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1.
The extraction of Te(IV) from aqueous solutions containing various ligands was studied using various inert organic diluents
and other solvents. The extraction was carried out from solutions of various mineral (HCl, HBr, HI, HNO3) and organic (citric, oxalic) acids of various concentrations. The organic phase was an inert diluent (cyclohexane, CCl4, chloroform, benzene, p-xylene, toluene, nitrobenzene) or a solution of 20 vol % Aliquat-336, 20 vol % trioctylamine, or 30 vol % TBP in p-xylene. A correlation between the distribution of Te(IV) and some physicochemical properties of the diluents and the possibility
of extraction separation radioactive Te isotopes and their daughters, i.e., radioactive I isotopes, were examined. In most
cases, the Te(IV) distribution ratio decreases in the order nitrobenzene > CHCl3 > CCl4 > p-xylene > benzene > toluene > cyclohexane.
Published in Russian in Radiokhimiya, 2007, Vol. 49, No. 4, pp. 353–358.
The text was submitted by the authors in English.
An erratum to this article is available at . 相似文献
2.
Khaled Metwally Laurent Robert Samuel Queste Bernard Gauthier-Manuel Chantal Khan-Malek 《Microsystem Technologies》2012,18(2):199-207
Microfluidics on foil is gaining momentum due to a number of advantages of employing thin films combined with the capability
of cost-effective high-volume manufacturing of devices. In this work, ultra-thin, flexible Y-microreactors with microchannels
of 100 μm width and 30 μm depth were fabricated in thermoplastic polymer foils. The fluidic pattern was hot roll embossed
in 125 μm thick poly-methyl-methacrylate (PMMA) and 130 μm thick cyclic-olefin-copolymer (COC) films using a dry-etched microstructured
silicon wafer as a flat embossing tool in a laminator. The sealing of the channels was performed with two different techniques,
one based on lamination of SU8 dry film resist (DFR) and the other one based on spin-coated poly-dimethylsiloxane (PDMS).
Testing of the interconnected microreactor was carried out using two dye colorant solutions to demonstrate mixing. 相似文献
3.
4.
I. A. Metwally 《Sensing and Imaging: An International Journal》2015,16(1):1-18
This paper presents a new design of a side-looking “flat spiral” self-integrating Rogowski coil that is wound by twin coaxial cable with individual sheath. The coil is tested with different impulse current waveforms up to 7 kA peak value to improve its performance. The coil design is optimized to achieve bandwidth and sensitivity up to 7.854 MHz and 3.623 V/kA, respectively. The coil is calibrated versus two commercial impulse-current measurement devices at different coil-to-wire separations, coil inclination angles, and impulse current waveforms. Distortion of the coil output voltage waveform is examined by using the lumped-element model to optimize the connections of the four cable winding sheaths and the coil termination resistance. Finally, the coil frequency response is investigated to optimize the coil design parameters and achieve the desired bandwidth (large low-frequency time constant), high rate of rise, no overshoot, very small droop, high rate of fall, and no backswing. 相似文献
5.
I. A. Metwally 《Instruments and Experimental Techniques》2016,59(2):250-257
This paper presents design, calibration and testing of a new tape-wound Rogowski coil for measuring large-magnitude pulsed currents. The performance of the coil is tested by different impulse current waveforms up to 9 kA peak value. The coil is calibrated versus two commercial impulse-current transformers with different impulse current waveforms. The coil design is optimized to work in the differentiating mode and achieve useful bandwidth and sensitivity up to 1 MHz and 102 mV/kA, respectively. Waveform distortion of the coil output voltage is examined by using the lumped-element model to optimize the parameters of the external passive integrator. It is desired to optimize the integrator parameters and achieve the desired bandwidth without having droop and backswing. To do so, the coil frequency response is investigated by making fast Fourier transform (FFT) of the impulse current waveforms and PSPICE simulation of the lumped parameter equivalent circuit of Rogowski coil and the external integrator. Finally, it is found that the PSPICE calculated sensitivity for the optimized integrator parameters deviates from the corresponding measured one by a percentage relative error of–0.05%. 相似文献
6.
7.
The fast and maximum thermal neutron fluxes from the DD-109 neutron generator at the University of Sharjah were experimentally measured by the activation technique using different neutron reactions. The thermal and fast neutron fluxes were found to be 2.960 × 10~6 and6.186 × 10~7 n/cm~2 s, respectively. This was done to verify the modeling results for the optimum moderator thickness needed to maximize the thermal neutron flux. The optimum moderator thickness was found to be between 3.5 and4 cm. The present data were compared with the detailed MCNP model-based calculation performed in earlier work to simulate the generator. 相似文献
8.
M. M. Metwally 《国际能源研究杂志》1993,17(5):413-424
This paper examines the impact of the fluctuations in oil revenue on the import patterns of the GCC countries. The study is a disaggregated analysis of the relationship between imports of various commodity groups, using two-digit SIT classifications and per capita income in each of the six members of the Gulf Cooperation Council (GCC). The research shows that the reduction in oil revenue since late 1982 has completely upset the import-income relationship which was developed during the boom years, 1974–1981. 相似文献
9.
Studies have been carried out on the synthesis, composition, stability, and ion-exchange properties of cationic resins from poly-condensation of Egyptian corncobs (as a source of inexpensive and renewable material) with phenol in the presence of parafonnaldehyde as a crosslinking agent. These exchangers are stable in water, organic solvents, thermal treatment and mineral acids (1 M). The samples, having a cation-exchange capacity up to 3.22 mEq g?1 of dry resin, are being introduced as a new cationic exchanger. The cationic exchanger shows a limited affinity for the binary separation of some divalent cations. 相似文献
10.
M. S. Metwally M. F. El-Hadi M. A. El-Wardany A. Abdel Razik 《Journal of Materials Science》1990,25(10):4223-4225
Samples of an acidic cation exchanger have been prepared by sulphonation of acrylonitrile butadiene styrene copolymer previously cross-linked with phenol-formaldehyde resin. The samples having a cation exchange capacity of 3.48 meqg–1, are being introduced as new catalysts in the hydrolysis of ethyl acetate. The synthesized cation exchanger shows good thermal and chemical stability. Hydrolysis rate constants (K
r values) for the catalysed reaction have been determined. The efficiency of the resin catalyst,q, is shown to be a function of resin concentration. 相似文献