氧化铋（BiOI）,构筑了石墨相氮化碳-碘氧化铋复合材料。采用X射线衍射仪（XRD）、傅里叶变换红外光谱仪（FT-IR）、紫外可见漫反射仪（UV-Vis-DRS）等对催化剂进行了表征。结果表明,当BiOI与g-C₃N₄物质的量比为0.5时,BiOI/g-C₃N₄催化剂具有高分散的BiOI颗粒及适中的禁带宽度,吸附和降解甲基橙性能最佳。回流温度为120 ℃时制备的BiOI/g-C₃N₄催化剂具有适中的粒径、比表面积和表面羟基浓度,吸附和降解甲基橙性能最佳,且该催化剂具有良好的重复使用性能。     

New approach for the preparation of nanoporous polyorganosilicate low‐k films

The distribution of pores and the mechanical properties of materials are the key factors in preparing satisfactory low‐k films. In the present study, a kind of silsesquioxane‐polyethylene glycol (SSQ‐PEG) was synthesized and used as a template to make the distribution of pores more even in the low‐k films. The crosslinking density of films could be adjusted by the sol‐gel of tetramethoxysilane/dimethoxydimethylsilane with various proportions. The porosity of films could also be adjusted with different proportions of pendant PEG chains introduced. A dielectric constant as low as 2.1 had been achieved for nanoporous polyorganosilicate films with good tenacity. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 1238–1243, 2007     

灞河流域气候因子对水沙变化的影响

利用灞河流域蓝田气象站和马渡王水文站1960—2012年的气象、水文实测资料,分析灞河流域气候及水沙变化规律,同时运用相关性分析、灰色关联分析、多元线性回归模型等多种方法探讨了该流域水沙变化与气候变化的关系。结果表明:灞河流域降雨量、蒸发量、径流量和输沙量皆呈显著下降趋势,而气温呈上升趋势;降雨量与水沙都有重要的相关关系,1960—1990年影响径流量的气候因子敏感度由大至小依次为降雨量、气温、蒸发量,而1991—2012年则为降雨量、蒸发量、气温,当气温和蒸发量不变时,降雨量每增加1 mm,两阶段的年径流量分别增加0.14亿m3和0.08亿m3;1960—2012年影响输沙量的气候因子敏感度由大至小依次为降雨量、气温、蒸发量,当气温和蒸发量不变时,降雨量每增加1 mm,年输沙量增加0.668万t。     

Phase Relations in the System Al2O3–B2O3–Nd2O3

The phase relations at a temperature below "subsolidus" in the system Al₂O₃–B₂O₃–Nd₂O₃ are reported. Specimens were prepared from various compositions of Al₂O₃, B₂O₃, and Nd₂O₃ of purity 99.5%, 99.99%, and 99.9%, respectively, and fired at 1100°C. There are six binary compounds and one ternary compound in this system. The ternary compound, NdAl₃(BO₃)₄ (NAB), has a phase transition at 950°C ± 15°C. The high-temperature form of NAB has a second harmonic generation (SHG) efficiency of KH₂PO₄ (KDP) of the order of magnitude of the form which has been used as a good self-activated laser material, and the low-temperature form of NAB has no SHG efficiency.     

用RT5370模块实现的低成本嵌入式WiFi系统

介绍了在嵌入式系统上支持USB接口的WiFi模块RT5370的软硬件方案及其具体的移植实现。基于该方案,实现了智能手机通过WiFi遥控小车的控制系统。试验表明,低成本嵌入式WiFi是可行的,从而为当前热门的嵌入式系统采用WiFi探索了低成本的解决方案。