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排序方式: 共有94条查询结果,搜索用时 203 毫秒
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2.
Characterization and wear behavior of modified silicon nitride 总被引:3,自引:0,他引:3
E. Carrasquero A. Bellosi M.H. Staia 《International Journal of Refractory Metals and Hard Materials》2005,23(4-6):391-397
Silicon nitride-based materials are applied to many tribological components because of their superior thermal and mechanical properties and corrosion resistance. The purpose of this study is to investigate the wear performance of modified silicon nitride which contained 3 wt.% La2O3 and 3 wt.% Y2O3. The relationships between microstructure and mechanical properties have been also addressed. Vickers microhardness and toughness were measured, the later being determined by means of the direct crack measurement method (DCM). Scanning electron microscopy technique (SEM) coupled with energy dispersive X-ray spectroscopy (EDS) was used for the morphological characterization of the samples as well as for the characterization of the wear scars. Wear properties were studied under a load of 10 N by using the ball-on-disk tribometer. AISI 52100 steel balls and balls of WC + 6% Co (6 mm diameter) were used as static counterparts, respectively. Steady state friction coefficients of 0.66 and 0.62 were measured for the tribological pairs WC + 6 % Co/Si3N4 and AISI 52100/Si3N4, respectively. The wear mechanism was determined in each case, and comparison between the wear performance of the traditional and modified silicon nitride is also presented. 相似文献
3.
Nanoindentation Characterization of Submicro- and Nano-Sized Liquid-Phase-Sintered SiC Ceramics 总被引:1,自引:0,他引:1
Stefano Guicciardi Diletta Sciti Cesare Melandri Alida Bellosi 《Journal of the American Ceramic Society》2004,87(11):2101-2107
Submicro- and nano-sized liquid-phase-sintered SiC ceramics were mechanically tested by nanoindentation in the peak load range 5–400 mN. The submicro-sized sample showed a marked indentation size effect which the nano-sized samples did not exhibit. The relevance of indentation depth with respect to the microstructural scale has been outlined. In the investigated grain-size range, the hardness dependence on the grain size could be described by a load-dependent inverse Hall–Petch relation. Young's modulus was less microstructure- and load-dependent. Because of the very fine microstructure, the nano-sized SiC materials gave lower elastic values than the submicro-sized SiC ceramic. 相似文献
4.
Gert Roebben Omer Van der Biest Diletta Sciti Alida Bellosi Corneliu Sarbu Tom Lauwagie 《Journal of the American Ceramic Society》2005,88(8):2152-2158
Detailed stiffness and internal friction ( Q −1 ) versus temperature curves were obtained for liquid-phase-sintered silicon carbides using advanced resonant beam analysis up to 1400°C. As-sintered materials display a stable Q −1 -peak near 1100°C, superimposed on an increasing background. The change of stiffness associated with the damping peak is quantitatively related to the amount of matter in pockets of the amorphous intergranular phase in which the refractory SiC matrix grains are embedded. The successful removal of the amorphous pockets by annealing at 1900°C is deduced from the disappearance of the damping peak and confirmed with transmission electron microscopy. 相似文献
5.
The crystal structure and molecular conformation of 2-cyano-4-bromo-4′-N,N-diethylaminoazobenzene (C17H17N4Br, mol. wt. = 357·2 a.m.u) has been determined from X-ray diffraction data; triclinic, P (No. 2), a = 10·132(11) Å, b = 12·216(16) Å, c = 6·966(11) Å, α = 104·21(9)°, β = 92·67(12)°, γ = 97·22(7)°, V = 826·5(9) Å3, Z = 2, Dc = 1·436 g cm?3, F(000) = 378, λ(MoKα) = 0·71069 Å, μ(MoKα) = 26·0 cm?1. The structure was solved by the multiple solution direct method and refined by full-matrix least-squares to R = 0·059 for 1538 independent observed reflections. The azobenzene skeleton is planar to within 0·06 Å. Most significant bonding data are: NN, 1·290(8) Å; BrC, 1·866(6) Å; mean CN (azo) 1·380(8) Å; NNC, 113·6(4) and 115·3(4)°; NCC (cis relative to NN) 125·9(4)° and 126·7(4)°; NCC (trans) 116·8°(5)° and 116·1(4)°. 相似文献
6.
A solid state bonding technique under hot pressing was used for joining alumina with thin metal sheets of Ni, Cu and Fe. The microstructure and microchemistry of the ceramic–metal interface and of the fracture interface were examined using scanning electron microscopy (SEM) energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD), in order to identify the adhesion mechanisms and the nature of strength limiting flaws. Interaction between the selected metals and alumina can be physical or physico-chemical in nature: very low amounts of interfacial compounds were formed, depending on the processing conditions and on the presence of oxygen in the system. Fracture and toughness tests indicated that high ceramic–metal interface strengths (up to 177 MPa) were achieved under the adopted processing conditions and that strength and toughness were directly related. Moreover, an increase in hardening in the metal interlayer at a distance of 2–3 m from the interface was observed in the samples with high strength values. The mechanical behaviour was related to several factors that strongly depend on the bonding conditions: plastic deformation of the metal, metal creep, metal intrusion and diffusion into alumina, and chemical reactions at the interface. © 1998 Chapman & Hall 相似文献
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9.
Characterization of hot-pressed silicon nitride-based materials by microhardness measurements 总被引:2,自引:0,他引:2
The microhardness A Si3N4-based materials may be related to their phase and chemical compositions and to microstructural parameters such as porosity, grain size and secondary phases. By reducing the amount of intergranular phase, the microhardness may reach values up toHV
500 = 3000 kg mm–2. Moreover, a comparison among different materials must include the microhardness tests in a wide range of values of the applied load. The relationd
n
=B
1 +B
2
d
2, obtained from those of Meyer and Kick, gives two constants:B
1 may represent one class of materials andB
2 is specific for each single material. 相似文献
10.
E. Verné E. Bona A. Bellosi C. Vitale Brovarone P. Appendino 《Journal of Materials Science》2001,36(11):2801-2807
Na2O-CaO-SiO2 glass- and glass-ceramic matrix/Ti particle biocomposites have been prepared by means of two processes: pressureless sintering and hot pressing. Time and temperature sintering conditions were optimised on the basis of the thermal properties of mixed glass and Ti powders, determined by Differential Thermal Analysis, Differential Scanning Calorimetry, Hot Stage Microscopy, Dilatometry. Each sintered sample was characterised by means of X-ray diffraction, Scanning Electron Microscopy, EDS, density measurements, Young's modulus, induced crack propagation by Vickers indentations, three point bending test, K
IC measurements. The in vitro bioactivity was investigated on the sintered composites by soaking them in a simulated body fluid (SBF) with the same ion concentration of the human plasma. 相似文献