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排序方式: 共有133条查询结果,搜索用时 0 毫秒
1.
Todd?L.?KurthEmail author Girma?Biresaw Atanu?Adhvaryu 《Journal of the American Oil Chemists' Society》2005,82(4):293-299
The frictional behaviors of methyl oleate (MO), methyl palmitate (MP), methyl laurate (ML), and methyl stearate (MSt) as additives
in hexadecane have been examined in a boundary lubrication test regime using steel contacts. It was found that the transient
attributes of coefficient of friction (COF)-time spectra are a sensitive measure of adsorption equilibria. Critical additive
concentrations were defined and used to perform novel and simple Langmuir analyses that provide an order of adsoprtion energies:
MSt>MP>MO≥ML. Application of Langmuir, Temkin, and Frumkin-Fowler-Guggenheim adsorption models via nonlinear fitting of a general cooperative model demonstrates the necessary inclusion of cooperative effects in the applied
model. In agreement with the qualitative features of steady-state COF-concentration plots, MSt modeling requires minimal cooperative
interaction terms. However, MO, MP, and ML data require large attractive interaction terms to be adequately fitted. Primary
adsorption energies calculated via the cooperative model are necessarily decreased, whereas total adsorption energies correlate well with values obtained via critical concentration analyses. These results and comparisons with previous adsorption studies of MO and MSt suggest that
primary (ester-surface) and secondary (alkyl-surface) adsorbate-adsorbent, adsorbate-adsorbare, and (free-additive) adsorpt-adsorpt
interactions collectively determine both the calculated primary and the cooperative interaction energies. 相似文献
2.
The feasibility of chromium(VI) to induce graft copolymerization of methyl methacrylate onto nylon-6 was investigated in the presence of nitrogen. The rate of grafting was determined by varying monomer concentration, chromium(VI) concentration, temperature, acidity of the medium, solvents, inorganic salts, and redox system. The graft yield increases significantly by increasing the monomer concentration. The graft yield increases with increase of [Cr(VI)] up to 0.025 mole/liter. With further increase of [Cr(VI)], the graft yield decreases. The increase of acid concentration up to 0.395 mole/liter results the increase in graft yield. Beyond this concentration the graft yield decreases. The graft yield increases with increase in temperature up to 55°C and thereafter it decreases. The graft yield is medium dependent. The graft yield increases with increasing thiourea concentration upto 0.0025 mole/liter but beyond this concentration, the percentage graft yield decreases. A suitable kinetic scheme has been proposed and the rate equation has been evaluated. 相似文献
3.
Influence of Distributed Particle Size on the Determination of the Parabolic Rate Constant for Oxidation by the Powder Method 总被引:1,自引:0,他引:1
The established analysis for the study of oxidation using powder specimens is based on the assumption of monosized particles. The experiments, however, are conducted on powders with a distributed particle size. Here we present a statistical approach for the calculation of the rate constant for oxidation. The results of the analysis are applied to new data on oxidation studies of dense powders of silicon carbonitride amorphous ceramics. The monosized model requires a wide range of values for the rate constant to fit the short term and the long-term data, leading to considerable ambiguity in the estimate of the parabolic rate constant, k p , for oxidation. In contrast the statistical model fits over the entire range of data, yielding a much more reliable value for k p . For example, the monosized approach gave a value in the range 19.7 × 10−18 < k p < 2.7 × 10−18 m2 /s. In contrast, the statistical model yields a specific value of 4.5 × 10−18 m2 /s. 相似文献
4.
Bio-Inspired Artificial Fast-Adaptive and Slow-Adaptive Mechanoreceptors With Synapse-Like Functions
Hung Quang Huynh Tran Quang Trung Atanu Bag Trung Dieu Do M. Junaid Sultan Miso Kim Nae-Eung Lee 《Advanced functional materials》2023,33(42):2303535
Development of artificial mechanoreceptors capable of sensing and pre-processing external mechanical stimuli is a crucial step toward constructing neuromorphic perception systems that can learn and store information. Here, bio-inspired artificial fast-adaptive (FA) and slow-adaptive (SA) mechanoreceptors with synapse-like functions are demonstrated for tactile perception. These mechanoreceptors integrate self-powered piezoelectric pressure sensors with synaptic electrolyte-gated field-effect transistors (EGFETs) featuring a reduced graphene oxide channel. The FA pressure sensor is based on a piezoelectric poly(vinylidene fluoride-trifluoroethylene) (P(VDF-TrFE)) thin film, while the SA pressure sensor is enabled by a piezoelectric ionogel with the piezoelectric-ionic coupling effect based on P(VDF-TrFE) and an ionic liquid. Changes in post-synaptic current are achieved through the synaptic effect of the EGFET by regulating the amplitude, number, duration, and frequency of tactile stimuli (pre-synaptic pulses). These devices have great potential to serve as artificial biological mechanoreceptors for future artificial neuromorphic perception systems. 相似文献
5.
Betal Atanu Bera Jayanta Alam Mahfooz Gandi Appala Naidu Sahu Satyajit 《Journal of Computational Electronics》2022,21(1):227-234
Journal of Computational Electronics - The strain- and electric field-dependent electronic and optical properties of monolayer GaInS2 have been calculated using density functional... 相似文献
6.
Joonho Shin Atanu Naskar Dongjoon Ko Semi Kim Kwang-sun Kim 《International journal of molecular sciences》2022,23(12)
Owing to the rapid spread of antibiotic resistance among Staphylococcus species, effective and low-risk alternatives to antibiotics are being actively searched. Thymol (THO), the most abundant component of the oil extracted from thyme, can be considered as a natural antibacterial alternative. However, the low antibacterial activity and non-selectivity of THO limit its usage as a universal anti-Staphylococcus agent. Herein, we report the bioconjugation of THO with ZnO nanoparticle (ZO), which resulted in the TZ nanocomposite (NC), as a potent and selective antibacterial agent against Staphylococcus species, particularly S. epidermidis. The cell-free supernatant (CFS) of ATCC 25923 cultures was employed for the production of TZ NC. Successful production of TZ NC was confirmed via X-ray diffraction (XRD), Fourier-transform infrared (FT-IR) spectroscopy, and ultraviolet–visible (UV–Vis) studies. TZ NC had selective efficacy against Staphylococcus species, with MIC values 2–32-fold lower than THO. The antibacterial mechanisms of TZ NC are proposed to involve membrane rupture, suppression of biofilm formation, and modulation of new cell wall and protein-synthesis-associated cellular pathways. Its biocompatibility against HCT116 cells was also checked. Our findings suggest that the TZ nanocomposite could improve the selectivity and bactericidal activity of THO against target species. 相似文献
7.
8.
Hong-Sik?Hwang Atanu?Adhvaryu Sevim?Z.?ErhanEmail author 《Journal of the American Oil Chemists' Society》2003,80(8):811-815
Synthetic lubricant basestocks were prepared from epoxidized soybean oil (ESO) and 2-ethylhexanol (2-EH) to be used alone
or with polyalphaolefin (PAO). Sulfuric acid-catalyzed reaction of ESO with 2-EH involves a ring-opening reaction at the epoxy
group followed by transesterification at the ester group. Reaction with other catalysts including p-toluenesulfonic acid, Dowex 50W-8X, boron trifluoride, and sodium methoxide was also examined. Pour points of the products
were observed as lows as −21 and −30°C without and with 1% of pour point depressant, respectively. When the hydroxy groups
in the products were esterified with an acid anhydride, lower pour points were observed. Pour point depression of the product
by adding PAO has been tested. Oxidative stability of the product was examined using pressurized DSC and compared with those
of synthetic lubricant basestocks, PAO, and a synthetic ester. 相似文献
9.
Nanoscale silver cluster protected by sodium polyacrylate (PAA) was prepared through the reduction of aqueous silver nitrate solution containing PAA. PAA concentration was varied against a fixed concentration of silver nitrate to optimize the PAA to metal ratio, in which stable colloidal solution of silver nanoparticles of 7 ± 3 nm size could be obtained. These PAA-protected silver nanoparticles in clusters of nanoscale dimension (nanoclusters) were dispersed into the artificial heterogeneous matrix fabricated from aqueous solution of polyacrylate and protein (bovine serum albumin, BSA) by adjusting the pH in the acidic region. PAA-protected Ag-nanoparticle and Ag/PAA-BSA composites were characterized by UV-VIS spectroscopy and TEM. 相似文献
10.
This paper provides an alternative test procedure for the problem oftesting of normal mean for one sided alternative when the variance is known in case of costly trials. The proposed test is based on a sampling scheme which we call 'continuous adaptive design'. Some exact andasymptotic results related to the test and design are studied. 相似文献