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ZHANG Jia-wei ZONG Zhi-min WANG Tao-xia XIE Rui-lun DING Ming-jie CAI Ke-ying HUANG Yao-guo GAO Jin-sheng WU You-qing WEI Xian-yong 《中国矿业大学学报(英文版)》2007,17(2):197-200
Five Shenfu char samples were prepared from Shenfu raw coal at different temperatures (950, 1100, 1200, 1300 and 1400℃) using a muffle furnace. Demineralization of the char samples was performed by treating them with 10% nitric acid for 10 min in a CEM Discover microwave reactor. The gasification of the chars, and corresponding demineralized chars, in a carbon dioxide (CO2) atmosphere was conducted in a Netzsch STA 409Cl31F tempera- ture-programmed thermogravimetry apparatus. The effects of charring temperature and demineralization on the gasification reactivity of chars were systematically investigated. The results show that a char formed at a lower temperature is more reactive except for demineralized char formed at 1100℃, which is less reactive than char formed at 1200℃. Demineralization decreases the char reactivities toward gasification with CO2 to a small extent. 相似文献
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依次用体积比为1:2的甲醇/四氢呋喃和二硫化碳(CS2)/四氢呋喃混合溶剂对新疆黑岱沟(HDG)煤进行彻底萃取.在40℃和60℃下用30%双氧水溶液氧化得到萃余煤,用GC/MS分析了反应混合物中的水不溶物的CS2可溶物(A)和水溶液的苯可溶物(B),并用FTIR分析了反应混合物中水溶液的苯不溶物(C),以寻求煤的高附加值利用及其大分子结构信息.结果表明:在A中均检出多种羧酸和长链烷烃,在60℃下氧化所得A的收率较高,且其中含氧化合物的种类更多;在40℃下氧化所得B中只检出蒽和少量直链烷烃,在60℃下氧化所得B中只检出少量的蒽;C中羟基和取代芳环含量较高,只是60℃下氧化所得的C的收率更高,且含羟基更丰富. 相似文献
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