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将铝电解干式防渗料用于稀土熔盐电解试验,该干式防渗料能阻止电解质中LiF的渗透但不能阻挡LaF3的渗透。以铝电解用干式防渗料为基体,通过添加CaO、MgO、La2O3、Fe2O3和SiC等成分进行改性,研究改性后的防渗料的防渗效果。结果表明,添加CaO、La2O3或MgO,会加快稀土熔盐对防渗料的腐蚀破坏,但添加Fe2O3或SiC的防渗料有较好的防渗性能,而同时添加Fe2O3和SiC的干式防渗料效果最好。 相似文献
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研究了LiF-LaF3体系下,以La-Ni合金和La金属作可溶性阳极,以Ta为阴极,熔盐电解精炼镧过程中不同工艺条件对槽电压、沉积物形貌、产物杂质含量的影响。采用扫描电镜(SEM)对电解精炼所得La沉积物形貌进行观察,采用电感耦合等离子体质谱法(ICP-MS),辉光放电质谱法(GD-MS),高频燃烧-红外法与惰气脉冲-红外热导法进行最终产品金属La的成分分析。结果表明:槽压与电流之间的线性关系受到接触压降、熔盐性质等因素的影响,控制较高电解温度、使用La-Ni合金代替金属La作阳极时槽压较低;沉积物均为枝晶形貌,电流密度增大导致沉积物的形貌由三维多面体转变为二维片状,电解温度升高导致颗粒几何规则性减弱,低电流密度下沉积物生长机制应为阶梯状生长;金属杂质中W,Ta可由50~100μg·g-1降至2~3μg·g-1,使用La阳极的实验所得精炼产物金属镧纯度为99.867%(分析77个杂质元素)。 相似文献
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DES(Data encryption standard)是ISO颁布的数据加密标准,通过对DES算法的分析,提出了用DSP实现数据加密标准算法,通过循环或迭代,将简单的基本运算(如左移、右移、模2加法等)和变换(选择函数、置换函数)构造成数据流的非线性变换(加密变换或解密变换),从而实现对计算机数据进行密码保护.DSP快速运算有利于数据加密、解密和数据的传输. 相似文献
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本文对1Cr11MoV静叶片钢进行了冷轧变形的研究。确定了宽展面积与压缩面积的关系,各道次的宽展面积与压缩面积比值,宽展与压下量的关系,以及压下量沿轧件宽向的分布。为选择坯料外形和尺寸,孔型设计以及制定压下制度提供依据。 相似文献
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Multimedia Tools and Applications - In this paper, a simple method was demonstrated to fabricate polydimethylsiloxane (PDMS) microfluidic chips used in rapid diagnosis based on printing the liquid... 相似文献
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Compared to conventional Mg-Al and Mg-Zn system magnesium alloys, the Mg-Zn-Y-Zr heat-resistant alloy exhibits high thermal stability due to the addition of Y earth element, which is an ideal candidate for producing high strain rate superplasticity (HSRS, strain rate >= 1 x 10(-2) s(-1)). Recently, the HSRS of Mg-Zn-Y-Zr alloy was achieved by friction stir processing (FSP), because the FSP resulted in the generation of fine and equiaxed recrystallized grains and fine and homogeneous second phase particles. However, the study on superplastic deformation mechanism of FSP Mg-Zn-Y-Zr alloy at various parameters is limited relatively. Therefore, at the present work, six millimeters thick as-extruded Mg-Zn-Y-Zr plates were subjected to FSP at relatively wide heat input range of rotation rates of 800 r/min to 1600 r/min with a constant traverse speed of 100 mm/min, obtaining FSP samples consisting of homogeneous, fine and equiaxed dynamically recrystallized grains and fine and uniform Mg-Zn-Y ternary phase (W-phase) particles. With increasing rotation rate, within the FSP samples the W-phase particles were broken up and dispersed significantly and the recrystallized grains were refined slightly, while the fraction ratio of the high angle grain boundaries (grain boundaries misorientation angle >= 15 degrees) was increased obviously. Increasing rotation rate resulted in an increase in both optimum strain rate and superplastic elongation. For the FSP sample obtained at 1600 r/min, a maximum elongation of 1200% was achieved at a high-strain rate of 1x10(-2) s(-1) and 450 degrees C. Grain boundary sliding was identified to be the primary deformation mechanism in the FSP samples at various rotation rates by superplastic data analyses and surfacial morphology observations. Furthermore, the increase in rotation rate accelerated superplastic deformation kinetics remarkably. For the FSP sample at 1600 r/min, superplastic deformation kinetics is in good agreement with the prediction by the superplastic constitutive equation for fine-grained magnesium alloys governed by grain boundary sliding mechanism. 相似文献