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排序方式: 共有135条查询结果,搜索用时 15 毫秒
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Antonio M. Locci Roberto Orrù Giacomo Cao Zuhair A. Munir 《Journal of the American Ceramic Society》2006,89(3):848-855
The simultaneous synthesis and densification of dense TiC–TiB2 composite has been investigated starting from Ti, B4 C, and C as reactants, and using the spark plasma sintering (SPS) technique. The optimal conditions for complete conversion of the reactants to the composite were determined for different applied DC current levels. A kinetic investigation performed allows us to conclude that solid-state diffusion is the mechanism governing the synthesis process. It is seen that TiC is the first phase formed, while TiB2 formation occurs afterward. Two intermediate boride phases, i.e. TiB and Ti3 B4 , are also formed but, as the SPS holding time was augmented, they were gradually and completely converted to TiB2 . Moreover, it is found that in order to reach relatively high dense products, an electric current needs to be applied for time intervals longer than those required for obtaining complete conversion. A pure dense product (relative density ∼98%) was obtained when an electric pulsed current of 1100 A and a mechanical pressure of 20 MPa were applied for about 4 min. 相似文献
4.
Local-strain and linear-elastic fracture-mechanics (LEFM) methodologies have been investigated for prediction of the corrosion-fatigue
life of notched components of specially developed Al-2.5Mg alloys exposed to Arabian Gulf seawater environment. Corrosion-fatigue
crack initiation life estimates were obtained using strain-life relationships; corrosion-fatigue crack propagation life estimates
were obtained using LEFM relationships. The total corrosion-fatigue life was considered to be the sum of the crack initiation
and crack propagation lives. Estimated corrosion-fatigue lives were compared with experimentally obtained corrosion-fatigue
life data using center-notched specimens of three types of Al-2.5Mg alloys (containing different amounts of chromium) exposed
to Arabian Gulf seawater environment. Two notch geometries, a circular notch (K
t= 2.42) and an elliptical notch (K
t= 4.2), were investigated. Good corrosion-fatigue life predictions can be obtained using local-strain and LEFM methodologies
by determining the relevant material constants via a few simple fatigue tests on smooth specimens and a few crack-growth-rate
tests in the environment at the frequency of interest. 相似文献
5.
Experimental and modeling results on the field-activated combustion synthesis (FACS) of Nb5 Si3 are reported. In the absence of an electric field and without reactant preheating, Nb5 Si3 cannot be prepared by self-propagating high-temperature synthesis (SHS). Under the influence of a field a self-sustaining combustion wave is established whose rate of propagation decreases with traveled distance. For relatively low field values, the wave propagation mode changes from a continuous (smooth) to a spin mode. The product of synthesis depends on the mode of propagation. Synthesis during continuous wave propagation results in the formation of Nb5 Si3 , primarily in the α-modification. In contrast, when the wave propagates in a spin mode, the product is NbSi2 with unreacted niobium. The present observations demonstrate a case where the field effect is not localized, as was the case in previous studies. The difference in behavior is attributed to differences in the electrical conductivities of the product phases. 相似文献
6.
Sawsan A. Rahimuddin Samir M. Khoja Marzoki M. Zuhair Nazlin K. Howell Jonathan E. Brown 《European Journal of Lipid Science and Technology》2007,109(7):647-655
Ultraviolet A (UVA) radiation causes oxidative damage to human skin cells. This damage may be reduced or prevented using plant compounds as photoprotectants. To investigate the relationship between chemical structure and UVA‐protective activity, three structurally related flavonoids, namely luteolin, luteolin‐7‐O‐glucoside (both present in artichoke) and luteolin‐4'‐O‐glucoside (present in wild carrot), were studied. Human skin fibroblasts exposed to UVA (250 and 500 kJ/m2) were treated with each flavonoid (30 µM) for 18 h prior to irradiation. The extent of lipid peroxidation in the cellular extracts was assessed as lipid peroxides and malondialdehyde (MDA). Luteolin and luteolin‐7‐O‐glucoside both prevented a significant increase in lipid peroxides at 250 kJ/m2, but at 500 kJ/m2 their effectiveness was clearly attenuated. Contrastingly, luteolin‐4'‐O‐glucoside was pro‐oxidant at both radiation doses. Measurements of MDA levels highlighted that luteolin was clearly more effective than the two glucosides at both 250 and 500 kJ/m2. Overall, these results show clear differences between the three flavonoids and suggest that the B ring 3',4'‐dihydroxy group, lacking in luteolin‐4'‐O‐glucoside, may be particularly important. Flavonoid: transition metal ion chelation studies confirmed the influence of the 3',4'‐dihydroxy group, which is also relevant to the quenching of singlet oxygen. These features as well as the greater lipophilic nature of luteolin together explain the superior activity of this flavonoid which may be potentially useful as a supplement in photoprotective skin preparations. 相似文献
7.
Yasuhiro Kodera Takeshi Yamamoto Naoki Toyofuku Manshi Ohyanagi Zuhair A. Munir 《Journal of Materials Science》2006,41(3):727-732
The ordering of stacking-disordered silicon carbide prepared from the elements by high energy ball milling was investigated
during sintering. A sharp increase in density in the temperature region 1700–1800°C was associated with a decrease in the
disorder. Samples which had low disorder density showed a more continuous sintering behavior with temperature. Highly dense
(up to 99% relative density) SiC can be obtained at 1900°C under a pressure of 70 MPa with no hold time. Similar results were
observed for structurally disordered carbon with 10 at% of boron. The sintering behavior exhibited an abrupt density increase
in the narrow temperature region of 1450–1600°C and was associated with disorder-order transformation. 相似文献
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9.
Sagir Adamu Abdul-Rashid Bawah Oki Muraza Zuhair Malaibari Mohammad M. Hossain 《加拿大化工杂志》2020,98(11):2425-2434
Dry (CO2) reforming of methane is conducted over two newly synthesized Ni20/Ce-γAl2O3 and Ni20/Ce-meso-Al2O3 catalysts. The x-ray diffraction (XRD) patterns indicated that Ni20/Ce-meso-Al2O3 exhibits a better dispersion of nickel, while Ni20/Ce-γAl2O3 has larger amounts of nickel crystallites. The temperature programmed desorption (TPD) kinetics analysis indicated that Ni20/Ce-meso-Al2O3 had a lesser metal-support interaction than the Ni20/Ce-γAl2O3. The thermal gravimetric analysis (TGA) indicated that the incorporation of ceria into the Al2O3 matrix helps to stabilize Ni20/Ce-meso-Al2O3 during dry reforming of methane. The temperature programmed reduction (TPR) indicated that the synthesized catalysts were sufficiently reducible below 750 °C. A fixed bed reactor evaluation (at 750 °C) showed that both catalysts can facilitate methane reforming to syngas with minimal coking throughout the 30 hours time-on-stream (TOS). However, Ni20/Ce-meso-Al2O3 is more promising in terms of prolonged stability for dry reforming applications. Moreover, the syngas yield for Ni20/Ce-γAl2O3 is close to equilibrium prediction during the first 1 hour of reaction time. 相似文献
10.
Nawaf N. Hamadneh Waqar A. Khan Waqar Ashraf Samer H. Atawneh Ilyas Khan Bandar N. Hamadneh 《计算机、材料和连续体(英文)》2021,66(3):2787-2796
In this study, we have proposed an artificial neural network (ANN) model to estimate and forecast the number of confirmed and recovered cases of COVID-19 in the upcoming days until September 17, 2020. The proposed model is based on the existing data (training data) published in the Saudi Arabia Coronavirus disease (COVID-19) situation—Demographics. The Prey-Predator algorithm is employed for the training. Multilayer perceptron neural network (MLPNN) is used in this study. To improve the performance of MLPNN, we determined the parameters of MLPNN using the prey-predator algorithm (PPA). The proposed model is called the MLPNN–PPA. The performance of the proposed model has been analyzed by the root mean squared error (RMSE) function, and correlation coefficient (R). Furthermore, we tested the proposed model using other existing data recorded in Saudi Arabia (testing data). It is demonstrated that the MLPNN-PPA model has the highest performance in predicting the number of infected and recovering in Saudi Arabia. The results reveal that the number of infected persons will increase in the coming days and become a minimum of 9789. The number of recoveries will be 2000 to 4000 per day. 相似文献