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Here, a novel melt electrospinning method to produce few‐micron and nanometer thick fibers is presented, in which a polymer‐coated wire with a sharp tip is used as the polymer source. The polymer coating is melted via Joule heating of the source wire and extracted toward the target via electrostatic forces. The high viscosity and low charge density of polymer melts lower their stretchability in melt. The method relies on confining the Taylor cone and reducing initial jet diameter via concentrated electrostatic fields as a means to reduce the diameter of fibers. As a result, the initial jet diameter and the final fiber diameter are reduced by an order of magnitude of three to ten times, respectively, using wire melt electrospinning compared to syringe‐ and edge‐based electrospinning. The fiber diameter melt electrospun via this novel method is 1.0 ± 0.9 µm, considerably thinner than conventional melt electrospinning techniques. The generation of thin fibers are explained in terms of the electrostatic field around the wire tip, as obtained from finite element analysis (FEA), which controls the size and shape of the melt electrospun jet.  相似文献   
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Tripti Vashisth 《LWT》2011,44(7):1649-1657
Three drying technologies [i.e., vacuum belt drying (VBD), hot air drying (HAD), and freeze drying (FD)] were evaluated for the processing of muscadine pomace in terms of their impact on drying time requirement, moisture content (MC), water activity (aw), total phenolics content (TPC), and antioxidant activity (AA). Muscadine pomace discs of two thicknesses (2 and 4 mm) were dried using 16 different time-temperature combinations for VBD, 12 different time-temperature and air velocity combinations for HAD, and one treatment for FD. The TPC and AA in lyophilised samples were 583 ± 8 and 608 ± 16 μmol GAE/g d.w. and 2.21 ± 0.15 and 2.30 ± 0.17 mmol Fe2+ E/g d.w. for the 2 and 4 mm thick discs, respectively. The VBD treatment of 60-80-100-100 °C for 60 min (i.e., TV2) for 2 mm thick discs showed the highest TPC value, and no significant (P > 0.05) differences were observed in AA of 2 mm thick discs dried by VDB and FD. The TPC and AA for the VBD treatment of 60-80-100-100 °C for 90 min and HAD treatment of 70 °C at 0.6 m/s for 3 h for the 2 mm thick discs were not significantly (P > 0.05) different compared to freeze dried samples. For 4 mm thick samples, the TPC and AA for the VBD treatments of 60-80-100-100 °C, 60-90-120-120 °C, 70-90-110-110 °C, 80-90-100-100 °C, and 90-105-120-120 °C for 90 min as well as 70-90-110-110 °C for 60 min were not significantly (P > 0.05) different compared to those for freeze dried discs. VBD is a promising drying technology, as the resultant products possessed high TPCs and were dried in less than ¼ of the time compared with that of FD.  相似文献   
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As part of developing a computer-aided diagnosis system for the early detection/classification of brain tumors, this paper presents an Information set-based sigmoid features and a classifier using MR images. A set of information values constituting an Information set springs forth on fitting a membership function to a set of information source (attribute) values, the sum of which gives the certainty/uncertainty in the attribute values to a class, say, the pixel intensities in an MRI to a disease class. This certainty/uncertainty representation is not attempted in the existing methods, thus failing to produce efficient features. To this end, Hanman-Anirban (HA), Mamta-Hanman (MH), and Possibilistic Renyi entropy functions are employed including the pervasive membership function in the generation of four types of sigmoid features. The pervasive Information set results from the use of pervasive membership function that is a combination of the membership function and non-membership function. Furthermore, the Shannon-Hanman Transform classifier is formulated using the t-norm of error vectors between the training and test feature vectors, and its parameters are learned through the Pervasive learning model. The proposed system comprising features, classifier, and the learning model is tested on two Brain MRI’s datasets. The t-norm based fusion of two features has also been experimented. The Shannon-Hanman Transform classifier along with the Pervasive learning model is found to outperform the other classifiers in the literature with the highest accuracy of 99.51% for the two-class classification with a fusion of two features and 99.09% for the three-class classification with a sigmoid MH feature.

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A new type of potassium doped manganese oxide nanowires were synthesized using a simple hydrothermal route. The reduction of MnO4- in the presence of acetate species led to the formation of the Multi-filamentous nanowire structure. Detailed TEM and chemical characterizations indicated that potassium ions were homogeneously distributed in the nanowires. XPS results show a clear binding energy shift (1 eV) for K(2p) peak in nanowires compared with its starting material of KMnO4. Detailed synthetic condition investigation indicated that the presence of acetate ions played an important role in the formation of such a type of nanowires other than layered structures.  相似文献   
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The effects of annealing temperature on the sol–gel-derived ZnO thin films deposited on n-Sh100 i substrates by sol–gel spin coating method have been studied in this paper.The structural,optical,and electrical properties of ZnO thin films annealed at 450,550,and 650 °C in the Ar gas atmosphere have been investigated in a systematic way.The XRD analysis shows a polycrystalline nature of the films at all three annealing temperatures.Further,the crystallite size is observed to be increased with the annealing temperature,whereas the positions of various peaks in the XRD spectra are found to be red-shifted with the temperature.The surface morphology studied through the scanning electron microscopy measurements shows a uniform distribution of ZnO nanoparticles over the entire Si substrates of enhanced grain sizes with the annealing temperature.Optical properties investigated by photoluminescence spectroscopy shows an optical band gap varying in the range of 3.28–3.15 eV as annealing temperature is increased from 450 to 650 °C,respectively.The fourpoint probe measurement shows a decrease in resistivity from 2:1 10 2to 8:1 10 4X cm with the increased temperature from 450 to 650 °C.The study could be useful for studying the sol–gel-derived ZnO thin film-based devices for various electronic,optoelectronic,and gas sensing applications.  相似文献   
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Zn2SiO4:Mn2+ particles are used as green phosphors in plasma display panels and cathode ray tubes. In this study, we report the synthesis of zinc silicate phosphors by flame spray pyrolysis using different Zn-sources and under different process conditions. The XRD and luminescence measurement showed the phosphors prepared from Zn-nitrate source to have better crystallinity and emission characteristics. The luminescence properties of the phosphor particles were found to improve both at higher methane flow rates during pyrolysis and at higher annealing temperatures.  相似文献   
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We use first-principles-based density functional theory (DFT) calculations to investigate the structural, elastic, and electronic properties of various pristine and oxygen (O)-functionalized double transition metal (DTM) MXenes with general formulas of M2′M′′C2 and M2′M′′C2O2, where M′ = Mo, Cr and M′′ = Ti, V, Nb, Ta. The dynamic stability of the DTM MXenes are assessed and elastic stiffness constants (Cij) are used to investigate the mechanical stability and properties of the compositions. The calculated elastic properties of the pristine Mo-based MXenes are found to be superior compared to Cr-based compounds. Furthermore, the O-functionalized MXenes exhibit improved in-plane elastic constants, Young's moduli, and shear moduli compared to their pristine counterpart. We observe that the hybridization of the energy states results in stronger covalent interactions as such increased elastic properties for the M2′M′′C2O2 MXenes. Ashby plot clearly demonstrates superior materials properties of O-functionalized Mo-based DTM MXenes compared to other commonly known two-dimensional materials. All the MXenes exhibit metallic character evident from the density of states (DOS) calculations. Additionally, the work functions are studied and the calculated values are higher in the case of O-functionalized MXenes. Overall, this work will be a guide for future investigations on the mechanical properties of DTM MXenes for their targeted applications in structural nanocomposites.  相似文献   
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